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40results about How to "Good high temperature and corrosion resistance" patented technology

Preparation method of positively-charged ceramic micro-nano fiber membrane

The invention discloses a preparation method of a positively-charged ceramic micro-nano fiber membrane. The preparation method comprises the steps of adding spinnable polymer in a solvent, then adding a ceramic precursor in the solvent, and obtaining spinning solution after stirring and aging; pouring the spinning solution in a micro pump, adopting an injection needle head which is scraped smoothly as a spray nozzle, and obtaining composite fiber through electrostatic spinning; firstly roasting the composite fiber in anoxic atmosphere at 200-500 DEG C, then roasting the composite fiber in inertia or reducing atmosphere at 400-400 DEG C for 1-5 hours, and obtaining the positively-charged ceramic micro-nano fiber membrane. According to the preparation method of the positively-charged ceramic micro-nano fiber membrane, disclosed by the invention, the positively-charged ceramic micro-nano fiber membrane which is prepared by combining the electrostatic spinning and a step-by-step roasting technology has high porosity, high specific surface area, high surface electrical performance and good high-temperature-resisting and corrosion-resisting performances, has great advantages of separating, shielding and removing bacteria and virus and has a wide application prospect in environment cleaning, pharmaceuticals production, bioengineering, foundation medicine and the like.
Owner:XIAN UNIV OF TECH

TiB2-Ni-based metal-ceramic composite feed for thermal spraying and preparation method of TiB2-Ni-based metal-ceramic composite feed

The invention discloses TiB2-Ni-based metal-ceramic composite feed for thermal spraying and a preparation method of the TiB2-Ni-based metal-ceramic composite feed. The preparation method comprises thefollowing steps: (1) in a protective atmosphere, adding TiB2 powder and Ni-based alloy powder into a stirring grinder, adding a process control agent, a binding agent and a grinding medium, and thencarrying out grinding, so as to obtain slurry of composite powder A; (2) carrying out spray granulation on the slurry of the composite powder A in a spray drying system, so as to obtain composite powder B; (3) carrying out heat preservation on the composite powder B in drying equipment, so as to obtain composite powder C; and (4) passing the composite powder C through a spheroidizing system, so asto obtain high-sphericity composite powder. The powder prepared through the preparation method disclosed by the invention is high in flowability and excellent in performance; the demand of thermal spraying equipment for the powder flowability can be met; the problem that nanometer metal-ceramic composite powder is hard to spray can be solved; and the improvement of the coating surface performancecan be facilitated.
Owner:SOUTH CHINA UNIV OF TECH

Preparation method of high-temperature-resistant anti-corrosion ceramic coating

The invention provides a preparation method of a high-temperature-resistant anti-corrosion ceramic coating. A nickel-based alloy transition layer is prepared on the surface of a substrate through a cold spraying technology, the ceramic coating is prepared on the surface of the nickel-based alloy transition layer, and the surface of the ceramic coating is remelted. According to the preparation method of the high-temperature-resistant anti-corrosion ceramic coating provided by the invention, the nickel-based alloy transition layer is prepared on the surface of a steel substrate through cold spraying, and the problems that as a traditional thermal spraying technology is adopted for preparing the transition layer, tensile stress is left in the coating, cracks and stripping are caused due to the fact that the tensile stress is easily and continuously increased in the subsequent thermal spraying of the ceramic coating are solved, and the internal stress of the cold spraying coating is pressure stress, a part of tensile stress generated by heating can be offset, then the binding force between the transition layer and the ceramic coating is improved, the outer surface layer of the prepared high-temperature-resistant anti-corrosion ceramic coating is compact, the inner layer of the prepared high-temperature-resistant anti-corrosion ceramic coating is porous, and the binding strength between the ceramic coating and the transition layer and the binding strength between the transition layer and the substrate are high, the high-temperature-resistant and corrosion-resistant performance is excellent, and the service life is long.
Owner:JIHUA LAB

Preparation method of low naphthalene high-boiling-point aromatic solvent for rubber resin plasticizer

The invention discloses a preparation method of a low naphthalene high-boiling-point aromatic solvent for a rubber resin plasticizer. The preparation method of the low naphthalene high-boiling-point aromatic solvent for the rubber resin plasticizer comprises the following steps: firstly, preparing a supported hydrogenation catalyst and a naphthalene remover; secondly, using cracked C10 fraction asa raw material to carry out hydrogenation and naphthalene removing treatment in sequence; and thirdly, adding the cracked C10 fraction to a rectifying tower; opening a vacuum system of the rectifyingtower; adjusting the vacuum degree of the vacuum system at -0.09 MPa; starting a reboiler heat conduction oil heating system of the rectifying tower; controlling the tower top temperature at 165.5 DEG C and the tower bottom temperature at 269.2 DEG C to carry out rectification under vacuum; condensing a vapor phase of the rectifying process by using a tower top condenser of the rectifying tower;enabling a condensate to enter a reflux drum; condensing and trapping non-condensed vapor phase by using a tower top condensing trap of the rectifying tower; enabling the trapped condensate to enter the reflux drum; controlling reflux amount; and collecting a fraction with temperature of 260-280 DEG C to prepare a target product. The preparation method of the low naphthalene high-boiling-point aromatic solvent for the rubber resin plasticizer, disclosed by the invention, has the advantages of simple operation, low cost, low naphthalene content of the prepared aromatic solvent, no toxicity andenvironmental protection.
Owner:PENG CHEN NEW MATERIALS TECH CO LTD

Graphene-based high-temperature-resistant anticorrosive paint and preparation method thereof

The invention relates to a graphene-based high-temperature-resistant anticorrosive paint and a preparation method thereof, and belongs to the technical field of anticorrosive materials, wherein the graphene-based high-temperature-resistant anticorrosive paint is obtained by mixing a component A and a component B according to a mass ratio of 9:1; the component A comprises the components in percentage by mass: 50 to 70% of a binding agent and 30 to 50% of a pigment filler; the binding agent comprises the components in percentage by mass: 60% of polymethylphenyl siloxane modified epoxy resin and40% of organic silicon; the pigment filler comprises the following components: graphene, chromium dioxide, titanium dioxide, zinc oxide, alumina powder, barium sulfate, magnesium carbonate, calcium carbonate, white carbon black micro-powder, quartz powder, graphite powder, green silicon carbide micro-powder, silicon carbide micro-powder, corundum micro-powder, silica powder, organic bentonite, mica powder and the balance being copper chromite black, iron oxide black and carbon fibers; and the component B is a curing agent. The anticorrosive paint has good comprehensive performance, strong corrosion resistance and high temperature resistance, and good comprehensive performance.
Owner:广东阿尔法工程材料有限公司

Preparation method of nickle-based high temperature and corrosion resistant welding wire

The invention belongs to the field of welding material and particularly relates to a preparation method of a nickle-based high temperature and corrosion resistant welding wire. The preparation methodcomprises the following steps: 1, preparing the raw materials according to the proportion, wherein chromium and partial nickle are prepared in the form of nickel-chromium intermediate alloy, adding other raw materials except titanium, chromium and partial nickle into a vacuum induction furnace, carrying out bottom argon blowing, and after the raw materials are completely melted, starting to carryout top blowing oxygen; 2, adding the nickel-chromium intermediate alloy 5-10 minutes after top blowing oxygen to melt and disperse the nickel-chromium intermediate alloy, stops blowing oxygen when the carbon content is reduced to less than 0.03%, and carrying out top blowing argon and bottom blowing argon simultaneously; 3, keeping bottom blowing argon, adding ferrosilicon and aluminium block insteel ladle for deoxidation, and then adding lime and fluorite for slagging and desulfuration; 4, casting melted liquid into alloy ingot, and annealing the alloy ingot; 5, forging the annealed alloy ingot at 1100-1200 DEG C into alloy billets, and rolling the alloy billets into wire rods; 6, carrying out acid pickling and coping to remove oxide skins and corrosion substance on the surfaces of thewire rods, annealing the wire rods, and drawing the wire rods into a welding wire; and annealing the welding wire.
Owner:DANYANG HUALONG SUPERIOR STEEL

Preparation method of low naphthalene high boiling point aromatic hydrocarbon solvent for rubber resin plasticizer

The invention discloses a method for preparing a low-naphthalene and high-boiling-point aromatic hydrocarbon solvent used for rubber resin plasticizers, comprising the following steps: firstly preparing a loaded hydrogenation catalyst and a naphthalene-removing agent, and then using cracking C 10 The distillate is used as raw material, which is subjected to hydrogenation and denaphthalene treatment in sequence, and finally added to the rectification tower, and the vacuum system of the rectification tower is turned on, and the vacuum degree is adjusted to ‑0.09MPa; the reboiler of the rectification tower is started to be heated The system controls the tower top temperature at 165.5°C and the tower bottom temperature at 269.2°C, and performs vacuum rectification. The gas phase of the rectification process is condensed by the top condenser of the rectification tower, and the condensate enters the reflux tank, and the uncondensed gas phase undergoes rectification. The condensate trap at the top of the tower is condensed and collected, and the captured condensate enters the reflux tank, the reflux flow is controlled, and the fraction at 260‑280 ° C is collected to obtain the target product. The method is simple in operation, low in cost, low in naphthalene content in the prepared aromatic hydrocarbon solvent, non-toxic and environment-friendly.
Owner:PENG CHEN NEW MATERIALS TECH CO LTD

Preparation method of positively charged ceramic micro-nano fiber membrane

The invention discloses a preparation method of a positively-charged ceramic micro-nano fiber membrane. The preparation method comprises the steps of adding spinnable polymer in a solvent, then adding a ceramic precursor in the solvent, and obtaining spinning solution after stirring and aging; pouring the spinning solution in a micro pump, adopting an injection needle head which is scraped smoothly as a spray nozzle, and obtaining composite fiber through electrostatic spinning; firstly roasting the composite fiber in anoxic atmosphere at 200-500 DEG C, then roasting the composite fiber in inertia or reducing atmosphere at 400-400 DEG C for 1-5 hours, and obtaining the positively-charged ceramic micro-nano fiber membrane. According to the preparation method of the positively-charged ceramic micro-nano fiber membrane, disclosed by the invention, the positively-charged ceramic micro-nano fiber membrane which is prepared by combining the electrostatic spinning and a step-by-step roasting technology has high porosity, high specific surface area, high surface electrical performance and good high-temperature-resisting and corrosion-resisting performances, has great advantages of separating, shielding and removing bacteria and virus and has a wide application prospect in environment cleaning, pharmaceuticals production, bioengineering, foundation medicine and the like.
Owner:XIAN UNIV OF TECH
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