The invention discloses a method for removing iron and regenerating
tungsten powder from high-iron reduced
tungsten powder, and belongs to the field of nonferrous
metallurgy. The method is characterized in that the high-iron
tungsten powder is used as a
raw material, and is mixed with an acidic high-valence iron
dissolution liquid and an additive, the low-temperature
dissolution treatment is carried out at the temperature of 3-15 DEG C under an ultrasonic condition for
iron removal, after
dissolution, the insoluble tungsten powder and a
ferrous dissolution liquid are obtained through separation, the gradient washing treatment is carried out on the insoluble tungsten powder, so that the residual
ferrous dissolution liquid is fully washed out, moreover, the phenomenon that the iron is hydrolyzed and is left in the tungsten powder is avoided, and
drying and cooling are carried out on the washed wet tungsten powder to obtain a pure tungsten powder product. According to the method, the ironis simply and efficiently removed from high-iron-containing boat charge generated in the tungsten powder reduction process, moreover, purification and regeneration of the tungsten powder are realized, the
system water is completely recycled, no waste water and waste residue are discharged, and the method is suitable for the tungsten powder which is at the edge of a boat and generated in various
tungsten oxide reduction processes and the tungsten powder product polluted by an iron ware, and has the advantages of being high in
raw material adaptability, simple in technological process, thoroughin
iron removal, clean and environment-friendly.