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52results about How to "Increase the amount of introduction" patented technology

Self-suction gas-liquid mixing impeller

The invention relates to a self-suction gas-liquid mixing impeller, which mainly consists of a shaft joint, a hollow disk, and guide vanes. Both the top plate and the bottom plate of the hollow disk can be provided with guide vanes; Structures with varying thickness. The impeller of the present invention can inhale gas through the negative pressure generated during the rotation process, and disperse the gas into the liquid in the form of micro-bubbles. It has the characteristics of large suction volume, good gas-liquid mixing effect, low energy consumption, and no clogging of the impeller, and is widely used. It is used in the fields of gas-liquid mixing and reaction, and phase separation, and forms a variety of special equipment, such as wastewater biochemical treatment equipment, air flotation equipment, waste gas purification equipment, and gas purification equipment in the fields of chemical industry, pharmaceuticals, metallurgy, food, papermaking, etc. Liquid contact and reaction equipment, etc.
Owner:CHINA PETROLEUM & CHEM CORP +1

Preparation method of quaternary ammonium type positive ion polyurethane base polyether block hydrophilic silicone softener ultra-micro emulsion and product thereof

ActiveCN103497307AImprove soft feelGood application performanceGrip property fibresVegetal fibresPrepolymerIon
The invention relates to a preparation method of quaternary ammonium type positive ion polyurethane base polyether block hydrophilic silicone softener ultra-micro emulsion and a product thereof. The preparation method comprises the steps that raw materials comprising polymerization monomers, a modifier, an adjuvant and distilled water are prepared; dehydration pre-treatment is conducted on polyether ether glycol; the pre-polymerized reaction is conducted on the dehydrated polyether ether glycol, an end hydroxyl polysiloxane linear body and diisocyanate under the catalyst function of a polymerization catalyst, and a prepolymer is prepared; the chain extension reaction is conducted on the prepolymer, a tertiary amine chain extender agent and an aminosilane coupling agent and an intermediate is prepared; a polymerization stropping agent is added and the reaction is stopped, and a quaternization reagent is added for conducting a quanternization reaction; a product is prepared through emulsification. The preparation method of quaternary ammonium type positive ion polyurethane base polyether block hydrophilic silicone softener ultra-micro emulsion can give unique soft waxy style for various fabric weaving products, is used for improving the soft feel of various kinds of fabric products, does not affect the hydrophilia of natural fiber fabrics, and has good application performance and wide application prospects.
Owner:中山市天信助剂实业有限公司

Method for preparing silicone acrylic emulsion with high solid content and high silicon content

The invention relates to a method for preparing a silicone acrylic emulsion with high solid content (of over 50 percent), high organic silicon content (of over 15 percent) and low emulsifier consumption (of less than 2.5 percent), in particular a silicone acrylic emulsion for preparing high-grade exterior wall coating materials. The method comprises steps of preparing a vinyl polysiloxane emulsion by using octamethylcyclotetrasiloxane, tetravinyl tetramethylcyelo tetrasiloxane, dodecylbenzene sulfonic acid, sodium dodecyl benzene sulfonate, a non-ionic emulsifier NP-40 and deionized water through acid catalyzed ring opening, and performing silicone acrylic emulsion copolymerization of the vinyl polysiloxane emulsion and acrylic monomers in the presence of a thermal initiator to prepare the stable silicone acrylic emulsion with high solid content, high organic silicon content and low emulsifier consumption. By the method, problems that the silicon content cannot be improved substantially, the solid content is low and the emulsifier consumption is high in the preparation of the silicone acrylic emulsion are effectively solved. The silicone acrylic emulsion has excellent weather resistance, stain resistance, water resistance and the like, and has high cost performance; and the application range of the silicone acrylic emulsion is greatly widened.
Owner:武汉强力荷新材料有限公司

Inorganic-organic polymer processing agent for drilling fluid and preparation method thereof

The invention provides an inorganic-organic polymer processing agent for drilling fluid polymerized from sulfonic acid monomer, carboxylic acid monomer, nonionic monomer and inorganic material in the presence of initiator, and the inorganic material includes bentonite. The inorganic-organic polymer processing agent for drilling fluid has good effect on filtration reduction effect in fresh water drilling fluid, brine drilling fluid, saturated brine drilling fluid and compound brine drilling fluid. The inorganic-organic polymer processing agent for drilling fluid has strong anti-sloughing capability and high permeability recovery, can control hydration and dispersion of the shale effectively, can control mud making of the clay effectively, and has good effect on hydrocarbon reservoir protection. Moreover, the preparation method is simple, the sources of raw materials are wide, and the promotion prospect is wide. The invention also provides a preparation method of inorganic-organic polymer processing agent for drilling fluid.
Owner:CHINA PETROLEUM & CHEM CORP +1

Steel fiber reinforced internal curing high-strength silicate ceramsite and preparation method thereof

The invention discloses steel fiber reinforced internal curing high-strength silicate ceramsite and a preparation method thereof. Raw materials of the ceramsite are composed of dried material powder and steel fibers, wherein the doping amount of the steel fibers accounts for 0.5-3.0% of the volume of the dried material powder; the dried material powder comprises the following components in percentage by mass: 12-40% of fly ash, 25-28% of quick lime, 20-50% of diatomite and 10-15% of yellow sand. The preparation method comprises the following steps: performing wet balling, naturally curing, andperforming hydrothermal synthesis, thereby obtaining the steel fiber reinforced internal curing high-strength silicate ceramsite. The prepared ceramsite has cylinder compressive strength of 12-28MPa,a water absorption rate of 15-30% within an hour and obviously improved elasticity modulus, and can be used for preparing light concrete of an LC45-80 structure. The steel fiber reinforced internal curing high-strength silicate ceramsite disclosed by the invention has the advantages of simplifying the process and saving the equipment, energy and raw materials, the internal curing effect of lightweight aggregate on concrete can be effectively improved, and the problems that the conventional lightweight aggregate is low in cylinder compressive strength and high-grade lightweight aggregate concrete is difficultly prepared are well solved.
Owner:NANJING UNIV OF SCI & TECH

Method for preparing polyrotaxane cross-linker based on beta-cyclodextrin and product

The invention discloses a method for preparing a polyrotaxane cross-linker based on beta-cyclodextrin. The method comprises the steps of firstly, preparing polyetheramine / beta-cyclodextrin quasi-polyrotaxane by using beta-cyclodextrin and polyetheramine, and then, preparing the polyetheramine / beta-cyclodextrin / maleic anhydride polyrotaxane cross-linker by further using the polyetheramine / beta-cyclodextrin quasi-polyrotaxane and maleic anhydride. Compared with the prior art, the method disclosed by the invention has the advantages that the intake of double bonds of the prepared water-soluble polyrotaxane cross-linker is increased, the reaction activity is enhanced, and the preparation cost can be reduced.
Owner:CHONGQING UNIVERSITY OF SCIENCE AND TECHNOLOGY

Lithium battery, lithium battery diaphragm and preparation method of lithium battery diaphragm

An embodiment of the invention discloses a preparation method of a lithium battery diaphragm. The method comprises the steps of adding 10-15 parts by mass of poly(vinylidene fluoride-chlorotrifluoroethylene) and 2-7 parts by mass of lactic acid into 50-80 parts by mass of an organic solvent, and carrying out stirring and dissolving; adding 0.5-5 parts by mass of an initiator and 2-10 parts of a hydrogenation reducing agent, and then carrying out stirring and reacting; adding a reaction mixture into an alkaline aqueous solution, carrying out stirring and precipitating, and carrying out filtering, washing and drying precipitates to obtain poly(vinylidene fluoride-chlorotrifluoroethylene-lactic acid) copolymer resin; and preparing the lithium battery diaphragm from the poly(vinylidene fluoride-chlorotrifluoroethylene-lactic acid) copolymer resin. The lithium battery diaphragm is prepared from the poly(vinylidene fluoride-chlorotrifluoroethylene-lactic acid) copolymer resin, so that the lithium battery diaphragm has the characteristics of being degradable, resistant to electrolyte corrosion and high in tensile strength.
Owner:DONGGUAN DONGYANG SOLAR SCI RES & DEV CO LTD

Preparation method of high-thermal-conductivity CNTs directed modification ceramic-based composite material

The invention relates to a preparation method of a high-thermal-conductivity CNTs directed modification ceramic-based composite material. A prefab is subjected to interface layer and matrix preparation in a high-temperature furnace so that the relative density of the prefab can reach 30%-70%; ultra-short pulse lasers are adopted to prepare ceramic-based composite material thickness-direction directed holes; ultrasonic dispersion is adopted to prepare a CNTs solution, and in combination with a vacuum soaking method, filling and sealing are conducted to form CNTs directed columns; a CVI method is adopted to further compact the prefab, and the high-thermal-conductivity CNTs directed modification ceramic-based composite material is finally obtained. The technology has the advantages that through the high-thermal-conductivity CNTs directed columns, the heat conductivity of the composite material in the thickness direction is greatly improved; a CNTs interlayer dispersion structure and the CNTs directed columns form a strong heat conduction network, and the overall heat conductivity of the composite material is improved; the directed holes have designability, the size, interval and distribution of the directed holes can be designed according to engineering requirements, and operation is simple.
Owner:NORTHWESTERN POLYTECHNICAL UNIV

Preparation method of nuclear shell structure high-silicon silicone acrylic emulsion used for building exterior wall

The invention discloses a preparation method of nuclear shell structure high-silicon silicone acrylic emulsion used for building exterior walls. Firstly, the invention uses octavinyl cyclotetrasiloxane, octamethylcyclotetra siloxane, dodecylbenzene sulfonic acid, sodium dodecyl benzene sulfonate, emulsifier 0P-10 and deionized water to prepare unsaturated organo-siloxane low polymer emulsion; theorgano-siloxane low polymer emulsion, acrylate monomer mixture, initiator A, emulsifier, pH value regulator, molecular weight regulator and deionized water are adopted to polymerize nuclear emulsion;and finally, silicon acrylic nuclear emulsion, deionized water, anion / non-ion emulsifier, acrylate monomer mixture, VTES coupling agent and initiator B are adopted to polymerize nuclear emulsion to prepare high-silicon silicone acrylic emulsion. The method of the invention effectively inhibits organosilicon self-polymerization, so that the silicone acrylic emulsion of the invention has high silicon content and stable storage, has the properties of favorable weather resistance, smudge resistance, water resistance and the like, has high gloss and beautiful degree and can satisfy the requirements of high-grade buildings on exterior wall paint.
Owner:TIANJIN URBAN CONSTR COLLEGE

Organic-inorganic composite coating material, preparation method thereof, and method for preparing wear-resistant coating by using organic-inorganic composite coating material

The invention discloses an organic-inorganic composite coating material, a preparation method, and a method for preparing a wear-resistant coating by using the organic-inorganic composite coating material. The preparation method of the organic-inorganic composite coating material comprises the following steps: taking tetraethoxysilane as a precursor, and adding a silane coupling agent to prepare ahybrid silica sol; and reacting the hybrid silica sol with a titanium dioxide sol to obtain the organic-inorganic composite coating material. A matrix is pretreated, then is impregnated in the organic-inorganic composite coating material for 1-2 min, then is pulled out at a constant speed and stands for 2-4 h, and then the coating material is dried to form the wear-resistant coating on the matrix. The prepared organic-inorganic composite coating material can form the flat and compact coating on the surface of the matrix, so the wear resistance of the matrix is remarkably improved; the preparation method is simple, the production efficiency is high, and the organic-inorganic composite coating material has wide application prospects in the field of explosion-proof materials.
Owner:HEBEI UNIVERSITY OF SCIENCE AND TECHNOLOGY

Anti-shrinkage concrete and preparation process thereof

The invention relates to the technical field of concrete preparation and relates to anti-shrinkage concrete. The anti-shrinkage concrete is prepared from, by weight, 200-260 parts of cement, 30-45 parts of mineral powder, 70-110 parts of coal ash, 740-840 parts of yellow sand, 1000-1020 parts of gravels, 3-7 parts of a water reducing agent, 1-5 parts of an expanding agent, 1-5 parts of an antifoaming agent and 170-200 parts of water. By adjustment of a ratio of raw materials of the concrete and adding of functional additives, the concrete shrinkage rate is decreased, harmful cracks of concretestructures due to early shrinkage, dry shrinkage and cold shrinkage are effectively reduced, great crack resistance and seepage prevention effects are achieved, and accordingly concrete strength is improved.
Owner:浙江三门永泰建材有限公司

Remediation method of saline-alkali land soil

The invention discloses a remediation method of saline-alkali land soil. The remediation method specifically comprises the following steps of 1, selecting a certain day of the first ten days of May with sunny and rainless weather, laying a degradable waterproof thin film on the bottom after the soil is deeply dug, then laying a layer of a super-water-absorption sponge on the thin film, and then conducting backfilling of a little soil; 3, after the backfill soil is leveled, laying a layer of a salinity anion adsorption thin film on the surface of the soil, then continuing to conduct backfillingof a little soil, then laying a layer of a salinity anion adsorption thin film, then continuing to conduct backfilling of a little soil, laying a layer of a super-water-absorption sponge, and repeating the step until soil backfilling is finished; 3, after soil backfilling is completely finished, conducting exposure on the soil in the sun for 40-60 days, then ploughing the soil under to great depth, and taking away the salinity anion adsorption thin film in the soil and soil of 1-2 cm in thickness on the surface of the thin film to complete soil remediation. By means of the remediation method,by adsorbing and removing salinity cations contained in the soil, the salinity content in the soil is reduced accordingly, and the purpose of improving soil quality is improved.
Owner:孙天民

Brine separation in tall soap oil preparation

InactiveUS7084238B2Decreasing soap oil formationLimit carbon dioxide solubilityFatty oils/acids recovery from wasteNatural resin processSaline waterSodium bicarbonate
A process for separating sodium bicarbonate brine from crude tall oil or for separating sulfate brine from soap oil, such as in a recovery process in a pulp mill. A water solution having an increased density is added during the neutralization of crude tall oil soap with carbon dioxide or acidulation of soap oil with sulfuric acid.
Owner:LINDE AG

Preparation method of novel amino silicone oil modified acrylate anti-doodling emulsion

The invention discloses a preparation method of a novel amino silicone oil modified acrylate anti-doodling emulsion, which comprises the following steps: reacting an epoxy group with an amino group, adding glycidyl methacrylate during emulsion polymerization, introducing the epoxy group to the molecular chain of the emulsion, and reacting with amino-terminated silicone oil to prepare the novel amino silicone oil modified acrylate anti-doodling emulsion. According to the novel amino silicone oil modified acrylate anti-doodling emulsion disclosed by the invention, silicone oil is introduced through a cross-linking reaction, so that the problems that an organic silicon monomer is difficult to polymerize, silane active groups are easy to generate self-crosslinking, the introduction amount of organic silicon is relatively low, volatile organic compounds are polluted and the like caused by a conventional process are solved. The emulsion prepared by the invention not only has the characteristics of extremely strong adhesive force, better ethanol resistance, scrubbing resistance, mechanical shearing resistance and the like, but also has excellent high temperature resistance, weather resistance and chemical resistance, and can be widely applied to the fields of coatings, printing ink, adhesives and the like.
Owner:ANHUI XOANONS CHEM +1

Inorganic-organic polymer treatment agent for drilling fluid and preparation method therefor

The present invention provides an inorganic-organic polymer treatment agent for a drilling fluid, wherein the treatment agent is polymerized and formed by a sulfonic acid monomer, a carboxylic acid monomer, a nonionic monomer and inorganic material under the action of an initiator; and the inorganic material contains an aluminum-magnesium silicate inorganic gel. The inorganic-organic polymer treatment agent provided by the present invention has a relative strong reduction fluid loss effect in a fresh water drilling fluid, a saline water drilling fluid, a saturated saline water drilling fluid and a composite saline water drilling fluid, and further has a relative strong collapse prevention capability to control hydration and dispersion of mud shale and clay mud-making effectively. The recover value of permeability is high. The treatment agent has a relatively good hydrocarbon reservoir protecting effect. The inorganic-organic polymer treatment agent is simple in production process, wide in raw material sources, and vast in popularizing prospect. The present invention further provides a preparation method for the inorganic-organic polymer treatment agent for the drilling fluid.
Owner:CHINA PETROLEUM & CHEM CORP +1

High-wear-resistance organic silicon modified polyurethane elastomer and preparation method thereof

The invention relates to a high-wear-resistance organic silicon modified polyurethane elastomer and a preparation method thereof, and belongs to the technical field of polyurethane application. According to the high-wear-resistance organic silicon modified polyurethane elastomer disclosed by the invention, polyester polyol, reaction type organic silicon, isocyanate, a silane coupling agent and an antioxidant are used as raw materials to carry out pre-reaction, and then the polyester polyol is supplemented to prepare a polyurethane prepolymer; and reacting the polyurethane prepolymer with a chain extender to obtain the high-wear-resistance organic silicon modified polyurethane elastomer. The polyurethane elastomer disclosed by the invention not only has excellent mechanical strength, but also has relatively high wear resistance, and meets the requirements of the market on the high-wear-resistance polyurethane elastomer; meanwhile, the invention provides a simple and convenient preparation method.
Owner:SHANDONG INOV POLYURETHANE

Carbon fiber reinforced SiAlOC composite material and preparation method thereof

The invention discloses a carbon fiber reinforced SiAlOC composite material and a preparation method thereof, a three-dimensional carbon fiber prefabricated part is used as a reinforcement, and the preparation method comprises the following steps: preparing the carbon fiber prefabricated part, placing the carbon fiber prefabricated part under a vacuum condition with the pressure of less than 500 Pa, impregnating the carbon fiber prefabricated part with an Al-containing polysiloxane precursor solution, carrying out heat preservation on the impregnated carbon fiber prefabricated part, then carrying out cross-linking curing at 120-200 DEG C, carrying out cracking for 30-120 minutes at 1000-1200 DEG C in an inert atmosphere and repeating the dipping-curing-cracking period. The C / SiAlOC composite material solves the problem that the high temperature resistance of the C / SiAlOC composite material is limited, and has the advantages of low cost, good thermal stability, simple process flow, lowequipment requirements and the like.
Owner:NAT UNIV OF DEFENSE TECH

Mesoporous-microporous composite Y molecular sieve with through hole structure and preparation method thereof

The preparation method comprises the following steps: pretreating a B-Beta molecular sieve with a high boron content to prepare a boron-containing precursor, adding a silicon source, an aluminum source, an alkali source, a crystallization guiding agent and water into the boron-containing precursor, enabling the gel ratio to be (0.5-20)Na2O:1Al2O3:(3-40)SiO2:(0.005-2.0)B2O3:(80-800)H2O, stirring for 0.5-4 hours at the temperature of 5-70 DEG C, heating the gel to 80-120 DEG C, crystallizing for 12-100 hours to obtain a heteroatom B-Y molecular sieve with higher boron content, and carrying out ammonium exchange and hydrothermal hyperstabilization treatment on the synthesized heteroatom B-Y molecular sieve twice to obtain the mesoporous-microporous composite Y molecular sieve with a through hole structure. The mesoporous-microporous composite Y molecular sieve prepared by adopting the method provided by the invention has rich mesoporous structures, good connectivity between pore channels, low diffusion resistance in the pore channels of the molecular sieve, and high accessibility and utilization rate of active centers.
Owner:CNOOC TIANJIN CHEM RES & DESIGN INST +1

Method for treating inferior oil product by combined process

The invention discloses a method for treating an inferior oil product by a combined process. The method comprises the following steps: allowing an inferior oil raw material and hydrogen to enter a mixer for saturated hydrogen dissolution, and allowing an obtained mixture to pass through a hydropretreating zone; and separating a reaction effluent, allowing a separated reaction effluent and catalytic-cracked circulating oil to enter a hydrotreating reaction zone, separating an obtained reaction effluent, allowing obtained hydrotreated residual oil to undergo a catalytic cracking reaction, allowing obtained circulating oil and / or an oil slurry to be circulated to a hydropretreating reaction zone, and allowing a part of obtained circulating oil to be circulated to the hydrotreating reaction zone; wherein the reaction temperature t1 of the hydropretreating reaction zone is higher than the reaction temperature t2 of the hydrotreating reaction zone. The method provided by the invention can increase the utilization rate of a main hydrotreating catalyst, prolongs the operation cycle of a combined device, and increases the operation efficiency of a device.
Owner:CHINA PETROLEUM & CHEM CORP +1

Air volume multiplier fresh air duct suitable for integrated air-conditioning window

The invention provides an air volume multiplier fresh air duct suitable for an integrated air-conditioning window. The air volume multiplier fresh air duct suitable for the integrated air-conditioningwindow comprises an air suction opening, a motor, a turbofan, an air guiding cavity and an air duct. Coarse, medium and high efficiency air filter screens are arranged on the air suction opening in sequence to be connected with the external environment. The air guiding cavity is a long-strip-shaped wing type cavity, the inside of the air guiding cavity and outside of the air guiding cavity are smooth walls, and the tip of the air guiding cavity is in a thin-seam-opening shape. Sound absorbing materials are evenly arranged in the air guiding cavity and the air duct. According to the air volumemultiplier fresh air duct suitable for the integrated air-conditioning window, fresh air volume introduced by the integrated air conditioning window is greatly increased by the coanda effect, the effect of air multiplier is achieved, the indoor air exchange efficiency is effectively improved, the requirement of indoor fresh air volume is reached, and at the same time the fresh air can be subjected to purification and noise reduction treatment. The air volume multiplier fresh air duct suitable for the integrated air-conditioning window provides a new solving way to solve the problem of difficultly introducing the fresh air into a general residence, the performance of the air-conditioning is improved, and the improvement of indoor air quality is facilitated.
Owner:SICHUAN UNIV

Mullite fiber reinforced metal-based composite ceramic sheet and preparation method thereof

The invention provides a mullite fiber reinforced metal matrix composite ceramic sheet and a preparation method thereof.The preparation method comprises the steps that calcined aluminum oxide, magnesian soil, nanoscale fused quartz, monazite, bentonite, pyrophyllite, black talc, potassium albite, aluminum powder and sodium tripolyphosphate are mixed and then subjected to ball milling treatment, and mixed powder is obtained; performing pulping and spray granulation to obtain green body powder; the preparation method comprises the following steps: preparing a ceramic thin plate blank, pressing the blank powder into a ceramic plate-shaped blank, sintering the ceramic plate-shaped blank to obtain a ceramic thin plate blank, glazing the ceramic thin plate blank, grinding the surface, and polishing to obtain the mullite fiber reinforced metal-based composite ceramic thin plate. The invention has the advantages of simple preparation process and low raw material cost, and can be applied to the commercial fields of architectural decoration ceramics, protective materials and the like. By optimizing the solid-phase reaction sintering schedule and regulating and controlling the internal mullite crystal phase precipitation rate and precipitation amount, the prepared large-size ceramic sheet is excellent in mechanical property and wide in potential commercial market.
Owner:SHAANXI UNIV OF SCI & TECH

Inorganic-organic polymer treatment agent for drilling fluid and preparation method thereof

The invention provides an inorganic-organic polymer treatment agent for drilling fluid, wherein the treatment agent is formed by polymerization of sulfonic acid monomers, carboxylic acid monomers, nonionic monomers and inorganic materials under the action of an initiator; And the inorganic material includes aluminum magnesium silicate inorganic gel. The inorganic-organic polymer treatment agent provided by the invention has strong fluid loss reducing effect in freshwater drilling fluid, brine drilling fluid, saturated brine drilling fluid and composite brine drilling fluid. It also has a strong anti-collapse ability, can effectively control the hydration and dispersion of mud shale, control clay slurry, and has a high permeability recovery value, which has a good oil and gas layer protection effect. Moreover, the production process is simple, the source of raw materials is wide, and the promotion prospect is broad. The invention also provides a preparation method of an inorganic-organic polymer treatment agent for drilling fluid.
Owner:CHINA PETROLEUM & CHEM CORP +1

Method for treating residual oil through combined technology

The invention discloses a method for treating residual oil through a combined technology. The method for treating the residual oil through the combined technology comprises the steps of after inferiorraw material oil and hydrogen are mixed, making an obtained mixture pass through a hydrogenation pre-treatment region at first; and separating a reaction effluent, which is obtained after a reactioneffluent and catalytic cracking circulating oil enter a hydrogenation treatment reaction region, to obtain residual oil subjected to hydrogenation, carrying out a catalytic cracking reaction to obtaincirculating oil and / or slurry oil, and circulating the obtained circulating oil and / or slurry oil to the hydrogenation pre-treatment reaction region, wherein reaction temperature t1 of the hydrogenation pre-treatment reaction region is higher than reaction temperature t2 of the hydrogenation treatment reaction region. By means of the method, the utilization rate of a main catalyst for hydrogenation treatment can be improved, a running period of an integrated device is prolonged, and the running efficiency of the device is improved.
Owner:CHINA PETROLEUM & CHEM CORP +1

Inorganic-organic polymer treatment agent for drilling fluid and preparation method thereof

The invention provides an inorganic-organic polymer treating agent used for drilling fluid. The treating agent is prepared from a sulfonic acid monomer, a carboxylic acid monomer, a non-ionic monomer and an inorganic material by polymerization under the action of an initiator, wherein the inorganic material contains lithium magnesium silicate inorganic gel. The inorganic-organic polymer treating agent provided by the invention has strong effect of reducing filtrate loss in fresh-water drilling fluid, saltwater drilling fluid, saturated saltwater drilling fluid and compound saltwater drilling fluid. The treating agent also has strong anti-sloughing ability, can effectively control hydration dispersion of clay-shale and slurry making of clay, and has high permeability recovery rate and good hydrocarbon reservoir protection effects. Meanwhile, the treating agent has the advantages of simple production process, wide raw material sources and extensive popularization prospects. The invention also provides a preparation method for the inorganic-organic polymer treating agent used for the drilling fluid.
Owner:CHINA PETROLEUM & CHEM CORP +1

Carbon fiber reinforced SiYOC composite material and preparation method thereof

The invention discloses a carbon fiber reinforced SiYOC composite material and a preparation method thereof. A three-dimensional carbon fiber prefabricated part is used as a reinforcement body, yttrium-modified silicon resin is used as a precursor, the C / SiYOC composite material is obtained through repeated dipping, curing and cracking, in the process, a carbon fiber prefabricated part (such as three-dimensional braided fabric, a felt body and the like) is used as a framework, a Y-modified silicon resin precursor is impregnated under a vacuum condition, the C / SiYOC composite material is obtained by performing cross-linking curing on a precursor after thermal treatment, high-temperature cracking is performed to convert the precursor into a SiYOC ceramic matrix, and repeated dipping-curing-cracking is performed when the mass gain of the sample in the period is not more than 1% compared with that of the sample at the end of the previous period. The C / SiOC composite material has the advantages of low cost, good high-temperature resistance, low equipment requirement and the like, and the high-temperature resistance of the C / SiOC composite material can be effectively improved.
Owner:NAT UNIV OF DEFENSE TECH
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