Patents
Literature
Hiro is an intelligent assistant for R&D personnel, combined with Patent DNA, to facilitate innovative research.
Hiro

169results about How to "Low raw material requirement" patented technology

Method for producing pitavastatin calcium raw material

The invention relates to a method for preparing the raw materials of pitavastatin calcium, which uses an (E)-7-[2-cyclopropyl-4-(4-fluorophenyl)-3-quinolyl]-5-hydroxyl-3- carbonyl-6-heptene acid ester as a beginning raw material to generate a heptenoic acid through being reduced and reacted by adding an alkali and an acid; a D-(+) benzyl methylamine is added to generate a mixture of a benzyl methylamine salt, and crystallize to separate out a (3R, 5S)-dihydroxy-7-[2-cyclopropyl-4-(4-fluorophenyl)-3-quinolyl]-6- heptenoic acid D-(+) benzyl methylamine through the different solubility of the mixtures in a separating agent, and the separating agent is a mixed liquid of a methyl isobutyl ketone and an acetone or an ethanol; finally adds lye to hydrolyze and prepare the pitavastatin calcium salt. The method of the invention is selectively reduced to a pair of isomers by using a determined reduction agent, generates salt by reacting with the D-(+) benzyl methylamine and effectively separates a needed isomer by utilizing the different solubility of various isomers to the separating agent. The invention has the advantages of simple preparing technique, low requirements for the raw materials and high conversion rate of the obtained products.
Owner:JIANGSU WANBANG BIOPHARMLS

New process for preparing modified melamine polyphosphate

The invention discloses a new process for preparing modified melamine polyphosphate, which comprises the following steps: (1) adding water, phosphoric acid and a modifier into a reaction kettle, and heating to 20-70 DEG C; (2) adding melamine, heating to 90-100 DEG C, and reacting for 2-5 hours; (3) cooling the product obtained after the reaction in the step (2), filtering, and drying; and (4) carrying out polymerization reaction on the product, which is subjected to the step (3), at 300-450 DEG C for 10-120 minutes. The synthesis and modification of the melamine polyphosphate are carried out synchronously, so that the invention has the advantages of short reaction time, low requirements for raw materials, simple and convenient technical operation, and low environmental pollution; the prepared melamine polyphosphate has the advantages of favorable compatibility with resin, low solubility in water, and excellent thermal stability, and the temperature can reach about 360 DEG C when the weight loss is 2%, so that the modified melamine polyphosphate can satisfy the processing requirements of no halogen and flame retardancy for glass fiber reinforced nylon and polyester.
Owner:ZHEJIANG RES INST OF CHEM IND CO LTD +2

Method for performing continuous low-energy-consumption salt removal by utilizing flow battery redox reaction as well as application thereof

The invention discloses Method for performing continuous low-energy-consumption salt removal by utilizing flow battery redox reaction as well as application thereof. The method comprises the step of removing salt through a salt-removing flow battery device, wherein the salt-removing flow battery device takes positive and negative electrode active flow materials as the positive and negative electrodes of the flow battery as well as takes a salt solution as electrolyte of the flow battery; and the salt-removing flow battery device also comprises an isolating device for isolating the salt solution from the positive and negative electrode active flow materials as well as also comprises an anion exchange membrane and a cation exchange membrane. The salt-removing flow battery device is low in flow electrode salt-removing work voltage, extremely low in energy consumption, high in specific capacity and high in cycle performance, and the positive and negative electrode materials can be reused,so that the true salt-removing aim can be achieved. The method provided by the invention is low in low energy consumption, can continuously perform electrochemical redox reaction and environment-friendly novel seawater desalination technology, and can be used for solving the problem of insufficient supply of fresh water resources.
Owner:SOUTH CHINA NORMAL UNIVERSITY

Separation process of natural free radical scavenger in Saxifraga tangutica and application of natural free radical scavenger

The invention relates to the technical field of separation of natural free radical scavengers in Saxifraga tangutica, in particular to a separation process of a natural free radical scavenger in Saxifraga tangutica and application of the natural free radical scavenger. The separation process comprises the following six steps: extraction, coarse separation via a microporous resin column, online free radical scavenger component screening, preparation via a reversed-phase preparative column, reversed-phase preparative liquid chromatographic purification of Fr1-1and hydrophilic/reversed-phase two-dimensional liquid chromatographic purification of Fr1-3. The method is low in cost, and product purity is greater than 95%; a technical means adopted by the invention can realize large-scale production: requirements on raw materials are not high, cost is low, and batch preparation is easy; room-temperature cold leaching extraction with methanol is adopted, so operation is easy; the microporous resin column is adopted for coarse separation, and a microporous resin separation material can be loaded in a medium-pressure column chromatography system, so large-scale production can be easily realized; and reversed-phase preparative liquid chromatography or hydrophilic preparative liquid chromatography used in separation and purification is a rapid isocratic method.
Owner:CHINA ACAD OF SCI NORTHWEST HIGHLAND BIOLOGY INST

Method for recycling valuable metal from sulfur concentrate cinders

The invention belongs to the technical field of mineral separation and metallurgy and particularly relates to a method for recycling valuable metal from sulfur concentrate cinders. The method comprises the following steps: sequentially adding bentonite and a calcium chloride solution into the sulfur concentrate cinders to form a mixed material; wetly grinding the mixed material; spraying water into the wetly-grinded mixed material to generate raw grains, and drying; roasting the dried grains by using natural gas to obtain iron grains and smoke; washing the smoke and filtering to obtain PbSO4 sediment, AgCl sediment and a single substance Au; adding iron blocks into a filtering solution to displace the single substances Cu, Au and Ag; filtering again and adding a sodium hydrosulfide solution into the filtering solution; adjusting the pH by using lime milk; filtering to obtain lead; and adding the lime milk into the filtering solution to adjust the pH, and filtering and drying to obtain Zn(OH)2. The method provided by the invention is simple in process and is efficient and environmental friendly; the requirements on raw materials are low and the recycling rate of the valuable metal is high; the valuable metal in the sulfur concentrate cinders is recycled by using a low production cost.
Owner:ZHAOJIN MINING +1

Tunnel slag tapping, sand and gravel processing and concrete processing and conveying integrated equipment and process

PendingCN110130920ASolve the transportation problemReduce in quantityTunnelsMixing operation plantSlagMaterial resources
The invention discloses a tunnel slag tapping, sand and gravel processing and concrete processing and conveying integrated equipment and process. The tunnel slag tapping, sand and gravel processing and concrete processing and conveying integrated equipment comprises mobile crushing equipment, wherein a discharging port of the mobile crushing equipment is sequentially connected with a material pre-sorting system, an aggregate processing system and a concrete processing system through a telescopic conveying belt group, and a discharging port of the concrete processing system is connected with aconcrete belt conveying system; after materials in a tunnel blasting area B are preliminarily crushed by the moving crushing equipment, the materials are transported into the pre-sorting system and the aggregate processing system to prepare fine aggregates and fine sand with different gradations, finally transported into the concrete processing system to prepare concrete, and transported to a tunnel construction area through the concrete belt conveying system for concrete construction after penetrating through a lining trolley. The manpower and material resources are reasonably utilized and distributed, the automatic construction of a tunnel is achieved, high flexibility and good safety performance are achieved, and the construction efficiency and quality of the tunnel are greatly improved.
Owner:GUIZHOU CHENGZHI HEAVY IND SCI TECH

Multi-degree of freedom human-simulated rigid-flexible mixing hand and manufacturing technology thereof

The invention discloses a multi-degree of freedom human-simulated rigid-flexible mixing hand and a manufacturing technology thereof, and belongs to the technical field of robots. Each soft finger includes metacarpophalangeal joints and interphalangeal joints, wherein a central air flue communicates with a central air cavity. A plurality of metacarpophalangeal joint air cavities surround the central air flues. A layer of fiber limiting threaded pipes are wound around the metacarpophalangeal joint air cavities. The central air flues and the tail ends of the multiple metacarpophalangeal joint aircavities are inserted into a finger base. A ventilating cavity is formed inside the body of a hard palm, and the hard palm fix the soft fingers through screws. Each central air flue, each metacarpophalangeal joint cavity and each central air cavity achieve air inflow through capillary silica gel hoses. The active degree of freedom is multiple, the human hand joint structure is simulated, and thejoint angle and motion relations are close to human hand parameters. Due to the joint type structure, compared with a continuous bent soft claw, the hand has the larger enveloping space, the grabbingperformance is better, the flexibility is good, and the hand has the good adaptability for soft and fragile objects and unstructured environment.
Owner:HARBIN INST OF TECH

Environmental-friendly organic silicon water blocking prevention agent for drilling fluid and preparation method and application thereof

The invention provides an environmental-friendly organic silicon water blocking prevention agent for a drilling fluid and a preparation method and application thereof. The organic silicon water blocking prevention agent comprises a hydrophobic group and a hydrophilic group, wherein the hydrophobic group is a polymethyl hydrosiloxane chain; the hydrophilic group is a sulfonic acid group and hydroxyl. The organic silicon water blocking prevention agent is prepared from methylsiloxane and vinyl siloxane through hydrolytic condensation reactions and grafting reactions with sulfonic acid group monomers. By adopting the organic silicon water blocking prevention agent provided by the invention, surface tension can be relatively well reduced, water wetting on the surfaces of pores can be turned into vapor wetting, flow-back of filtrate can be improved, gas permeability can be improved, and water blocking damage caused by a reservoir can be remarkably reduced; in addition, the organic silicon water blocking prevention agent is low in foaming rate, good in foam inhibition and elimination property, easy in preparation raw material obtaining, safe and feasible in reaction condition and easy inindustrial production.
Owner:BC P INC CHINA NAT PETROLEUM CORP +1

Boron-free high-performance glass fiber and preparation method thereof

The invention discloses a boron-free high-performance glass fiber and a preparation method thereof and belongs to the technical field of materials. The boron-free high-performance glass fiber is prepared from the following raw materials in percentage by weight: 30-55% of blast furnace slag, 1-15% of fly ash, 42-50% of quartz sand, 0-15% of zinc oxide, 0-2% of magnesium oxide and 0-3.5% of calcium oxide. According to the boron-free high-performance glass fiber, the adversely effects of the volatilization of boron on a kiln, the environment and the production cost are avoided, and the boron-free high-performance glass fiber has the advantages of excellent performance, reasonable process parameters, low production cost and environmental friendliness and furthermore, the raw materials can directly adopt industrial-grade raw materials and the effect is not affected.
Owner:UNIV OF JINAN

Fine purification method for sterol

The invention relates to a refining method of high content natural plant sterol, the natural plant crude sterol with the weight percentage of 35 percent to 80 percent weight content is selected and added in petroleum ether or other mixed solvents for stirring and filtration, a solid phase I is selected, the solid phase I is added in the petroleum ether or other mixed solvents for evenly stirring and filtration, a solid phase II is taken and added in ethanol solution for heating and stirring, activated carbon is added, the heating temperature is 60 to 80 DEG C, the holding time is 0.5 to 2 hours, heat filtration is carried out, then slow stirring and slow cold separation crystallization are carried out, the solution is subject to constant temperature filtration after cold separation, and the filtrate is dried by constant temperature air blow to obtain refined plant sterol. The technique has short route, simple operation, wide processing range of the crude sterol, small energy consumption and low cost, yield and purity both achieve higher standards, thus providing a certain degree of protection for increasing the economic benefit of enterprises.
Owner:NINGBO DAHONGYING BIO ENG

Boron-free high-performance glass fiber taking pulverized fuel ash and desalted river sand as raw materials, as well as preparation method thereof

The invention discloses a boron-free high-performance glass fiber taking pulverized fuel ash and desalted river sand as raw materials, as well as a preparation method thereof, belonging to the technical field of materials. The boron-free high-performance glass fiber is prepared from the following raw materials in percentage by weight: 30-55% of pulverized fuel ash, 0-15% of blast-furnace slag, 40-50% of desalted river sand, 0-12%of magnesium oxide, and 0-6% of calcium oxide. The high-performance glass fiber can be prepared in a common refractory material liner smelting furnace by pretreating the pulverized fuel ash and adding a less amount of blast furnace slag, magnesium oxide and calcium oxide through taking pulverized fuel ash and desalted river sand as raw materials, the strength and elastic modulus are obviously higher than those of the common E glass and ECR, Advantex boron-free glass and the like, the preparation processes are simple, the smelting temperature is at 1400-1420DEG C, a difference between the fiber forming temperature and liquid phase temperature is more than 70DEG C which is far higher than the lowest standard of the glass fiber industrial production being 50DEG C, the production cost is low, and the glass fiber industrial production standard can be met. The component glass has higher chemical corrosion resistance and high-temperature resistance properties compared with the traditional E glass.
Owner:UNIV OF JINAN

Lithium sulfide/nano silicon carbon whole battery and preparation method and application thereof

The invention discloses a lithium sulfide / nano silicon carbon whole battery and a preparation method and application thereof. The preparation method includes following steps: dispersing lithium sulfate into water, dispersing an organic carbon source into an organic solvent, drying and granulating to prepare a composite precursor after sufficient mixing, and calcining at high temperature to obtain a carbon coated lithium sulfide composite anode material; respectively dispersing nano silicon, the organic carbon source and artificial graphite into the organic solvent, drying and granulating after sufficient mixing, and calcining at high temperature to obtain a carbon coated silicon carbon composite cathode material; assembling the carbon coated lithium sulfide composite anode material and the carbon coated silicon carbon composite cathode material to obtain the lithium sulfide / nano silicon carbon whole battery. The preparation method is simple in preparation process, simple and convenient to operate and suitable for large-scale production; the whole battery prepared by the method has the advantages of high first-time charging and discharging efficiency, high specific capacity and good circulating performance, can meet needs of high-capacity electronic equipment and is suitable for electromobiles or portable electronic products.
Owner:SOUTH CHINA NORMAL UNIVERSITY

Ceramic coating protection gradient carbon-ceramic composite material and preparation method thereof

ActiveCN113582713AStable high temperature mechanical propertiesImprove high temperature mechanical propertiesCeramic compositeCarbide coating
The invention discloses a ceramic coating protection gradient carbon-ceramic composite material and a preparation method thereof. The ceramic coating protection gradient carbon-ceramic composite material comprises: a gradient carbon-ceramic composite material which is provided with a concave structure on the surface thereof and is a gradient C/C-ZrC-SiC composite material; and an ultrahigh-temperature ceramic coating which is continuously arranged along the surface of the gradient carbon-ceramic composite material and the inner wall surface of the concave structure. The ultrahigh-temperature ceramic coating is an indissolvable metal carbide coating formed by diffusing and infiltrating indissolvable metal along the surface of the gradient carbon-ceramic composite material and reacting the indissolvable metal with the surface of the gradient carbon-ceramic composite material. Therefore, the formed ceramic coating is a three-dimensional jack structure coating, the interfacial strength of the ceramic coating is far higher than that of a two-dimensional plane coating, the surface area of the coating is greatly increased due to the arrangement of the concave structure, meanwhile, the flow resistance of melt on the surface of the composite material can be improved, then the overall temperature resistance of the composite material can be improved, and the risk of coating stripping is reduced.
Owner:CENT SOUTH UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products