A zinc leaching slag treatment method comprises the following steps: 1) The dried zinc leaching slag is evenly mixed with coke powder, and then the mixture is added to a volatilization kiln through a feeding scraper-trough conveyer at the tail of the kiln; 2) under the high-temperature condition of the volatilization kiln, the mixture generates kiln slag and smoke, valuable metals in the zinc leaching slag are deoxidize, as a result, lead and zinc steam is generated and gathered in the smoke, and gold, silver and copper enters to the kiln slag; 3) the kiln slag is delivered to a smelting furnace, furnace burden is added from the top of the smelting furnace, oxygen-enriched air is blown through an oxygen lance, the furnace hearth is stirred, the smelting temperature of the smelting furnace and the ratio of oxygen quantity to kiln slag dry measure are controlled, and slagging smelting is completed; 4) after the slagging smelting carried out in step 3), the valuable metals gold, silver and copper in the kiln slag are gathered in matte, the generated lead steam is gathered in smoke, and the kiln slag is cooled gradually. According to the zinc leaching slag treatment method, the technological process is short, the energy consumption is low, the cost is low, and the valuable metal recovery rate is high.