Preparation method of bi-system high-temperature superconducting material
A superconducting material and high-temperature superconducting technology, applied in the field of high-temperature superconducting wire rod preparation, can solve the problems of uneven Bi-2212 wire and strip, affecting the performance uniformity of wire and strip, and improving the current-carrying performance of difficult-to-wire strip. , to achieve the effect of improving engineering current density, reasonable design and low manufacturing cost
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Embodiment 1
[0018] (1) Prepare the Bi-2212 powder into a strip with a cross-sectional size of 4.2mm×0.2mm by using powder tube method and cluster drawing technology;
[0019] (2) Mix the organic solvent ethanol and the binder amino resin in a mass ratio of 50:1 to form a colloid, then add Bi-2212 powder 12 times the mass of the amino resin to the colloid and stir evenly to obtain a suspension;
[0020] (3) After the band material described in step (1) is wiped clean with ethanol, it is guided by pulleys and dip-coated in the liquid tank in which the suspension described in step (2) is housed, and then it is baked by a drying oven through pulley guides. Drying, the length of the drying furnace is 1 meter, the temperature is 100 ° C, and the running speed of the strip is 1 m / s; the dried strip is wound on the winding machine to obtain a bismuth-based high-temperature superconductor coated with a superconducting film. Guide strip material;
[0021] (4) The bismuth-based high-temperature sup...
Embodiment 2
[0024] The preparation method of this example is the same as that of Example 1, except that the binder is phenolic resin or polyvinyl butyral.
[0025] The silver-to-silver ratio of the bismuth-based high-temperature superconducting strip prepared in this example is reduced from 2 to 1.5 before adding the superconducting film, and the critical current performance of the strip is also increased by about 19%.
Embodiment 3
[0027] (1) Prepare the Bi-2212 powder into a strip with a cross-sectional size of 4.2mm×0.2mm by using powder tube method and cluster drawing technology;
[0028] (2) Mix the organic solvent methanol and the binder amino resin in a mass ratio of 100:1 to form a colloid, then add Bi-2212 powder 15 times the mass of the amino resin to the colloid and stir evenly to obtain a suspension;
[0029] (3) After the band material described in step (1) is wiped clean with ethanol, it is guided by pulleys and dip-coated in the liquid tank in which the suspension described in step (2) is housed, and then it is baked by a drying oven through pulley guides. Drying, the drying furnace is 1 meter long, the temperature is 700 ° C, and the running speed of the strip is 10 m / s; the dried strip is wound on the winding machine to obtain a bismuth-based high-temperature superconductor coated with a superconducting film. Guide strip material;
[0030] (4) The bismuth-based high-temperature supercond...
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