2481 results about "Manganese salt" patented technology

The present invention relates to energy source material technology, and is preparation process of high density spherical lithium nickel-cobalt-manganate as positive electrode material for lithium ion cell. The preparation process includes the reaction of nickel salt, cobalt salt, manganese salt, ammonium hydroxide and ammonian in water solution to synthesize spherical or spheroid precursor Ni1 / 3Co1 / 3Mn1 / 3 (OTHER)2, washing, drying and mixing with lithium carbonate; and high temperature treatment in the air at 750-950 deg.c for 8-48 hr to obtain spherical lithium nickel-cobalt-manganate. The spherical lithium nickel-cobalt-manganate has great bulk density reaching 2.25-2.50 g / cu cm after vibration densifying, average grain size of 3-7 microns, and reversible specific capacity up to 172-185 mA.hr / g.

The invention discloses a carbon-coated ternary positive electrode material and a preparation method thereof. The preparation method comprises the following steps: S1, preparing a ternary positive electrode material precursor by taking nickel salt, cobalt salt and manganese salt as raw materials; S2, preparing a conductive carbon dispersion system, wherein conductive carbon is dispersed in water containing an organic carbon source; S3, adding the ternary positive electrode material precursor and a lithium compound into the conductive carbon dispersion system, and mixing uniformly to obtain a mixture; S4, drying the mixture under a vacuum condition; S5, carrying out high temperature treatment on the dried mixture under a closed condition or in an inert gas protection atmosphere so as to obtain the carbon-coated ternary positive electrode material. The carbon-coated ternary positive electrode material is uniform in coating, simple to operate, low in cost and high in efficiency; the conductive carbon and the ternary positive electrode material are simultaneously coated with network-shaped amorphous carbon which serves as a conductive medium or a channel of the conductive carbon and the ternary positive electrode material, thereby greatly improving the rate performance of the ternary positive electrode material.

The invention belongs to the field of preparation techniques of nanophase materials and green energy resources, and relates to a preparation method of a nano positive material LiNi1 / 3Mn1 / 3Co1 / 3O2 applied to a lithium ion battery. By using the method, the defects that the calcining temperature needed by a current synthetic material is high, the calcining time is long, the particle sizes of a product are not uniform, and the like, are mainly solved. The preparation method comprises the following steps: adding a certain amount of template agent in a mixed aqueous solution of a nickel salt, a manganese salt and a cobalt salt, and then, dripping a precipitant and a complexing agent into the obtained mixture to form a precipitate; subjecting the precipitate and the mixed aqueous solution to a high-pressure thermal reaction in a hydrothermal kettle, cleaning and baking the obtained product to be dry, so as to obtain a nickel manganese cobalt oxide; and finally, uniformly mixing the nickel manganese cobalt oxide with the lithium salt to prepare a final product by calcining and cooling. By using the preparation method, the product with favorable electrochemical performance can be obtained within a shorter calcining time; the energy consumption is decreased; and the preparation method has obvious economic benefit in the large-scale application of industrial synthesis.