The invention discloses pure-
titanium metal surface micro-arc oxidation treatment
electrolyte and an
antimicrobial bioactive coating preparation method thereof, belongs to a medical
titanium metal surface modification technology, and aims to provide a micro-arc oxidation treatment
electrolyte which can remarkably improve pure-
titanium metal surface bioactivity and
coating bonding strength and a
coating preparation method thereof. The
electrolyte comprises a
compound system including the components of
calcium acetate,
sodium phosphate and a
zinc oxide precursor, wherein the phosphorous
ion concentration is 0.5 to 1.0 M, the
molar ratio of Ca to P is 0.2 to 1.0, and the designed Zn<2+> concentration accounts for 10 to 20 percent of the total concentration. A biological
composite coating is directly generated on the surface of a
titanium metal surface in-situ by adopting the electrolyte and a micro-arc oxidation technology. The
coating has high
bonding strength with a substrate, dense inner layer, coarse and porous outer layer, high bioactivity and high
antibacterial property; moreover, the used raw materials are easy to obtain; the process is simple and easy to operate; and the electrolyte has stability,
reusability, and low production cost and is suitable for industrial production.