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423 results about "Tert-butylbenzene" patented technology

Method of producing low-shrink polypropylene tape fibers

Improvements in preventing heat- and moisture-shrink problems in specific polypropylene tape fibers are provided. Such fibers are basically manufactured through the initial production of polypropylene films or tubes which are then slit into very thin, though flat (and having very high cross sectional aspect ratios) tape fibers thereafter. Such fibers (and thus the initial films and / or tubes) require the presence of certain compounds that quickly and effectively provide rigidity to the target polypropylene tape fiber after heat-setting. Generally, these compounds include any structure that nucleates polymer crystals within the target polypropylene after exposure to sufficient heat to melt the initial pelletized polymer and upon allowing such a melt to cool. The compounds must nucleate polymer crystals at a higher temperature than the target polypropylene without the nucleating agent during cooling. In such a manner, the "rigidifying" nucleator compounds provide nucleation sites for polypropylene crystal growth. Upon slitting of the initial film and / or tube, the fiber is then exposed to sufficient heat to grow the crystalline network, thus holding the fiber in a desired position. The preferred "rigidifying" compounds include dibenzylidene sorbitol based compounds, as well as less preferred compounds, such as sodium benzoate, certain sodium and lithium phosphate salts (such as sodium 2,2'-methylene-bis-(4,6-di-tert-butylphenyl)phosphate, otherwise known as NA-11). Specific methods of manufacture of such inventive tape fibers, as well as fabric articles made therefrom, are also encompassed within this invention.
Owner:MILLIKEN & CO

Nitrile rubber/modified silica-gel powder blend and preparation method thereof

The invention provides a nitrile rubber / modified silica-gel powder blend and preparation method thereof. The method comprises the following steps: adding nitrile rubble in an open mill or internal mixer; plasticating for 3-5 minutes; adding zinc oxide, eleaostearic acid, deposited white carbon black, modified silica-gel powder, sulfur, promoter and peroxide; carrying out mixing and milling at 40-60 DEG C, and obtaining the nitrile rubber / modified silica-gel powder blend; the promoter is tetrabenzylthiuramdisulfide and N-t butyl-2-benzothiazolesulfenamide; compression molding of the blend is carried out in a flat vulcanizer, and the vulcanizing temperature is 150-200 DEG C, and the vulcanizing time is 10-30 minutes, and the nitrile rubber / modified silica-gel powder blended vulcanized rubber is prepared. The blended vulcanizied rubber has the advantages of good low temperature resistance, high temperature resistance and higher fracture elongation rate. The invention can improve regeneration utilization rate of wasted silicone rubber, extend application range of silica-gel powder, and the invention has the advantages of simple processing technology, low production cost and good economic benefit.
Owner:SOUTH CHINA UNIV OF TECH +1

Polymer blend compatibilization using isobutylene-based block copolymers

Compatibilized blends of an isobutylene polymer and an unsaturated diene polymer are prepared by utilizing a compatibilizing agent comprising a block / graft copolymer containing polyisobutylene segments and C4 to C6 alkyl-substituted styrene polymer segments, such as poly(t-butylstyrene) segments.
Owner:EXXONMOBIL CHEM PAT INC

Suspension polymerization process

The present invention is a method of making polymeric particles having a predetermined and controlled size and size distribution. The method includes dissolving a polymer in a solvent to form a solution wherein the solvent is substantially immiscible with water. A suspension of small droplets of the solution is formed in water containing a water soluble promoter and a stabilizer comprising a surfactant free copolymer by high shear agitation. The stabilizer includes (i) about 55 to about 95 percent by weight, based on total monomer weight, of an addition polymerizable p-tert-butyl styrene and / or (ii) about 5 to about 45 percent by weight, based on total monomer weight, of an addition polymerizable ionic monomer. The solvent is removed from the droplets and the solidified polymer particles are separated from the water. The present invention as provides polymer particles having a core of polymer coated with a layer of smaller particles of a copolymer of the stabilizer described in the method.
Owner:EASTMAN KODAK CO

Preparation and application method of polyvinyl chloride (PVC) resin terminator

InactiveCN102492064ADifficult to constitute migrationNot easy to cause volatile lossPhosphoric Acid EstersPolymer science
The invention relates to a preparation and application method of a polyvinyl chloride (PVC) resin terminator, belonging to the technical field of chemical products. The invention particularly relates to a liquid antioxidant product, which mainly comprises 2,6-di-bert-butyl-4-(1-phenylethyl)phenol and is obtained by carrying out catalytic alkylation reaction on 2,6-di-bert-butyl phenol and styrene as raw materials. An organic solvent is added into the liquid antioxidant product which mainly comprises the 2,6-di-bert-butyl-4-(1-phenylethyl)phenol, and is sufficiently stirred to obtain the liquid antioxidant product HKY-10. The HKY-10 is compounded with a benzofuran ketone antioxidant and a phosphite ester antioxidant to obtain an oil-soluble compound liquid terminator product as a terminator for a general-purpose PVC resin product preparation process by a suspension method; and the liquid terminator is added in a polymerization reaction process to obtain a PVC resin product with stable properties, thereby enhancing the aging whiteness of the PVC resin product. The PVC resin terminator has the characteristics of no toxicity and environmental protection, and does not generate water pollutants.
Owner:CHANGZHOU UNIV

Calixresorcinarene compound, photoresist base comprising the same, and composition thereof

A calixresorcinarene compound represented by the following formula (1):wherein eight Rs are n (n is an integer of 1 to 7) substituents that are one or more types of substituents selected from groups represented by the following formula (2), and m (m is an integer shown by 8-n) hydrogen atoms; and R's, which may be the same or different, are each a straight-chain aliphatic hydrocarbon group having 2 to 12 carbon atoms, a branched aliphatic hydrocarbon group having 3 to 12 carbon atoms, a phenyl group, a p-phenylphenyl group, a p-tert-butylphenyl group, and an aromatic group represented by the following formula (3), or a substituent formed by combining two or more of these substituents:wherein R″ is a hydrogen atom or a substituent selected from the substituents represented by the formula (2).
Owner:KINOSHITA HIROO +2

90-degree special temperature selflimiting electric tracing band

InactiveCN101795507AEnhance positive temperature coefficient effectSolve the service lifeHeating element shapesSilicic acidSalicylic acid
The invention discloses a 90-degree special temperature selflimiting electric tracing band, which comprises a conductive core, and a PTC material layer, a polymer insulating inner protective sleeve, an aluminum-magnesium alloy shielding layer and a polymer insulating outer protective sleeve which are covered outside the conductive core in turn, wherein the PTC material is prepared by mixing and melting the following raw material components in part by weight: high-density polyethylene 86-87, carbon black 12-14, tribasic lead sulfate heat stabilizer 0.11-0.13, lead silicate 0.04-0.06, styrenated phenol antioxygen 0.05-0.15, p-tert-butylphenyl salicylate light stabilizer 0.12-0.14 and tribromophenol fire retardant 0.05-0.15. The highest temperature of the band is maintained at 90+ / -5 DEG C, and the band can be used as solar electric tracing band in places with large temperature difference.
Owner:芜湖科阳新材料股份有限公司

Dielectric rubber body for packaging sensor and radio-communication system taking dielectric rubber body as carrier

The invention relates to a dielectric rubber body for packaging a sensor. The dielectric rubber body is characterized in that the formula thereof comprises 60-70 parts of chlorinated butyl rubber, 10-20 parts of butadiene styrene rubber, 20-30 parts of natural rubber, 20-30 parts of light calcium carbonate, 30-40 parts of carbon black, 5-10 parts of conductive carbon black, 1-3 parts of stearic acid, 2-5 parts of magnesium oxide, 1-5 parts of octyl phenol-phenolic resin, 3-6 parts of zinc oxide, 1-3 parts of N-tertiary butyl-2-benzothiazole sulfenamide, 0.5-2 parts of tetramethyl thiuram disulfide, and 0.5-2 parts of insoluble sulphur. The dielectric rubber body disclosed by the invention is used for a conductive radiofrequency device in tire; the device comprises a radio assembly and an antenna, and can be used for tracking and recording data during manufacturing, sales and use; and the measurement range covers temperature, pressure or other physical parameters in tire. During the loading process of a sensor, the conductive material with a certain dielectric constant and a certain adhesive force disclosed by the invention is chosen, so that the device can be firmly connected with a tire and can be used for transmitting data more stably; simultaneously, via high elasticity and good mechanical property of rubber, the device can withstand the stress brought by cyclic deformation of the tire excellently.
Owner:QINGDAO TONGSHENGTONG RUBBER & PLASTIC

Antifreeze Concentrate and Coolant Compositions and Preparation Thereof

An antifreeze composition having improved thermal stability is provided. In one embodiment, the antifreeze concentrate composition comprises from 50 to 99 wt. % of a glycol-based freezing point depressant selected from the group of: alkylene glycols, glycol monoethers, glycerins, and mixtures thereof; 0.01 to 10 wt. % of at least one of a 2-ethylhexanoic acid, isononanoic acid and 3,5,5-trimethylhexanoic acid; and 0.01 to 5 wt. % of at least one of octanoic acid, nonanoic acid, decanoic acid, undecanoic acid, dodecanoic acid, neodecanoic acid, benzoic acid, 2-hydroxybenzoic acid, p-terbutylbenzoic acid, and mixtures thereof. In one embodiment, the composition is employed as a concentrate in admixture with 10 to 90 wt. % water.
Owner:ARTECO NV

A method of preparing a high-performance wood plastic composite by utilization of waste polystyrene

InactiveCN105348837AGood dispersionStrong interface bindingPolytetrafluoroethyleneBenzotriazole
A method of preparing a high-performance wood plastic composite by utilization of waste polystyrene is disclosed. The method includes a step of drying corn straw, smashing, sieving, dipping with an acid, and adding a silane coupling agent KH-550 and N,N-bis(2-hydroxyethyl) alkyl amine to obtain modified corn straw; a step of smashing waste polystyrene foam to obtain pretreated polystyrene; a step of fully mixing the modified corn straw, nanometer titanium dioxide, molybdenum disulfide, nanometer aluminium hydroxide, nanometer zinc stannate, a silane coupling agent KH-560, a silane coupling agent KH-570, a foaming agent, polytetrafluoroethylene, dicumyl peroxide and the pretreated polystyrene, maintaining the temperature at 140-155 DEG C for 2.5-5 min, and allowing the mixture to stand to obtain a preheated material; and a step of fully mixing the preheated material, nylon, polycarbonate, sulfonated polystyrene, benzotriazole, tris(2,4-ditert-butylphenyl) phosphite, pentaerythritol dioleate and butadiene styrene rubber, and performing hot press processing.
Owner:ANHUI GUANGYUAN TECH DEV

Process for producing 1,4-(2,4-diaminophenyloxy)-2,5-di-t-butyl benzene

The invention relates to a preparation method of 1,4-double(2,4-diamino phenoxy)-2,5-d-tert-butylbenzene, comprising the steps as following, after being put into the solvent system of the solution of palladium or carbon hydrazine hydrate and saturated fatty alcohol for reaction for 1 to 5 hours with the temperature of 70 to 85 DEG C, the 1,4-double(2,4-dinitro phenoxy)-2,5-d-tert-butylbenzene is filtered when being hot, mother liquor is cooled off, pure water is dripped in, crystal products are precipitated, filtered, and dried in vacuum, and crystals of the 1,4-double(2,4-diamino phenoxy)-2,5-d-tert-butylbenzene are gained. The method has the simple operation, needs no subsequent refining and purifying technique, takes little time, has the products with the high yield and the purity of more than 99 percent, and is suitable for industrial production.
Owner:DONGHUA UNIV

Improve method for preparing N-tert-butylbenzothiazolesulfenamide

The invention belongs to the field of fine chemical engineering, and relates to an improved method for preparing N-tert-butylbenzothiazolesulfenamide. 2-benzothiazolethiol and tertbutylamine are taken as raw materials, and undergo oxidation reaction by using sodium hypochlorite as an oxidant in the presence of an ionic or nonionic surfactant, and after the reaction is finished, a proper amount of reducing agent is added to remove unreacted sodium hypochlorite so as to improve the stability in the process of drying the product. In the method, sulfuric acid and sodium hydroxide are not needed, so that wastewater amount is small, the product yield is over 95 percent, the smelting point is 105DEG C, and the insoluble matter content in methanol is stabilized in a range of 0.28 to 0.68 percent and reaches the national standard. The consumption of main raw materials is low, and the method is suitable for industrial production.
Owner:CHINA PETROLEUM & CHEM CORP +1
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