The invention discloses a
halogen-free synergistic
flame-retardant silica
aerogel preparation method, which comprises: S1, mixing a
halogen-free
flame retardant agent, an inorganic synergist and a first
solvent, and carrying out ball milling dispersing to obtain a suspension A; S2, uniformly mixing a
silicon source and water, adding an acidic
aqueous solution, uniformly mixing to obtain a
silicic acid
sol, adding the suspension A obtained in the S1 to the
silicic acid
sol, uniformly mixing, adjusting the pH value to 5-6, adding a
drying control chemical additive, stirring, heating, carrying out
thermal insulation, and crushing to obtain a
sol B; and S3, taking the sol B obtained in the S2, carrying out
solvent exchange, modifying with a
silane coupling agent, and
drying to obtain the
halogen-free synergistic
flame-retardant silica
aerogel. According to the present invention, the halogen-free synergistic flame-retardant silica
aerogel has advantages of good flame-retardant property, low
combustion heat value,
low density, good hydrophobicity, large specific surface area, simple operation, and low production cost.