The invention relates to a preparation process for a thermosensitive controlled-release material for a marine antifouling agent, which belongs to the field of marine antifouling technologies. The process comprises the following steps: dissolving
chitosan in an HAc solution, adding tween 80 and
acetone, carrying out high speed stirring and ultrasonic treatment, then adding isopropanol to form an oil / water dispersion
system which is in an emulsified clear state, adding
sodium tripolyphosphate for a cross-linking solidification reaction, carrying out
filtration so as to remove liquor, flushing aresidual
solvent with
acetone and water, and carrying out
refrigeration and
vacuum drying so as to obtain microencapsulated particles; dissolving
chitosan in the HAc solution again, dissolving sodiumbeta-glycerophosphate in water, adding a
sodium beta-glycerophosphate solution into a
chitosan solution under the conditions of
ice water bath and stirring, continuing stirring, and adjusting the pH value of the solution to be 7.0; and dispersing the microencapsulated particles with water, then adding the dispersed particles into the chitosan solution, carrying out stirring, and then carrying outcentrifugation and
drying so as to obtain the thermosensitive controlled-release material. The preparation process is simple and is convenient to control; and the
prepared material has good quality, good
controlled release performance, environment friendliness and a good application effect.