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126results about How to "Control oxidation" patented technology

Silane and borane treatments for titanium carbide films

Methods of treating metal-containing thin films, such as films comprising titanium carbide, with a silane / borane agent are provided. In some embodiments a film comprising titanium carbide is deposited on a substrate by an atomic layer deposition (ALD) process. The process may include a plurality of deposition cycles involving alternating and sequential pulses of a first source chemical that comprises titanium and at least one halide ligand, a second source chemical comprising metal and carbon, wherein the metal and the carbon from the second source chemical are incorporated into the thin film, and a third source chemical, wherein the third source chemical is a silane or borane that at least partially reduces oxidized portions of the titanium carbide layer formed by the first and second source chemicals. In some embodiments treatment forms a capping layer on the metal carbide film.
Owner:ASM IP HLDG BV

Plasma enhanced liner

It is, an object of the present invention to provide a process of forming a refractory metal liner that includes depositing a layer of refractory metal on a first conductive layer, where at least half of the depositing is carried out in the presence of an amount of passivating agent that is sufficient to impede subsequent reaction of at least a top half of the layer of refractory metal with the first conductive layer and is less than an amount of passivating agent necessary to form a stoichiometric refractory metal with the passivating agent. The process also includes annealing the refractory metal and the first conductive layer in a first element ambient, thereby forming a stoichiometric refractory metal with the first element in at least a portion of the top half of the layer of refractory metal.
Owner:GLOBALFOUNDRIES INC

Low-pressure casting method, cooling control process and exhaust system of large impeller

The invention discloses a low-pressure casting method, a cooling control process and an exhaust system of a large impeller. The low-pressure casting method comprises the steps that a manufactured forming element and a manufactured mold core are dried, and a low-pressure casting mold of the impeller is preheated; a casting material is put in a casting device, heating and smelting are carried out to form a casting solution, and slag removal is carried out on the casting solution when the casting solution reaches the set temperature; the casting mold of the impeller is assembled, and the casting mold of the impeller and the casting device are connected to form an impeller casting system; the low-pressure casting device is subjected to low-pressure mold filling along a set pressure curve; after mold filling is finished, the low-pressure casting mold of the impeller is cooled; and after the temperature of the low-pressure casting mold of the impeller is reduced to the set temperature, the impeller is taken out to be cleaned. In the casting process, the pressure and the speed are adjusted, and therefore short run can be reduced; aluminum liquid oxidization can be controlled by adjusting the aluminum liquid temperature; and shrinkage porosity can be reduced by adjusting the cooling process.
Owner:HIMILE MECHANICAL SCI & TECH (SHANDONG) CO LTD

Preparation method for Mg2Si thermoelectricity material

The present invention relates to a preparation method for an Mg2Si thermoelectricity material. The method comprises the following steps: (1) uniformly mixing Mg powder and Si powder under an Ar protection atmosphere to obtain a mixture; (2) placing the mixture in a glove box filled with Ar, and placing the glove box in a stainless steel vacuum ball milling tank to carry out intermittent ball milling to obtain uniformly-mixed powder; (3) carrying out tableting on the mixed powder to obtain a Mg-Si mixed powder tablet; (4) loading the Mg-Si mixed powder tablet into a graphite mold, and placing graphite mold in a tube furnace under an Ar atmosphere to carry out primary sintering and thermal insulation to obtain Mg2Si thermoelectricity material alloy powder; (5) carrying out tableting on the Mg2Si thermoelectricity material powder to obtain a Mg2Si alloy tablet; and (6) loading the Mg2Si alloy tablet into the graphite mold and placing the graphite mold in the tube furnace under an Ar atmosphere to carry out secondary sintering and thermal insulation to obtain the Mg2Si block thermoelectricity material. The preparation method has characteristics of simple process, easy operation and low cost. The obtained Mg2Si thermoelectricity material has characteristics of high product purity, small particle size and uniform distribution.
Owner:QINGHAI INST OF SALT LAKES OF CHINESE ACAD OF SCI

Durable conformal wear-resistant carbon-doped metal oxide-comprising coating

The present invention is related to carbon-doped metal oxide films. The carbon-doped metal oxide films provide a low coefficient of friction, for example ranging from about 0.05 to about 0.4. In addition, the carbon-doped metal oxide films applied over a silicon substrate, for example, provide anti-stiction properties, where the measured work of adhesion for a MEMS device cantilever beam coated with the carbon-doped metal oxide film is less than 10 μJ / m2. In addition, the carbon-doped metal oxide films provide unexpectedly good water vapor transmission properties. The carbon content in the carbon-doped metal oxide films ranges from about 5 atomic % to about 20 atomic %.
Owner:SPTS TECH LTD

Flue gas desulfurization and denitration device and method

The invention discloses a flue gas desulfurization and denitration device and method. The device comprises: a desulfurization container, the bottom of which is equipped with a desulfurization liquid material storage area, above which a flue gas inlet is disposed, with a flue gas washing and desulfurization structure being arranged above the flue gas inlet; a denitration container, the bottom of which is equipped with a denitration liquid material storage area, above which a flue gas washing and denitration structure is arranged, with a separation structure for removing solid particles and liquid drops being disposed above the flue gas washing and denitration structure, and a gas outlet being disposed at the top of the denitration container; an oxidization pipeline for communicating the desulfurization container and the denitration container; an atomization spray structure that is disposed in the oxidization pipeline and capable of providing structure connection together with chlorine dioxide, with the chlorine dioxide mist sprayed by the atomization spray structure being mixed with the flue gas in the oxidization pipeline. The flue gas desulfurization and denitration device and method provided by the invention can realize high efficiency and high utilization oxidation of ClO2 to NO, are safe and convenient to operate, and are convenient for industrial application.
Owner:CHINA UNIV OF PETROLEUM (BEIJING)

Processing method of spherical health care red tea and product thereof

The invention relates to a processing method of spherical health care red tea and a product thereof, and belongs to the technical field of tea processing and making. The specific processing working procedures comprise picking, spreading, rocking, drying, rolling, primary spreading, primary stir-frying, spreading drying and dampening, secondary spreading and drying, repeated stir-frying, spreading drying and dampening, drying and packaging, and further comprise primary package color fixing working procedure and repeated package color fixing working procedure; the primary package color fixing working procedure is performed between the rolling working procedure and the primary spreading drying working procedure; and the repeated package color fixing working procedure is preformed between the spreading drying and dampening working procedure and the secondary spreading and drying working procedure; folium mori extract containing 1-Deoxynojirimycin is added in the repeated stir-frying working procedure, the content of 1-Deoxynojirimycin in the folium mori extract is 10% to 50%, and the adding amount of 1-Deoxynojirimycin is 0.1-1% of leaf dropping amount. For a product made by adopting the processing method of spherical health care red tea, the content of tea polyphenol in the product is 70-110 mg / g. The spherical health red tea has the beneficial effects of being beautiful in appearance, pure in taste, and mellow and full in fragrance; the product effects of reducing blood sugar and preventing and controlling diabetes are enhanced; and the benefits are greatly improved.
Owner:YUYAO CITY SICHUANGYAN TEA

Method for preparing sintered neodymium iron boron magnets in 3D cold printing mode

The invention provides a method for preparing sintered neodymium iron boron magnets in a 3D cold printing mode and belongs to the field of powder metallurgy. By wrapping the surfaces of neodymium ironboron magnetic powder with layers of oxygen-free organic film, the magnetic powder is prevented from being oxidized in the 3D cold printing process, meanwhile, printing slurry is prepared by adoptinga low-molecular-weight and low-oxygen gelatin system, printing orientation forming of the magnets is achieved through magnetizing, and after isostatic cool pressing and sintering are performed, sintered neodymium iron boron parts in complex shapes are finally obtained. Oxygen-free organic matter is adopted for wrapping the surfaces of the neodymium iron boron powder which is oxidized easily, theoxidation problem of the magnetic powder in the forming process is controlled, the 3D cold printing neodymium iron boron slurry is prepared by adopting the low-molecular-weight and low-oxygen gelationsystem, and the oxygenation situation of the magnets in the forming process are further controlled. The sintered neodymium iron boron magnets prepared through the method provided by the invention have the good magnetic performance, near-net forming of all complex shapes can be achieved, cutting machining of magnet complex parts is omitted, the production cost is greatly lowered, and resources aresaved.
Owner:UNIV OF SCI & TECH BEIJING

Additive for lubricant compositions comprising a sulfur-containing and a sulfur-free organomolybdenum compound, and a triazole or a derivatized triazole

A lubricating composition for use in heavy duty diesel engines which is formulated to allow the use of organomolybdenum compounds but which overcomes the issue of Cu and / or Pb corrosion. The lubricant is characterized by having a synergistic additive composition comprising (A) a sulfur-free organo-molybdenum compound, (B) a sulfur-containing organo-molybdenum compound and (C) a triazole derivative prepared by reacting 1,2,4-triazole, a formaldehyde source and an amine; (A), (B) and (C) being present in an amount sufficient to allow the lubricating composition to pass the High Temperature Corrosion Bench Test ASTM D 6594 with respect to Cu and / or Pb corrosion.
Owner:VANDERBILT CHEM LLC

Encapsulation of high temperature thermoelectric modules

A method of encapsulating a thermoelectric device and its associated thermoelectric elements in an inert atmosphere and a thermoelectric device fabricated by such method are described. These thermoelectric devices may be intended for use under conditions which would otherwise promote oxidation of the thermoelectric elements. The capsule is formed by securing a suitably-sized thin-walled strip of oxidation-resistant metal to the ceramic substrates which support the thermoelectric elements. The thin-walled metal strip is positioned to enclose the edges of the thermoelectric device and is secured to the substrates using gap-filling materials. The strip, substrates and gap-filling materials cooperatively encapsulate the thermoelectric elements and exclude oxygen and water vapor from atmospheric air so that the elements may be maintained in an inert, non-oxidizing environment.
Owner:GM GLOBAL TECH OPERATIONS LLC

Rubber-metal bonding enhancer for steel wire radial tyre and preparation method thereof

The invention belongs to the field of rubber chemicals and discloses a rubber-metal bonding enhancer for a steel wire radial tyre. The enhancer is prepared from four kinds of metal salts of cobalt, nickel, copper and zinc; and the proportion of the metal salts by metal molar mass: cobalt: nickel: copper: zinc is (50% to 70%): (20% to 40%): (6% to 10%): (2% to 4%). The preparation method of the bonding enhancer comprises the steps of: using the four kinds of metal salts as starting materials to sequentially prepare alkali carbonate metal composite salt by a temperature gradient method and a concentration step method, prepare an intermediate by a continuous dehydration method and prepare low cobalt boroacylate metal composite salt by a boroacylate replacement reaction to obtain the bonding enhancer. In the invention, the proportion of the cobalt is regulated to 50% to 70% from 100% in a traditional technology; and the consumption of precious metal cobalt is reduced; the cost is reduced by 10% to 20%. The physical and chemical indexes and utilization property of the product of the invention are equivalent to those of a boroacylate cobalt product; and the drawing force and retention rate of an aged product are better than those of the boroacylate cobalt product.
Owner:杭州新速工业助剂有限公司
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