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38results about How to "Suitable for batch preparation" patented technology

Method for preparing polymer micro lens array

The invention provides a method for preparing a polymer micro lens array, and relates to the field of micro mechanical machining. The problems that in an existing hot press molding method, the cycle is long, cost is high, efficiency is low, and the dimensional precision and the shape of micro lenses can not be guaranteed easily are solved. The method comprises the steps that a graphical photoresist mask is formed on the surface of a silicon substrate; a microporous array is etched through a dry method; the microporous array is evenly covered with a dimethyl silicone polymer thin film, the microporous array is in sealing connection with a cavity, the pressure of a cavity is adjusted to change the ball coronary deformation of the dimethyl silicone polymer thin film, and the pressure is kept constant; photosensitive gel is poured on the dimethyl silicone polymer thin film, and a photosensitive gel convex mold is obtained through ultraviolet curing demolding; a mixture of dimethyl silicone polymer prepolymer and a curing agent is poured in the photosensitive gel convex mold to be heated and cured to obtain a dimethyl silicone polymer concave mold; the concave mold is used for conducting hot pressing on carbonic ester base materials, and a carbonic ester base micro lens array is obtained after demolding. The method for preparing the polymer micro lens array is easy to operate, high in efficiency, low in cost, small in error, good in repeatability, lossless in demolding and suitable for mass production.
Owner:CHANGCHUN INST OF OPTICS FINE MECHANICS & PHYSICS CHINESE ACAD OF SCI

Method for synthesizing anatase type crystallizing titanium dioxide nano nuclear-shell or shell structure material by water phase one-step method

The present invention relates to preparation process of core-shell material and hollow material, and is especially water phase one-step synthesis process for preparing nanometer crystallized anatase type titania material in core-shell and hollow structure. Water soluble titanium peroxide precursor is treated through a sol-gel process so as to coat a nanometer titania layer onto the surface of polystyrene, and the nanometer titania layer in the shell is crystallized directly at relatively low temperature to form nanometer anatase type titania without needing sintering. Furthermore, the precursor may be controlled properly, so that the polystyrene core serving as the template may be dissolved spontaneously after the shell is formed and crystallized and nanometer hollow titania may be obtained directly in water phase. The present invention is simple, easy to operate, low in cost and suitable for batch production, and may find wide application in different aspects.
Owner:TECHNICAL INST OF PHYSICS & CHEMISTRY - CHINESE ACAD OF SCI

Preparation method of carbon-ceramic composite material based on unidirectional belt process

The invention relates to a preparation method of a carbon-ceramic composite material based on a unidirectional belt process. The preparation method comprises the steps of compositing a carbon fiber asa reinforcement with slurry prepared from high-carbon residue resin, so as to prepare a carbon fiber unidirectional belt, spreading the unidirectional belt as a layer, carrying out mold pressing andhot-pressure tank formation so as to prepare a preform, and carrying out carbonization and infiltration, so as to prepare a carbon fiber enhanced ceramic-base composite material. The preparation method has the beneficial effects that an interface layer does not need to be prepared on the surface of the carbon fiber, the uniform distribution of the fiber in a matrix can be realized by virtue of a unidirectional belt process, the continuous production can be realized, and the performance degradation caused due to twists formed during the weaving of traditional fibers is avoided.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS

Preparation method of bi-system high-temperature superconducting material

The invention discloses a preparation method of a bi-system high-temperature superconducting material, comprising the following steps of: preparing Bi-2212 powder into a bi-system tape material by adopting a powder tubing method and a clustered drawing technology; dissolving a bonder by using methanol or ethanol as a solvent and then adding the Bi-2212 powder to mix evenly so as to obtain suspension liquid; causing the bi-system tape material to pass through a liquid trough which is loaded with the suspension liquid and then guiding the bi-system tape material to pass through a drying furnace so as to obtain a bi-system high temperature superconducting tape material which is externally coated with a superconducting film; and carrying out semi-melting treatment on the bi-system high temperature superconducting tape material which is externally coated with the superconducting film and then obtaining the bi-system high-temperature superconducting tape material after cooling with a furnace. The preparation process of the invention is simple, reasonable in design, low in manufacturing cost and large in popularization. In the invention, a layer of Bi-2212 superconducting film is added on the surface of the bi-system tape material prepared by a PIT method so that the silver hypergeometric of the tape material is decreased, the effective superconducting area is increased and the engineering current density of the bi-system tape material is improved.
Owner:NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH

Preparation method for micro-piezoelectric actuator array structure

The invention discloses a preparation method for a micro-piezoelectric actuator array structure. The preparation method comprises the steps of carrying out thermal oxidation treatment on a silicon wafer, wherein the two sides of the silicon wafer are polished, and forming a silicon dioxide thin film on the surface; carrying out patterning treatment on the silicon dioxide thin film to form a mask pattern; carrying out inductive coupling plasma etching on the upper surface of the silicon wafer according the mask pattern to form a silicon supporting table; evaporating a gold layer on the upper surface of the silicon supporting table and the lower surface of a piezoelectric ceramic sheet separately, and bonding the silicon supporting table and the piezoelectric ceramic sheet by adopting an eutectic bonding method; carrying out physical thinning on the piezoelectric ceramic sheet; sputtering a gold / chromium thin film on the upper surface of the piezoelectric ceramic sheet to be used as the upper layer electrode of the piezoelectric ceramic sheet, and carrying out patterning treatment on the piezoelectric ceramic sheet by an excimer laser; and etching silicon from the lower surface of the silicon wafer by a wet etching method to form a silicon cavity, wherein the position of the silicon cavity is corresponding to that of the silicon supporting table. The micro-piezoelectric actuator array structure is simple and easy to implement the preparation method and high in compactness and piezoelectric property.
Owner:SHANGHAI INST OF TECH

Continuous preparation device and preparation method for bismuth-series high temperature superconductive thick film

The invention discloses a continuous preparation device and a preparation method for a bismuth-series high temperature superconductive thick film. The continuous preparation device comprises dipping equipment used for evenly dipping coating slurry on the outer surface of a wire and tape to be processed, drying equipment for drying the wire and tape (to be processed) dipped with the coating slurry, rolling equipment for rolling the wire and tape (to be processed) after drying treatment, and wire drawing equipment used for drawing the wire and tape (to be processed) to penetrate through the dipping equipment, drying equipment and rolling equipment in order; and the wire drawing equipment comprises a wire unwinding machine and a wire winding machine. The preparation method comprises the following steps of: 1, adjusting the wiring rate V; 2, dipping coating slurry; 3, drying; 4, rolling; and 5, winding a wire and performing heat treatment. The continuous preparation device and preparationmethod in the invention have the advantages of reasonable design, convenience in operation and realization, good preparation effect and high processing efficiency, and can be used for preparing a Bi-2212 superconductive thick film with a certain length and high current carrying performance.
Owner:NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH

Preparation method of fly-eye lens with free-form surface substrate

The invention provides a preparation method of a fly-eye lens with a free-form surface substrate. The free-form surface fly-eye lens with different gradients of sub-eyes is formed by controlling the film thicknesses of different areas of a film and regularly changing the morphology of the surface. Meanwhile, the imaging effect of each stage of sub-eyes under different object distances is perfected, and the problem that the focal lengths of off-axis light rays are not collinear due to spherical aberration is solved by introducing a free-form surface.
Owner:CHANGCHUN INST OF OPTICS FINE MECHANICS & PHYSICS CHINESE ACAD OF SCI

Cross beam assembly of passenger car

The invention relates to a cross beam assembly of a passenger car. The cross beam assembly comprises a front section beam assembly, a left connecting longitudinal beam assembly, a right connecting longitudinal beam assembly, a left back air bag support assembly and a right back air bag support assembly, wherein the left connecting longitudinal beam assembly and the right connecting longitudinal beam assembly are symmetrically arranged on back sides of left and right ends of a middle section of the front section beam assembly, and the left back air bag support assembly and the right back air bag support assembly are symmetrically arranged on back sides of left and right ends of the front section beam assembly. The cross beam assembly of the passenger car can overcome defects in the prior art, has the characteristics of high universality, high structural strength and the like and is suitable for batch and large-scale production and preparation, the production cycle can be effectively shortened, and the labor intensity can be reduced.
Owner:ANHUI ANKAI AUTOMOBILE

Preparation method of titanium dioxide-metal water-based nanometer composite sol

ActiveCN104226210AEffective Composite StructureAvoid heterogeneous nucleationNanotechnologyColloidal chemistry detailsWater basedSuperoxide
The invention discloses a preparation method of titanium dioxide-metal water-based nanometer composite sol. The preparation method comprises the following steps: 1, dissolving metal salt in water to obtain a metal salt water solution, and reflowing the metal salt water solution by heating while adding a reducing agent water solution until a reflowing water solution system discolors for later use, wherein a mol ratio of the added reducing agent to metal ions is 1-50; 2, dissolving titanate in an aqueous solution of hydrogen peroxide to obtain an aqueous solution of titanium superoxide, regulating the pH value of the aqueous solution of titanium superoxide by virtue of an inorganic aqueous alkali solution; and 3, adding the aqueous solution of titanium superoxide prepared in the step 2 into the discolored metal salt water solution prepared in the step 1 to obtain a composite solution, and reflowing the composite solution by heating to obtain the final product. According to the preparation method disclosed by the invention, a metal-oxide composite structure can be effectively formed, and the process operability is high; the preparation method is suitable for batch preparation, and has a possibility of industrialized production and wide practicability.
Owner:TECHNICAL INST OF PHYSICS & CHEMISTRY - CHINESE ACAD OF SCI

Biomass superstructure carbon as well as preparation method and application thereof

PendingCN114031076ARealize controllable constructionFast transferCarbon compoundsHybrid capacitor electrodesBiomassChemistry
The invention discloses biomass superstructure carbon and a preparation method and application thereof, and the method comprises the following steps: (1) preparation of a biomass precursor: adding ramie and a 1-6mol / L KOH solution into a reaction lining according to a material-liquid ratio of 1g: (30-40mL), then heating to 170-190 DEG C, reacting for 5-7h at 170-190 DEG C, cooling after the reaction is finished, then carrying out suction filtration to obtain KOH molecule pre-embedded ramie, and then drying to obtain the biomass precursor; and (2) preparation of the biomass superstructure carbon: uniformly mixing the biomass precursor and magnesium metal according to a mass ratio of (1-6): 1, heating to 650-750 DEG C in a protective gas environment, introducing CO2 with a gas flow of 15-25 sccm, and reacting at 650-750 DEG C for 30-90 minutes to obtain the biomass superstructure carbon. The preparation process is simple, the cost is low, batch production can be realized, and the prepared biomass superstructure carbon has a multi-level pore structure and a high specific surface area.
Owner:四川金时新能科技有限公司

Preparing method of hollow-structure titanium oxide/silicon oxide composite photocatalytic material

The invention discloses a preparing method of a hollow-structure nanometer titanium dioxide self-cleaning composite photocatalytic material high in specific surface area. The method includes the stepsof firstly, synthesizing a titanium and peroxide ammonia compound emulsion; secondly, drying titanium and peroxide ammonia compound microspheres; thirdly, conducting silicon oxide wrapping; fourthly,conducting sintering. Through the catalytic hydrolysis effect of silane, a silicon oxide shell layer is synthesized, and the hollow-structure SiO2 / TiO2 composite is obtained through the sudden drop of the size of the titanium and peroxide ammonia compound in the crystallizing process. The method is simple in process, high in operability, low in cost and suitable for batched preparation and has industrial production probability and wide application prospects.
Owner:NATURE ENVIRONMENTAL PROTECTION TECH

Preparation method of titanium oxide/calcium oxide/silicon oxide composite photocatalytic material in hollow structure

The invention discloses a preparation method of a titanium oxide / calcium oxide / silicon oxide composite photocatalytic material in a hollow structure. The preparation method comprises the following steps: (1) preparing a titanium and calcium peroxide compound precursor; (2) preparing titanium and calcium compound sol; (3) cladding silicon oxide; and (4) sintering. The preparation method adopts direct synthesis through a one-pot method at a liquid phase, and the requirement on equipment is low; the method has the advantages of simple procedure, high operability, relatively low cost, suitabilityfor batch preparation, industrial production possibility and extensive application prospect.
Owner:NATURE ENVIRONMENTAL PROTECTION TECH

Conductive titanium oxide ceramic sputtering target and preparation method thereof

The invention relates to a conductive titanium oxide ceramic sputtering target and a preparation method thereof. Specifically, the invention discloses a preparation method for a titanium oxide target.The preparation method comprises the following steps: 1) providing modified titanium oxide nanometer powder; 2) subjecting the modified titanium oxide nanometer powder to compression molding so as toobtain a green ceramic body; and 3) sintering the green ceramic body in a vacuum atmosphere or an inert atmosphere to obtain the titanium oxide target. The invention also discloses the titanium oxidetarget prepared by using the method and a titanium oxide film prepared through sputtering of the target. The method is simple in process, low in cost, and easy to prepare the titanium oxide target with uniform and stable performance, thereby facilitating preparation of the titanium oxide film with excellent performance.
Owner:宁波森利电子材料有限公司

Compressed sealing material for solid oxide fuel cell stack and preparation method of compressed sealing material

InactiveCN108054408AMeet high temperature insulationReduce gas leakage rateSealing/support meansFuel cellsMicrometer
The invention discloses a compressed sealing material for a solid oxide fuel cell stack and a preparation method of the compressed sealing material. An h-BN based sealing material is formed by combining 80-100wt% of h-BN ceramic micro powder and 0-20wt% of glass micro powder, wherein the thickness of the h-BN based sealing material is 0.25-0.3 millimeter, the grain size of the h-BN ceramic micro powder is 5-8 micrometers, the thermal expansion coefficient is 10.3*10<-6>K<-1>, the glass micro powder is selected from a SiO2-Na2O-K2O3 system, and the average grain size is 5 micrometers. The h-BNbased sealing material is used as a matrix, glass micro powder in different proportions is added, reliable sealing of the sealing material in the stack is achieved, the air leakage rate of the sealingmaterial can be effectively reduced, the high-temperature dynamic performance is improved, and a favorable sealing effect is further provided.
Owner:武汉华科福赛新能源有限责任公司

Method for manufacturing FRP reinforcement cage framework of prestressed pipe pile

The invention provides a method for manufacturing an FRP reinforcement cage framework of a prestressed pipe pile. A bottom plate, a positioning device, a shaping device and a bending device cooperateto complete the work, and the problems that in the traditional reinforcement cage framework manufacturing process, the traditional manufacturing mode is low in machining speed, bent rectangular-ambulatory-plane bundled steel bars may not be matched with main steel bars, detailed bending treatment is required, bundled steel bars have high hardness, bending in small places consumes much physical strength of personnel easily, manufacturing of the reinforcement cage frameworks in batches is difficult to realize through manual bending and the like are solved.
Owner:王蒙蒙

Co-self-assembled explosive with dense unit cell accumulation structure and preparation method thereof

The invention discloses a co-self-assembled explosive with a dense unit cell accumulation structure and a preparation method thereof. A fresh anhydrous formaldehyde-containing HNIW explosive solutionis prepared, a recrystallization technology is utilized for supersaturation, synergistic co-self-assembly of formaldehyde and HNIW is driven so as to form HNIW / HCHO co-self-assembled explosive crystals with a highly ordered accumulation structure and periodic arrangement. The molecular molar ratio of HNIW to formaldehyde molecules in the prepared co-self-assembled explosive is 2:1, and formaldehyde molecules are embedded in a unit cell cavity, so that the unit cell accumulation structure of the co-self-assembled explosive is very compact, the unit cell accumulation rate is as high as 84.01%, and the co-self-assembled explosive has good thermal stability and low sensitivity. Formaldehyde molecules are embedded to increase the unit cell accumulation dense rate and improve the reaction degree, released gas amount and safety performance of high-energy explosive, thus providing a new thought for high-energy explosive performance control.
Owner:INST OF CHEM MATERIAL CHINA ACADEMY OF ENG PHYSICS

Preparation method of bi-system high-temperature superconducting material

The invention discloses a preparation method of a bi-system high-temperature superconducting material, comprising the following steps of: preparing Bi-2212 powder into a bi-system tape material by adopting a powder tubing method and a clustered drawing technology; dissolving a bonder by using methanol or ethanol as a solvent and then adding the Bi-2212 powder to mix evenly so as to obtain suspension liquid; causing the bi-system tape material to pass through a liquid trough which is loaded with the suspension liquid and then guiding the bi-system tape material to pass through a drying furnaceso as to obtain a bi-system high temperature superconducting tape material which is externally coated with a superconducting film; and carrying out semi-melting treatment on the bi-system high temperature superconducting tape material which is externally coated with the superconducting film and then obtaining the bi-system high-temperature superconducting tape material after cooling with a furnace. The preparation process of the invention is simple, reasonable in design, low in manufacturing cost and large in popularization. In the invention, a layer of Bi-2212 superconducting film is added on the surface of the bi-system tape material prepared by a PIT method so that the silver hypergeometric of the tape material is decreased, the effective superconducting area is increased and the engineering current density of the bi-system tape material is improved.
Owner:NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH

A kind of conductive titanium oxide ceramic sputtering target material and preparation method thereof

The invention relates to a conductive titanium oxide ceramic sputtering target material and a preparation method thereof. Specifically, the present invention discloses a method for preparing a titanium oxide target, comprising the following steps: 1) providing modified titanium oxide nanopowder; 2) compressing the modified titanium oxide nanopowder into a ceramic green body; 3) sintering the ceramic green body in a vacuum atmosphere or an inert atmosphere to obtain the titanium oxide target. The invention also discloses a titanium oxide target material prepared by the method and a titanium oxide thin film obtained by sputtering the target material. The method has simple process, low cost and is easy to obtain a titanium oxide target material with uniform and stable performance, and further can obtain a titanium oxide thin film with excellent performance.
Owner:森祥(宁波)新材料有限公司

Preparation method of titanium dioxide-metal aqueous nanocomposite sol

ActiveCN104226210BEffective Composite StructureAvoid heterogeneous nucleationNanotechnologyColloidal chemistry detailsWater basedSuperoxide
The invention discloses a preparation method of titanium dioxide-metal water-based nanometer composite sol. The preparation method comprises the following steps: 1, dissolving metal salt in water to obtain a metal salt water solution, and reflowing the metal salt water solution by heating while adding a reducing agent water solution until a reflowing water solution system discolors for later use, wherein a mol ratio of the added reducing agent to metal ions is 1-50; 2, dissolving titanate in an aqueous solution of hydrogen peroxide to obtain an aqueous solution of titanium superoxide, regulating the pH value of the aqueous solution of titanium superoxide by virtue of an inorganic aqueous alkali solution; and 3, adding the aqueous solution of titanium superoxide prepared in the step 2 into the discolored metal salt water solution prepared in the step 1 to obtain a composite solution, and reflowing the composite solution by heating to obtain the final product. According to the preparation method disclosed by the invention, a metal-oxide composite structure can be effectively formed, and the process operability is high; the preparation method is suitable for batch preparation, and has a possibility of industrialized production and wide practicability.
Owner:TECHNICAL INST OF PHYSICS & CHEMISTRY - CHINESE ACAD OF SCI

Preparation method for novel electrical heating type air absorption element

The invention discloses a preparation method for a novel electrical heating type air absorption element. The preparation method comprises the following steps that (1), an air absorption alloy material is prepared, specifically, a crushed air absorption alloy is sieved through a vibrating sieving machine, air absorption alloy powder with the specific grain size range between upper and lower screens is obtained, the air absorption alloy powder with the grain size range is immersed in anhydrous ethanol to be subjected to ultrasonic treatment, and the treated air absorption alloy powder is dried for standby application; (2), a metal alloy pipe is prepared, specifically, micropores formed in a dot matrix net type structure are drilled in the pipe wall of the metal alloy pipe, and the drilled metal alloy pipe is cleaned through ultrasonic waves and dried in the air for standby application; and (3), the air absorption element is prepared, specifically, the metal alloy pipe is filled with the treated air absorption alloy powder, and the air absorption element is prepared. According to the preparation method, the technology process is simple and easy to control, the defects of powder falling, inconvenient assembly, wire breaking and the like of an existing air absorption element are overcome, and the air absorption element prepared through the method has higher mechanical strength and machining precision.
Owner:GRIMAT ENG INST CO LTD

A passenger car beam assembly

The invention relates to a cross beam assembly of a passenger car. The cross beam assembly comprises a front section beam assembly, a left connecting longitudinal beam assembly, a right connecting longitudinal beam assembly, a left back air bag support assembly and a right back air bag support assembly, wherein the left connecting longitudinal beam assembly and the right connecting longitudinal beam assembly are symmetrically arranged on back sides of left and right ends of a middle section of the front section beam assembly, and the left back air bag support assembly and the right back air bag support assembly are symmetrically arranged on back sides of left and right ends of the front section beam assembly. The cross beam assembly of the passenger car can overcome defects in the prior art, has the characteristics of high universality, high structural strength and the like and is suitable for batch and large-scale production and preparation, the production cycle can be effectively shortened, and the labor intensity can be reduced.
Owner:ANHUI ANKAI AUTOMOBILE

A kind of extruding die and method of corner expanding diameter by using bar material to prepare pipe

The invention discloses a corner diameter expanding extrusion die and method for preparing a tubular product by adopting a bar and belongs to the technical field of metal plastic working. The corner diameter expanding extrusion die comprises an upper mold plate, an extrusion core rod, an upper base plate, a core rod fixing plate, an unloading plate, a concave mold, a concave mold supporting plate,a spring, a convex mold supporting plate, a lower base plate, a lower mold plate, an inner guide pillar and an extrusion convex mold. The mold adopts the floating convex mold, and the front end of the extrusion core rod is of a cone-shaped structure, so that a material flows favorably and the extrusion force is reduced; axial extrusion, secondary corner extrusion and diameter expanding extrusiondeformation of the tubular product can be achieved by means of an extrusion channel formed by the extrusion core rod and the concave mold. The mold can achieve extruding, unloading and ejecting operations of the tubular product sequentially in one stroke, so that the extrusion die is high in production efficiency and suitable for batch preparation of superfine crystal tubular products, and can achieve industrial applications of a severe plastic deformation technique.
Owner:常熟市锡顺模具厂

A kind of preparation method of electric heating type getter element

The invention discloses a preparation method for a novel electrical heating type air absorption element. The preparation method comprises the following steps that (1), an air absorption alloy material is prepared, specifically, a crushed air absorption alloy is sieved through a vibrating sieving machine, air absorption alloy powder with the specific grain size range between upper and lower screens is obtained, the air absorption alloy powder with the grain size range is immersed in anhydrous ethanol to be subjected to ultrasonic treatment, and the treated air absorption alloy powder is dried for standby application; (2), a metal alloy pipe is prepared, specifically, micropores formed in a dot matrix net type structure are drilled in the pipe wall of the metal alloy pipe, and the drilled metal alloy pipe is cleaned through ultrasonic waves and dried in the air for standby application; and (3), the air absorption element is prepared, specifically, the metal alloy pipe is filled with the treated air absorption alloy powder, and the air absorption element is prepared. According to the preparation method, the technology process is simple and easy to control, the defects of powder falling, inconvenient assembly, wire breaking and the like of an existing air absorption element are overcome, and the air absorption element prepared through the method has higher mechanical strength and machining precision.
Owner:GRIMAT ENG INST CO LTD

High-insulation easily-rheological thermocouple boron nitride-based filling material and filling method

The invention relates to the field of boron nitride-based filling materials, and concretely relates to a high-insulation easily-rheological thermocouple boron nitride-based filling material and a filling method. The material comprises, by weight, 80-90 parts of boron nitride, 10-20 parts of glass micropowder and 1-2 parts of a binder. The rheological property of the filling material is improved by adding the glass micro powder. An h-BN ceramic block formed by extrusion is used as a possible filling material for thermocouple application, has a composite structure of a layered ceramic main body and a glass liquid phase surface in a working state, and can meet multiple requirements of high-temperature insulativity, structural stability, interface lubricity and the like of a sealing material. The filling material and a preparation method thereof are low in cost, simple to prepare, stable and reliable in quality and suitable for industrial batch preparation.
Owner:常州精瓷仪器科技有限公司

Method for synthesizing anatase type crystallizing titanium dioxide nano nuclear-shell or shell structure material by water phase one-step method

The invention relates to a preparation method of a core-shell-empty-shell structure material, in particular to a method for one-step synthesis of anatase-type crystallized titanium dioxide nano-core-shell or empty-shell structure material in an aqueous phase. In the present invention, the water-soluble titanium peroxide precursor is used for the first time to coat the nano-titanium oxide layer on the surface of polystyrene through the sol-gel method, and the shell-layer titanium oxide is directly crystallized into anatase nano-titanium dioxide at a relatively low temperature in the water phase without sintering. Not only that, through the control of the precursor, after the shell layer is formed and crystallized, the polystyrene core as the template can be dissolved spontaneously, so that the nano-titanium dioxide hollow shell structure can be directly obtained in the water phase. Compared with the traditional preparation method, the method of the present invention has simple flow, strong operability, relatively low cost, is suitable for batch preparation, has the possibility of industrial production, and is suitable for environmental purification, drug transportation, photonic crystals, etc. It has broad application prospects.
Owner:TECHNICAL INST OF PHYSICS & CHEMISTRY - CHINESE ACAD OF SCI

Cycloolefin copolymer microlens array with metal diaphragm and preparation method thereof

The invention discloses a cycloolefin copolymer microlens array with a metal diaphragm and a preparation method thereof. The preparation method disclosed in the present invention includes the steps: S101, using the first photolithography mask to form a first photoresist mask on the surface of the silicon wafer substrate by photolithography; S102, etching silicon wafer micropores on the silicon wafer substrate Array; S103. After paving the cycloolefin copolymer layer on the microwell array of the silicon wafer, heat and press to obtain the first cycloolefin copolymer array; S104. Using the reverse photolithography method to utilize the second photolithography mask Forming a second photoresist mask on the cycloolefin copolymer array to obtain a second cycloolefin copolymer array; S105, evaporating a layer of metal on the structural surface of the second cycloolefin copolymer array to obtain the second cycloolefin copolymer array Tricyclic olefin copolymer array; S106. Put the third cycloolefin copolymer array into acetone solution to obtain a cycloolefin copolymer microlens array with a metal diaphragm.
Owner:CHANGCHUN INST OF OPTICS FINE MECHANICS & PHYSICS CHINESE ACAD OF SCI

Gradient pore structure silk fibroin film and preparation method thereof

The invention discloses a preparation method of a gradient pore silk fibroin film. Blade-coating the regenerated silk fibroin wet film on a substrate, and drying to obtain a regenerated silk fibroin film; placing the regenerated silk fibroin membrane in water; and performing vacuum freeze drying on the regenerated silk fibroin film and the substrate, and stripping from the substrate after drying to obtain the gradient pore silk fibroin film. The method is simpler, more effective and more reliable, the flexible film has excellent mechanical and mechanical properties, the pore size presents gradient change in the thickness direction, and the flexible film has a compact layer and a porous layer, is excellent in biocompatibility, free of additives, free of templates, low in production cost, short in period, good in repeatability and suitable for batch preparation.
Owner:ZHEJIANG LAB
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