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36 results about "2-propenoic acid" patented technology

Super hydrophobic silicon-fluorine polymer/nanometer silica hybridization nanometer material and preparation method thereof

The invention relates to a super hydrophobic silicon-fluorine polymer / nanometer silica hybridization nanometer material and a preparation method thereof, relating to a super hydrophobic nanometer material and a preparation method thereof. The invention provides the super hydrophobic silicon-fluorine polymer / nanometer silica hybridization nanometer material with mild reaction condition, definite reaction product structure as well as simple and convenient operation and the preparation method thereof. The preparation method comprises the following steps of: firstly, preparing nanometer silica modified by a silane coupling agent; secondly, preparing a nanometer silica atom transfer radical surface initiator; thirdly, preparing a SiO2-poly-Methacryloxypropyltrimethoxysilane macromolecule initiator; and finally preparing the silicon-fluorine polymer / nanometer silica hybridization nanometer material. The silicon-fluorine polymer / nanometer silica hybridization nanometer material has excellent high temperature resistance, ultraviolet resistance, infrared radiation resistance, oxidative degradation resistance, chemicals resistance and contamination resistance. Polymethyl 2-propenoic acid, 2,2,3,3,4,4,4-heptafluorobutyl ester has very low surface energy and very good hydrophobicity, wherein the surface energy can be as low as 0.5-1.5mN / m, and the hydrophobic angle can be over 150 degrees.
Owner:XIAMEN UNIV

Dye sensitized photoelectric conversion device and manufacturing method thereof, electronic equipment, and semiconductor electrode and manufacturing method thereof

InactiveUS20100116340A1Degrade detection efficiency or photoelectric conversion efficiencyReduce quantum yieldElectrolytic capacitorsSemiconductor/solid-state device manufacturingSemiconductor electrodeTricarboxylic acid
In a dye sensitized photoelectric conversion device having an electrolyte layer (6) between a semiconductor electrode (3) including, for example, fine semiconductor particles to which a sensitizing dye is adsorbed and a counter electrode (5), two kinds of dyes are used as the dye, and the two kinds of dyes are adsorbed onto the surface of the semiconductor electrode (3) at the sites different from each other. The fine semiconductor particles include, for example, TiO2. Tris(isothiocyanate)-ruthenium(II)-2,2′:6′,2″-terpyridine-4,4′,4″-tricarboxylic acid and 2-cyano-3-[4-[4-(2,2-diphenylethenyl)phenyl]-1,2,3,3a,4,8b-hexahydrocyclopent[b]indol-7-yl]-2-propenoic acid are used, for example, as the two kinds of dyes. Thereby, a dye sensitized photoelectric conversion device such as a dye sensitized solar cell capable of obtaining higher light absorption rate and photoelectric conversion efficiency than in a case of using one kind of dye at high purity, as well as a manufacturing method thereof are provided.
Owner:SONY CORP

Method for preparing 2-methyl-2-propenoic acid 2-ethyl-2-[[(2-methyl-1-oxo-2-propenyl)oxy]methyl]-1,3-propanediyl ester

The invention discloses a method for preparing 2-methyl-2-propenoic acid 2-ethyl-2-[[(2-methyl-1-oxo-2-propenyl)oxy]methyl]-1,3-propanediyl ester, which comprises the following steps of: (1) putting main materials of trimethylolpropane and methacrylic acid into an esterification reaction container, adding a solvent, adding a catalyst and a polymerization inhibitor A, and performing mixing reaction to obtain a reaction material; (2) controlling the pressure in the esterification reaction container to be -0.04 to -0.08MPa, raising the temperature in the esterification reaction container until reflux flows out, keeping the temperature, and beginning cooling to normal temperature until no reflux flows out or an acid value in reaction solution is detected to be 30-50mgKOH / g; (3) transferring the reaction material to a washing container, adding alkali liquor, controlling the pH value of the reaction material to be 7-8, standing until the reaction material is layered, and discharging wastewater on the lower layer; and (4) transferring the reaction material of which the wastewater is removed to a distillation container, adding a polymerization inhibitor B, vacuumizing the distillation container, and distilling to remove methylbenzene to obtain the product. The product is high in purity, good in color, and high in yield.
Owner:天津市天骄化工有限公司

Antimicrobial polymeric compositions

A method for the preparation of polymers derived from acrolein and including poly(2-propenal, 2-propenoic acid), characterised in that the polymers are exposed to the presence of water, whereby such polymers exhibit increased antimicrobial activity. The polymers may be heated in the range of 40 to 150 deg.C. Further, the polymers may be prepared in the presence of polyethylene glycols, polyols and / or alkanols.
Owner:CHEMEQ

Coloring matter-sensitized photoelectric conversion element, process for producing the coloring matter-sensitized photoelectric conversion element, electronic equipment, semiconductor electrode, and p

This invention provides a coloring matter-sensitized photoelectric conversion element comprising an electrolyte layer (6) provided between a semiconductor electrode (3) formed of, for example, semiconductor fine particles, onto which a coloring matter for sensitizing has been adsorbed, and a counter electrode (5), wherein two types of coloring matters are used as the coloring matter and are adsorbed on respective different sites on the surface of the semiconductor electrode (3). The semiconductor particles are formed of, for example, TiO2. The two types of coloring matters are, for example, tris(isothiocyanato)-ruthenium(II)-2,2':6',2''-terpyridine-4,4',4''-tricarboxylic acid and 2-cyano-3-[4-[4-(2,2-diphenylethenyl)phenyl]-1,2,3,3a,4,8b-hexahydrocyclopent[b]indol-7-yl]-2-propenoic acid. The above constitution can realize the provision of a coloring matter-sensitized photoelectric conversion element, such as coloring matter-sensitized solar cells which can realize higher level of light absorbance and photoelectric conversion efficiency than the case where a single type of high-purity coloring matter is used, and a process for producing the coloring matter-sensitized photoelectric conversion element.
Owner:SONY CORP

Multi-action mode hydrophilic organic polymer monolithic column

The invention discloses a multi-action mode hydrophilic organic polymer monolithic column, which consists of a benzene-ring group-containing organic ionic monomer, an acrylate crosslinking agent, an initiator, and a pore-forming agent. The benzene-ring group-containing organic ionic monomer is N, N, N-trimethyl(vinylbenzyl)ammonium chloride, the crosslinking agent is 2-propenoic acid, (2,4,6-trioxo-1,3,5-triazine-1,3,5(2H,4H,6H)-triyl)tri-2,1-ethanediyl ester, the pore-forming agent is a mixture of methanol and dodecanol, and the initiator is azodiisobutyronitrile. The inventive capillary chromatographic column can provide hydrogen bonds and ion exchange interaction, but also can provide rich pi-pi interaction, and can meet the rapid separation requirements of neutral, acidic and alkaline polar substances.
Owner:FUZHOU UNIV

Efficient compatilizer for polyolefin-based wood-plastic composite

The invention discloses an efficient compatilizer for a polyolefin-based wood-plastic composite, and belongs to the field of efficient compatilizers. According to the efficient compatilizer for the polyolefin-based wood-plastic composite, in the EAA extruding process, a hydroxyl functional monomer, namely 2-propenoic acid-2-hydroxyl-3-phenoxypropyl ester, and another hydrophobic monomer, namely hexadecyl methacrylate, with the synergistic effect are added and subjected to a grafting reaction on EAA molecular chains under the effect of DCP, and thus an EAA graft polymer is formed. The preparedEAA graft polymer serves as the compatilizer for the polyolefin-based wood-plastic composite, thus compatibility and hydrophobic performance of waste plant fibers such as wood flour in polyolefin canbe greatly improved, an outer sheath with a display layer is arranged at the outer end of a screw rod, thus abrasion information is given to workers in time, thus workers replace the outer sheath conveniently, and the screw rod is protected against being prone to breaking.
Owner:JIANGSU HENGFENG CABLE
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