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36621results about How to "Suitable for industrial production" patented technology

Mono-active center Ziegler-Natta catalyst for olefinic polymerization

ActiveCN1884311AEasy to prepareHigh activity copolymerizationAluminoxaneZiegler–Natta catalyst
The invention relates to a new catalyst for single active central Ziegler-Natta alkene polymerization. Said catalyst takes salicylal containing dentate or substituted salicylal derivatives as electrons, and is prepared by adding pretreated carrier, metallic compound and electrons into magnesium compound / tetrahydrofuran solution. The catalyst can produce ethane homopolymer and copolymer with narrow molecular weight distribution (1.6-3.8) and even comonomer distribution, with high activity and under action of adjuvant catalyst of alkyl aluminium and alkyl aluminoxanes. The ethane polymerization, homopolymerization or combined polymerization of ethane and 1- olefin, ring olefin and polar monomer through slurry method or gas phase method by using said catalyst can be realized.
Owner:SHANGHAI INST OF ORGANIC CHEMISTRY - CHINESE ACAD OF SCI

High-performance two-dimensional layered Ti3C2-MXene membrane, preparation method thereof and application of membrane in water treatment

The invention belongs to the technical field of membrane preparation and water purification and discloses a high-performance two-dimensional layered Ti3C2-MXene membrane, a preparation method thereof and an application of the Ti3C2-MXene membrane in water treatment. The method comprises steps as follows: (1), Ti3AlC2 powder and an HF solution are mixed, stirred for a reaction, centrifugally washed and dried, and Ti3C2 powder is obtained; (2), the Ti3C2 powder and a solvent are mixed, stirred for the reaction, washed and dried, and treated powder is obtained; (3), the treated powder is dissolved in the solvent and subjected to ultrasonic treatment and centrifugation, a liquid supernatant is taken and dried, and a two-dimensional nanosheet is obtained; (4), a solution is prepared from the two-dimensional nanosheet and deposited on a porous substrate with a nano self-assembly technology, and the high-performance two-dimensional layered Ti3C2-MXene membrane is obtained. The membrane has ultrahigh water flux, higher selectivity and good mechanical property and stability; the method is simple, low in energy consumption and cost, good in repeatability and wide in applicability.
Owner:SOUTH CHINA UNIV OF TECH

Electrostatic spinning nanofiber membrane as well as preparation method thereof

The invention provides an electrostatic spinning nanofiber membrane as well as a preparation method thereof. The electrostatic spinning nanofiber membrane provided by the invention comprises a fiber membrane obtained by electrostatically spinning a high-melting-point polymer and a fiber membrane obtained by electrostatically spinning a low-melting-point polymer, wherein the difference on the melting points of the high-melting-point polymer and the low-melting-point polymer is not less than 10 DEG C. The electrostatic spinning nanofiber membrane provided by the invention is multipurpose and can be applied to the fields such as biomedicines, energy and chemical industry, gas and liquid filtration, waterproofness and windproofness, windproofness and heat insulation, moisture permeability and ventilation, environmental management and semiconductor sensors. According to the electrostatic spinning nanofiber membrane provided by the invention, electrostatic spinning is respectively carried out on the high-melting-point polymer and the low-melting-point polymer, and the high-melting-point polymer fiber membrane and the low-melting-point polymer fiber membrane obtained are composited and hot-pressed to obtain the electrostatic spinning nanofiber membrane. The preparation method provided by the invention is high in production efficiency and low in energy consumption, and is suitable for industrial production.
Owner:ZHEJIANG WEIXING IND DEV

Method for preparing electrodes of super capacitor based on nickel foam and products thereof

The invention discloses a method for preparing electrodes of a dissymmetric super capacitor based on nickel foam. The method comprises the steps: washing the nickel foam, soaking the nickel foam into a graphene oxide aqueous solution to obtain nickel foam in which graphene oxide deposits, serving the nickel foam in which the graphene oxide deposits as precursor materials, and respectively adopting a three-electrode method for preparaing a positive electrode and a negative electrode of the dissymmetric super capacitor, wherein the positive electrode is composed of composite materials of graphene, a carbon nanometer tube and the nickel foam, and the negative electrode is composed of composite materials of graphene, manganese dioxide and the nickel foam. The invention further discloses some other methods for preparing the electrodes of the super capacitor based on the similar principle, and products which correspond to the methods. By means of the methods and the products, respective high-ratio capacitance characteristics of the composite materials are fully played, and energy density of the super capacitor is improved. In addition, usage of various combined reagents can be avoided, and accordingly large-batch industrial production is conducted in a mode of convenient control, low cost and low energy consumption.
Owner:HUAZHONG UNIV OF SCI & TECH

Silicon-carbon composite material, lithium ion battery, and preparation method and application of silicon-carbon composite material

The invention discloses a silicon-carbon composite material, a lithium ion battery, and a preparation method and application of the silicon-carbon composite material. The preparation method of the silicon-carbon composite material comprises the steps: uniformly mixing silicon powder and silicon monoxide powder, then mixing with a solution containing an organic carbon source dispersant, and performing wet-process ball milling to obtain a slurry; uniformly mixing the slurry, graphite and a conductive agent, and performing spray drying to obtain spherical-like particles, wherein graphite is synthetic graphite and/or intermediate-phase graphite; mixing the spherical-like particles and asphalt, performing cladding processing under the inert atmosphere to obtain a cladded material; and then performing carbonizing processing to obtain the silicon-carbon composite material, wherein silicon powder, silicon monoxide powder, graphite and asphalt respectively accounts for 5-15%, 3-10%, 45-75% and 5-40% by weight of the sum of the above materials, and the organic carbon source dispersant and the conductive agent both accounts for 0.1-2% by weight of the sum of silicon powder, silicon monoxide powder and graphite. The silicon-carbon composite material has relatively good cycle performance, and can be directly used as a cathode material of the lithium ion battery. The preparation method is simple in technology, low in cost and applicable to industrial production.
Owner:SHANGHAI SHANSHAN TECH CO LTD

Method for extracting and refining rutin

A method for extracting and refining rutin comprises the following steps of (1) extraction: smashing raw materials, adding organic solvent into the smashed raw materials, performing extraction for 2-4 times, mixing extracting solution and concentrating the mixed extracting solution to thick extract with organic solvent content smaller than or equal to 5wt%; (2) alkali dissolution-acid sediment: adding alkaline water into the thick extract, then heating the mixture and stirring, filtering the heated mixture, regulating pH of alkaline filtrate to be 3-4, standing, filtering, drying to obtain a rutin pure product; and (3) mother liquor treatment: enabling obtained acid mother liquor to penetrate through a chromatographic column filled with resin, after the acid mother liquor penetrates through the chromatographic column, firstly using deionized water to wash a column bed until outflow liquid is neutral and colorless, introducing eluent into the chromatographic column and collecting eluate until outflow liquid is colorless, concentrating the eluate to the volume which is 5-10% of the original volume in a pressure reduction mode, cooling the concentrated eluate to achieve crystallization, filtering, using the deionized water to elute a filter cake, and drying the eluted filter cake to obtain a mother liquor rutin product. The prepared rutin is high in yield and purity, and the quality of the rutin reaches the international standard.
Owner:湖南莱崔尔生物科技有限公司

Stannum and carbon composite nano-fiber film negative-electrode material and preparation method thereof

ActiveCN101626075AExcellent discharge performance and charge-discharge cycle stabilitySimple configuration processElectrode manufacturing processesSolventCarbon composites
The invention relates to stannum / carbon nano-fiber composite film material used in the negative electrode of a lithium ion battery and a preparation method thereof and also provides an assembly method of the stannum / carbon nano-fiber composite film material generated according to the preparation method and used as the electrode of the lithium ion battery. The preparation method comprises the following steps: preparing an uniform spinning solution by mixing a stannum precursor compound, a solvent, a precursor polymer of carbon nano-fibers and an organic solvent together; obtaining a polymer nano-fiber film by electro spinning according to a suitable electrostatic spinning technology; and obtaining a stannum / carbon nano-fiber composite film used in the negative electrode of the lithium ion battery through final treatment technologies, such as preoxidation, carbonization, and the like, thereby effectively collaborating the electrochemical performance of stannum / carbon nano-fibers and improving the specific capacity, the first charge-discharge efficiency and the cycle performance of the lithium ion battery.
Owner:BEIJING UNIV OF CHEM TECH

Viscose fiber with plant source anti-bacterial function and aromatic smell, and preparation method thereof

The invention discloses a viscose fiber with a plant source anti-bacterial function and aromatic smell. The viscose fiber is composed of a viscose spinning solution, an anti-bacterial agent and an aromatic agent, wherein the anti-bacterial agent is mixed powder of a mint extract and a isatis root extract, wherein the weight percentage of the mint extract accounts for 40%-80%; and the weight percentage of the isatis root extract accounts for 60%-20%; the aromatic agent is mint oil coated by microcapsules; the anti-bacterial agent accounts for 1%-8% of the mass of methyl cellulose in the viscose spinning solution; the mint oil accounts for 0.2%-1% of the mass of methyl cellulose in the viscose spinning solution; and the viscose fiber is prepared by adopting a wet spinning method by using the viscose spinning solution, the anti-bacterial agent and the aromatic agent. The plant source extracts and the plant source essential oil are used as the anti-bacterial agent and the aromatic agent; and the anti-bacterial agent and the aromatic agent are uniformly distributed in the fiber, so that the anti-bacterial function and the aromatic smell of the fiber are durable. Since the plant source extracts and the aromatic agent are natural substances extracted from the plants, so that the viscose fiber has no side effect to human body.
Owner:BESTEE MATERIAL (TSINGTAO) CO LTD

Composite hard carbon cathode material of lithium ion battery and preparation method thereof

The invention discloses a composite hard carbon cathode material of a lithium ion battery and a preparation method thereof, aiming at improving the first coulombic efficiency. In the composite hard carbon cathode material, a coating object is coated outside a hard carbon matrix, a precursor of the hard carbon matrix comprises a thermoplastic resin which forms the hard carbon matrix by pyrolysis, and a precursor of the coating object is an organic matter. The preparation method comprises the steps of curing, pyrolyzing, pulverizing and coating. Compared with the prior art, a curing agent and adopant are added to the resin for curing, the cured mixture is taken as a carbon source, and then the carbon source is pyrolyzed and coated to finally obtain the composite hard carbon cathode material; and the first reversible capacity of the obtained composite hard carbon cathode material is more than 455.2mAh/g and the first coulombic efficiency thereof is more than 79.4% in the case of 0.2C, thus the obtained composite hard carbon cathode material has high capacity and high first coulombic efficiency, meets the requirement of the lithium ion battery with high capacity, high multiplying power and excellent high and low temperature cycle performance on the charge-discharge performances of the cathode material, has low production cost and is suitable for industrial production.
Owner:JIXI BTR GRAPHITE IND PARK CO LTD +2

Comprehensive extraction method for extracting tea seed oil, tea saponin and tea seed polysaccharide from tea seeds or camellia seeds

InactiveCN101942355AHigh purityRealize comprehensive utilization and developmentSugar derivativesSteroidsOil processingSlag
The invention discloses a comprehensive extraction method for extracting tea seed oil, tea saponin and tea seed polysaccharide from tea seeds or camellia seeds, belonging to the process fields of grain and oil processing and byproduct extraction. The method comprises the following steps of: with shelled tea seeds as a raw material, firstly, cooking to produce oil; then, adding an exogenous enzyme to obtain a boiled oil layer of a first level an emulsified oil layer, a water layer and a slag layer through zymolysis, blanching and still standing; demulsifying the emulsified oil layer to take boiled oil of a second level; mixing the oil layers of the two levels; centrifugalizing to obtain the tea seed oil; depositing the water layer in alcohol to separate the tea saponin and the tea seed polysaccharide; leaching the slag layer with water or monohydric alcohol to further separate the tea saponin and the tea seed polysaccharide; and purifying a clear solution which is leached with the water or the alcohol with a macroporous absorption resin chromatography column, eluting a resin adsorbate with a base and then an ethanol and collecting an ethanol eluant to obtain high-purity tea saponin. The tea seed oil, the tea saponin and the tea seed polysaccharide are synchronously prepared, thus the invention realizes that a tea seed or camellia seed resource is comprehensively extracted and utilized and has the advantages of simple process, less needed equipment and low cost.
Owner:SHANGHAI NORMAL UNIVERSITY

Lithium ion battery anode material manganese lithium phosphate and preparation method thereof

The invention discloses a manganese/lithium phosphate of lithium iron battery positive pole material and a production method thereof, the technical issue to be solved is to improve electrochemical performances of the positive pole material. The material of the invention includes substrates of manganese/lithium phosphate which are covered by a carbon material covering layer, the lithium covering the manganese/lithium phosphate behind the carbon material covering layer is spherical and has microscopic characteristics of being near spherical, rhombic, tapered, tabular, layered or/and block-shaped as well as of having 0.5-30 mum long and short axles. The production method comprises the following steps of: production of nanometer particles, liquid phase mixed reaction, production of precursor, sintering treatment, covering organic substances. Compared with the prior art, the invention improves the electron conductivity of the manganese/lithium phosphate by covering with carbon liquid phase, the carbon sufficiently covers active materials to efficiently prevent particle aggregation, the invention has the characteristics of about 4V of discharge voltage, high discharge and charge capacitance, excellent circulation stability, high safety, simple process, low cost and little influence on the environment.
Owner:SHENZHEN CITY BATTERY NANOMETER TECH

A method for preparing porous silicon by magnesia thermal reduction

InactiveCN102259858AImprove luminous efficiencyStable electrochemical performanceSilicon compoundsMagnesiumOxide
The invention belongs to the synthesis field of porous silicon materials, and particularly relates to a method for preparing porous silicon by magnesiothermic reduction. The method comprises the following steps: carrying out magnesiothermic reduction reaction based on silicon oxide SiOx (x = 0.5-2) as a raw material to generate a mixture of silicon and magnesium oxide; and then selectively dissolving away magnesium oxide with an acid so as to ultimately obtain a self-supported porous silicon material. Compared with the previous conventional electrochemical anodic etching methods, the method provided by the invention has the advantages that the use of expensive monocrystal silicon wafers is avoided, but simple, easily available and low-cost silicon oxide is used as the raw material, thereby not only reducing the cost but also increasing the yield; and the method has the advantages of simple preparation process, environmental friendliness, high preparation efficiency and good repeatability, is more suitable for industrial production, and is expected to be widely applied in the fields of lithium ion secondary batteries, optical materials, biomedical devices, gas-sensitive devices, etc.
Owner:TONGJI UNIV

Polymer/graphene anti-static coating, preparation method and application thereof

The invention discloses a polymer/graphene anti-static coating, a preparation method and application thereof. The coating comprises the following constituents by weight percent: 0.01 portions to 0.5 portions of graphene; 0 portion to 10 portions of conductive additive; 90 portions to 100 portions of polymer; and solvent; the preparation method thereof comprises the following steps: completely and uniformly mixing graphene and conductive additive in advance by various manners; preparing a graphene-conductive additive compound system; using the compound system as a base, adding in conductive additive and polymer along with the solvent, completely and uniformly mixing to obtain the coating. Additionally, an anti-static film can be prepared by using different film forming technologies. The polymer/graphene anti-static coating, the preparation method and application thereof effectively solve the problems that graphene in polymer is easy to agglomerate and difficult to be uniformly dispersed in the preparation process of anti-static coating and film; the anti-static performance and mechanical performance of the coating and the film are greatly increased; meanwhile, the preparation technology is easy to be operated; the production is continuous, and the coating and film are suitable for industrial production.
Owner:苏州格瑞丰纳米科技有限公司

Novel fast-set anticorrosion and wear-resistant epoxy powder coating and preparation process thereof

The invention relates to the field of chemical coating, in particular to epoxy powder coating applied to material conveying steel belts in oilfield oil pumping pipelines or coal transportation in the oil industry. In a formula, the coating comprises the following components in percentage by weight: 32-56% of epoxy resin, 8-14% of curing agent, 30-50% of pigments and fillers, 2-10% of resin modifier and 2-6% of assistant, wherein the epoxy resin in the formula is bisphenol A type epoxy resin, a mixture of the bisphenol A type epoxy resin and phenolic aldehyde modified epoxy resin, and phenolic aldehyde modified epoxy resin, and the curing agent is phenolic hydroxyl resin. The epoxy powder coating disclosed by the invention belongs to fast-set anticorrosion and wear-resistant epoxy powder coating, has the granularity being 10-125 mu m, is applied under general curing conditions that the curing temperature is 180-200 DEG C and the curing time is 3-10min, can be regulated according to user needs and is superior to like products in anticorrosion performance, coating film mechanical performance and wear resistance, a preparation process is simple, the labour productivity can be obviously increased, and the epoxy powder coating is suitable for industrialized production.
Owner:JIANGSU LANLING POLYMER MATERIAL CO LTD
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