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61results about How to "Dense particles" patented technology

Coking-resistant hydrocarbon cracking furnace pipe and preparation method thereof

The invention provides a coking-resistant hydrocarbon cracking furnace pipe and a preparation method thereof. A cracking furnace pipe is subjected to two-stage high-temperature heat treatment in a H2- and vapor-containing low-oxygen partial pressure gas atmosphere so that a manganese-chromium spinel coating is formed on the inner surface. In the first-stage high-temperature heat treatment, a mole ratio of H2 to vapor is in a range of 1792-107 and in the second-stage high-temperature heat treatment, a mole ratio of H2 to vapor is in a range of 1-1791. The manganese-chromium spinel has a structural formula of MnxCr3-xO4 and x is in a range of 0.5-1.5. The manganese-chromium spinel coating reduces deposition of coke on the inner wall of a radiation-section furnace pipe in hydrocarbon cracking and prolongs an operation period and a use life of the furnace pipe.
Owner:CHINA PETROLEUM & CHEM CORP +1

Semi-solid rheo-extrusion casting technology and equipment of hypereutectic Al-Si alloy casting

The invention provides a hypereutectic Al-Si alloy semi-solid rheological squeezing casting technique and a device, which pertains to a technical field of metal material semi-solid forming. The technique comprises the steps: alloy molten metal is smelted; hypereutectic Al-Si alloy semi-solid sizing agent is prepared by an electromagnetic stirring method; the sizing agent is cast into a holding furnace with a temperature of 610 DEG C-630 DEG C for storing; then a quantitative vacuum cup is utilized to cast the sizing agent into a mould which is preheated with a temperature of 150 DEG C-250 DEG C; the sizing agent is squeezing cast with a squeezing speed of 0.1mm / s-0.5mm / s, under moulding pressure of 50MPa-150MPa and with a pressure-keeping time of 10s-80s. The semi-solid continuous rheological squeezing casting of the hypereutectic Al-Si alloy products is realized, which improves the utilization ratio of the materials, reduces finishing allowance and reduces energy consumption but also refines granules of primary Si, refines and spheroidizes eutectic structure. The whole structure of a cast is compact with high-quality surface. The technique is simple and has short process, small investment of equipment, low cost and relatively strong practicability of the technique and the equipment.
Owner:KUNMING UNIV OF SCI & TECH

Muscovy duck formula pellet feed manufacturing method

The invention discloses a Muscovy duck formula pellet feed manufacturing method. The Muscovy duck formula pellet feed manufacturing method comprises the steps that cobs, poison sumac stem leaves and water spinach are saccharified, green plants comprising cucumbers and endive and cooked potatoes, cooked pumpkins, cooked Chinese yam, cooked pepper, cooked bone meal and the like are added, and after the mixing technology, the pellet manufacturing technology, the drying technology and the like are adopted, nutritive fitness type Muscovy duck daily feed is manufactured, wherein the feed is rich in vegetable protein, multivitamin, pectin and the like and capable of whetting appetite, promoting growth and achieving the functions of clearing heat and toxin and relaxing the bowel. The finished feed is rich in soft fiber, compact in pellet, good in taste, high in conversion efficiency and capable of preventing and treating staphylococcus aureus and dysentery which often attack Muscovy dusks.
Owner:东兰县科技情报研究所

Electronically conductive metal organic frame film and preparation method and application thereof

The invention discloses an electronically conductive metal organic frame film and a preparation method and an application thereof. The EC-MOFs film has high quality and controllable thickness, the disadvantage that an EC-MOFs nano porous film whose thickness and quality are not controllable layer and layer on the nanometer scale in the prior art is solved, and the EC MOFs film obtained in the invention applied to a room temperature chemical resistance type gas sensor has high selectivity and fast response.
Owner:FUJIAN INST OF RES ON THE STRUCTURE OF MATTER CHINESE ACAD OF SCI

Low-temperature thermal control phase change microcapsule and preparation method thereof

The invention provides a low-temperature thermal control phase change microcapsule and a preparation method thereof. The low-temperature thermal control phase change microcapsule takes paraffin alkane as a core material and urea resin as a shell, and further comprises a heat conduction filler, the heat conduction filler is added in the process of coating the paraffin alkane by the urea resin, and the amount of the added heat conduction filler is 5%-30% that of the paraffin alkane. The low-temperature thermal control phase change microcapsule prepared by the invention is solid-solid phase change, the problems of fusion flowing and permeation migration are avoided, the range of phase change temperature is wide, the latent heat is large, the condensate depression is small, the phase change process is stable, the phase change is reversible, the material further has a higher heat conduction property, and as a relatively ideal thermal control phase change material, the low-temperature thermal control phase change microcapsule can be widely used in the fields of thermal protection, like aerospace, precise instruments, and electron devices.
Owner:海鹰空天材料研究院(苏州)有限责任公司

Spherical rhenium powder preparation method

The invention relates to a spherical rhenium powder preparation method. The spherical rhenium powder preparation method is used for preparing spherical rhenium powder with the particle size ranging from 10 microns to 100 microns. According to the spherical rhenium powder prepared through the method, a small number of holes are formed inside a powder body, the content of hollow spheres is low, theapparent density is high, and powder compactness is good. According to the method, the plasma spherizing process is optimized, losses of the minute powder are reduced, and the yield of the spherical rhenium powder is increased.
Owner:CHONGQING MATERIALS RES INST

Telescopic compound fertilizer rotary drum granulator

The invention relates to a telescopic compound fertilizer rotary drum granulator comprising a support (1), a feeding port (2), a supporting wheel (4), a frame (8), and a discharging port (9). The frame (8) is provided with an inner cylinder (7) and an outer cylinder (6) sleeved on the inner cylinder (7), wherein the rotation directions of the inner cylinder (7) and the outer cylinder (6) are the same, but the rotation speeds of the inner cylinder (7) and the outer cylinder (6) are different. Granulating rods (3) are distributed in a threaded form on the outer wall of the inner cylinder (7). The inner cylinder (7) is arranged on the support (1) through a shaft, wherein the cylinder (7) can rotate. The outer cylinder (6) is arranged on the frame (8) through the supporting wheel (4). The feeding port (2) is arranged on one end of the outer cylinder (6), and the discharging port (9) is arranged on the other end of the outer cylinder (6). Compared to existing technologies, the granulator provided by the invention is advantaged in small volume, simple structure, high granulating rate, and no restriction on raw material performance. With the telescopic compound fertilizer rotary drum granulator provided by the invention, materials with any formula can be produced.
Owner:SHANGHAI RES INST OF CHEM IND

Manufacturing method of codonopsis lanceolata stem leaf pellet feed

The invention discloses a manufacturing method of codonopsis lanceolata stem leaf pellet feed. Stem leaves of perennial sprawl herbaceous plant codonopsis lanceolat, high-yield and high-quality vegetable pumpkin and mater convolvulus, auxiliary green red pepper and corns are adopted to undergo the process of raw material pretreatment, steaming processing pulping, burdening, pelleting and drying and the like, so that the daily feed which is rich in chlorophyll, pectin, vegetable protein and various vitamins and the like, promotes appetite and salivary secretion, enhances appetite and is nutritious, hygienic and suitable for poultry and fattening pigs is made. The finished product feed contains rich tough fibers, is compact in particles and good in palatability, has the effects of clearing heat and cooling blood, detoxicating and curing sore, loosening the bowel to relieve constipation and the like, and has good prevention and therapeutic effects on dysentery, lung abscess and intestinal dryness with constipation and the like which occur commonly in livestock.
Owner:汪永辉

Frictional heat self-sintering antifriction material

The invention belongs to the friction material field of friction stopping devices used in transport machinery and various engineering operation machineries, and relates to a friction heat self-sintering friction-resistant material. The material comprises the following raw materials by weight percent: 10 to 16 percent of adhesive, 8 to 20 percent of modified framework material, 10 to 20 percent of friction stabilizer, 10 to 25 percent of plasticizing fiber, 5 to 15 percent of various auxiliary agents, 3 to 13 percent of sintering material, 8 to 18 percent of friction-increasing agent, 2 to 8 percent of chopped glass fiber, 3 to 16 percent of petroleum coke and 4 to 16 percent of coke dust. The invention is characterized in that: ceramic-like material is converted into compound with low melting point by utilization of the heat on a friction surface; moreover, the conversion ensures that grains are refined and compact and distributed more evenly. Test result shows that the friction material has stable friction coefficient, small fluctuation, not more than +-0.035 deviation, less abrasion loss, long service life, no braking noise, no smoke and spark and no dust; moreover, the outstanding characteristic of the friction material lies in that the material does not cause damages on a brake drum (disc).
Owner:信义集团公司

Coking-inhibition hydrocarbon cracking furnace pipe and preparation method thereof

The invention provides a coking-inhibition hydrocarbon cracking furnace pipe and a preparation method thereof. The preparation method comprises the following steps that through a cracking furnace pipe as a barrel-shaped cathode, elemental manganese or a mixture of manganese and aluminum is treated according to a glow discharge principle to form manganese ions or a mixture of manganese ions and aluminum ions, the manganese ions or the mixture of manganese ions and aluminum ions fast permeates into an inner surface of the cracking furnace pipe at a high temperature along crystal defects and then form a manganese or manganese-aluminum permeated layer, and in low-oxygen partial pressure gas atmosphere containing H2 and water vapor, a high-temperature treatment process is carried out so that a manganese-chromium spinel or manganese-aluminum spinel coating is formed on the inner surface of the cracking furnace pipe. The manganese-chromium spinel or manganese-aluminum spinel coating can reduce coking and carburization of the cracking furnace pipe and prolong an operation period and a service life of the cracking furnace pipe.
Owner:CHINA PETROLEUM & CHEM CORP +1

Testing device and method for inducing calcium carbonate precipitation to solidify sandy soil by microorganisms in negative pressure environment

The invention discloses a testing device for inducing a calcium carbonate precipitation to solidify sandy soil by microorganisms in a negative pressure environment. The testing device comprises a culture box, an oxygen conveying device and a vacuumizing device. The invention further discloses a testing method for inducing the calcium carbonate precipitation to solidify the sandy soil by the microorganisms in the negative pressure environment. The method comprises the steps of manufacturing a sandy soil test piece, preparing a nutrient solution, mixing bacteria and the nutrient solution, debugging a culture environment, maintaining the aerobic negative pressure environment and the like. The disclosed testing method explores that under a negative pressure condition, along with the progressive increase of maintaining time, a rapid increased tendency appears in the strength of inducing the calcium carbonate precipitation to solidify the sandy soil by the microorganisms, and is superior tothe sand solidifying effect in a normal atmospheric pressure environment. The method has remarkable guiding significance in the actual application of negative pressure environmental engineering.
Owner:CHONGQING UNIVERSITY OF SCIENCE AND TECHNOLOGY

Film-base electric device

The present invention provides a film-base electric device comprising an electronic conductive metal organic frameworks (EC-MOFs) film. The EC-MOFs film is used as the active layer of the electric device. The electric device also includes more than two electrodes. At least one of the more than two electrodes is disposed on the EC-MOFs film or the more than two electrodes are disposed under the EC-MOF film. The EC-MOFs film of the present invention is applied to a room temperature chemical resistance type gas sensor with high selectivity and fast response, and has good effects.
Owner:FUJIAN INST OF RES ON THE STRUCTURE OF MATTER CHINESE ACAD OF SCI

Preparation method of ITO thin film

The invention belongs to the field of photoelectric materials, and provides a preparation method of an ITO thin film. The preparation method of the ITO thin film comprises the following steps that an indium source and a tin source are dissolved to prepare an indium source and tin source mixture organic solution, stabilizers and surfactants are added for ageing processing, and then ITO sol is obtained; after one time of pulling coating is conducted on the ITO solution on a base body, high-temperature preheating processing is conducted, then annealing processing is conducted, and the ITO thin film is obtained. The high-temperature preheating processing method comprises the step of preheating the base body coated with the ITO solution for 30 min in a muffle furnace at the temperature of 400-600 DEG C in the air atmosphere. According to the preparation method of the ITO thin film, the ITO thin film is prepared by the adoption of the sol-gel dip-coating technology. The preparation method is simple, the doping amount is easy to control, the obtained ITO thin film is flat in surface and compact in particle, the transmittance in the visible light region of the obtained ITO thin film reaches 90%, the electrical resistivity of the obtained ITO thin film reaches 4-10 levels, the power function of the obtained ITO thin film reaches 4.9 eV, and the requirement for thin film electrodes of solar cells can be met.
Owner:徐东

Bright black nickel electroplating solution, preparation method thereof, electroplated part and electroplating method of bright black nickel

The invention belongs to the technical field of electroplating, and particularly relates to a bright black nickel electroplating solution, a preparation method thereof, an electroplated part and an electroplating method of bright black nickel. The bright black nickel electroplating solution preparation method comprises the following steps that 1) under the condition that the temperature is 35-55 DEG C, every 5-25g of chitosan nickel complexes is dissolved in 1L of an additive A solution with the concentration of 10-45g / L; 2) 25-105g of nickel sulfates, 15-75g of nickel chlorides, 1-3g of magnesium sulfates, 2-10g of copper sulfates and 10-55g of ammonium thiocyanates are added into the solution sequentially and stirred until all the salts are completely dissolved; 3) 25-55g of additives Bare added and stirred until the additives B are completely dissolved; and 4) 20-65g of additives C and 1-6g of additives D are further added and stirred until the additives C and the additives D are completely dissolved, and the solution becomes a transparent or semitransparent solution and then is cooled to the room temperature. A bright black nickel coating prepared with the bright black nickelelectroplating solution has the advantages of being bright, compact, wear-resistant, corrosion-resistant, good in electrical conductivity and the like; and a coating crystal structure is uniform in grain size, stable in chemical composition and capable of being regulated and controlled.
Owner:东莞奕创表面处理科技有限公司

Method for improving weather resistance of decorative base paper titanium dioxide

The invention provides a method for improving weather resistance of decorative base paper titanium dioxide, and belongs to the technical field of decorative base paper titanium dioxide. The control is performed through salt treatment and calcination. The method comprises the following steps of A, using bleached slurry as raw materials; adding titanium dioxide sol into the raw materials; controlling the addition to meet the requirement that the proportion of TiO2 in the titanium dioxide sol to TiO2 in metatitanic acid is 2 to 6 percent; performing water washing; diluting the slurry subjected to water washing into 300 to 400g / L TiO2 slurry; B, adding potassium and phosphorus solution with the K2O / P2O5 ratio being 1.3 to 4.0 into the diluted slurry; performing stirring; adding aluminum-containing compound solution according to the Al2O3 to TiO2 proportion being 0.3 to 0.9 percent; performing stirring; C, performing pressurized filtering on the slurry material treated by the step B until the filter cake solid content is 45 to 55 percent; C, roasting the filter cake in the step C for 8 to 10h at the roasting temperature of 200 to 950 DEG C. Through the control on the salt treatment and roasting processes, the primary product weather resistance of the decorative base paper titanium dioxide is improved; the weather resistance of the decorative base paper titanium dioxide is further improved.
Owner:HEBEI MILSON TITANIUM DIOXIDE

Preparation device and preparation method of high-tap-density ternary precursor material

The invention discloses a preparation device of a high-tap-density ternary precursor material, which comprises a seed crystal reaction kettle (1), a thickener (7) and a seed crystal tank (8), the seed crystal reaction kettle is respectively connected with the thickener and the seed crystal tank, and a pipeline connected between the seed crystal reaction kettle and the seed crystal tank is connected with the thickener; a stirrer (2) and a baffle (5) are arranged in the seed crystal reaction kettle, and a guide cylinder (3) is arranged on the inner wall of the seed crystal reaction kettle (1). The preparation method comprises the following steps: preparing a mixed sulfate solution of nickel, cobalt and manganese; preparing a base solution and introducing protective gas; adding a mixed sulfate solution, industrial liquid alkali and ammonia water to the height of an upper-layer paddle, and starting a stirrer; extracting supernate by the thickener, returning the supernate to the seed crystal reaction kettle, and overflowing the supernate to the seed crystal tank; and introducing seed crystal particles into the seed crystal reaction kettle for continuous reaction to obtain a material with a target particle size, and treating the material to obtain the high-tap-density ternary precursor material. The prepared material is high in tap density and good in particle uniformity.
Owner:JINGMEN GEM NEW MATERIAL

Easily formed biomass fuel

InactiveCN104403715ADense particlesAvoid the problem of high demand and difficult collectionBiofuelsSolid fuelsNew energyAdhesive
The invention discloses easily formed biomass fuel, and relates to the technical field of fuel. The easily formed biomass fuel is prepared from the following raw materials in percentage by weight: 50-60% of ramulus mori, 30-40% of rice husk, 5% of high clay and 5% of a biomass combustion-supporting adhesive. Biomass granular fuel is prepared through procedures of crushing, drying, compression, screening, cooling and packaging. The high clay comprises 50-60% of silicon, 20-30% of aluminum oxide and 0.15-0.2% of iron. The mixed biomass granular fuel is dried, and the moisture content is up to 10-13%. By adopting the easily prepared biomass fuel, the problems that biomass fuel is single in component, the raw material processing yield is low and the formation rate is low are solved, the environment pollution caused by discarded or combusted ramulus mori is avoided as the ramulus mori and the rich husk are adopted as raw materials for preparing the biological fuel, new energy is developed, and the easily formed biomass fuel is an important method for increasing the income of farmers.
Owner:柳州东侯生物能源科技有限公司

Preparation method for spherical monocrystal tungsten powder for thermal spraying

The invention discloses a preparation method for a spherical monocrystal tungsten powder for thermal spraying. The preparation method comprises the following steps: firstly adding a certain amount of a mixture of lithium carbonate and sodium chloride in an ammonium tungstate solution as a mother solution, and concentrating to obtain a precursor through heating drying; then selecting a spherical tungsten powder as a mother crystal, adding the spherical tungsten powder in the precursor according to a certain ratio, uniformly mixing, and then placing the mixture in a tubular reduction furnace and carrying out hydrogen gas reduction, and then sequentially carrying out ultrasonic cleaning, vacuum drying and grinding spheroidization to prepare an intermediate; and carrying out airflow classification on the prepared intermediate to obtain the spherical monocrystal tungsten powder. The preparation method disclosed by the invention is simple in process equipment and high in production efficiency; and the prepared spherical monocrystal tungsten powder has a perfect crystal, compact particles, a high sphericity degree, high flowability, a high purity, a high coating hardness, a high powder-applying rate and a low porosity.
Owner:LUOYANG GOLDEN EGRET GEOTOOLS

CeO2-based composite solid electrolyte material and preparation method thereof

The invention discloses a CeO2-based composite solid electrolyte material and a preparation method thereof. The structural general formula of the CeO2-based composite solid electrolyte material is asfollows: Ce0.8Pr0.1La0.1O2-delta.x(Li0.5K0.5Cl), and delta is oxygen deficit. The Ce0.8Pr0.1La0.1O2-delta material is doped with a specific low-melting-point salt Li0.5K0.5Cl through a microwave combustion-supporting method, the CeO2-based solid composite electrolyte material is formed, the conductivity of the material in medium and low temperature stages can be greatly improved, the electrochemical performance of the material is improved, and the method is simple in preparation process, low in cost, quick, energy-saving and environment-friendly.
Owner:HEFEI UNIV

Preparation method of rare-earth composite alumina balls

The invention discloses a preparation method of rare-earth composite alumina balls. The preparation method includes the steps of S1, dissolving a rare-earth metal compound into water, dropwise addingan alkaline solution to regulate pH to 8-9, and stirring for 0.5-2 hours to obtain rare-earth metal hydroxide slurry; S2, mixing rare-earth metal hydroxide slurry, a binder and deionized water according to the mass ratio of (0.5-0.8):(0.8-1.2):(40-44), and stirring to obtain atomization slurry; S3, feeding an alumina material and the atomization slurry into the stock bin of a fluidized bed to perform granulation so as to obtain products; S4, baking to dry the products to obtain the needed rare-earth composite alumina balls. The rare-earth composite alumina balls prepared by the method is highabsorption efficiency to fluoride ions in wastewater.
Owner:福建璞睿泰科新材料科技有限公司

Nickel-cobalt-aluminum hydroxide precursor, preparation method thereof, anode material and battery

The invention relates to the field of electrochemical technologies, in particular to a nickel-cobalt-aluminum hydroxide precursor, a preparation method thereof, an anode material and a battery. The preparation method of the nickel-cobalt-aluminum hydroxide precursor comprises the steps that a surfactant is added into a reaction system of a chemical coprecipitation method for modification, growth of particles of the nickel-cobalt-aluminum hydroxide precursor is promoted, and the form of the nickel-cobalt-aluminum hydroxide precursor tends to be spherical. According to the preparation method, byadding the surfactant during chemical coprecipitation, size increase of the particles, particularly first-time particles, is benefited, granularity is uniform, the form tends to be spherical, variousactive groups exist on the organization structure of the nickel-cobalt-aluminum hydroxide precursor, therefore, metal ions are chelated or adsorbed, or crystals can grow directionally or generate hydrogen-bond interaction with other compounds. As a result, the material structure is more complete, the degree of crystallinity is higher, and the electrochemical performance of the precursor is improved.
Owner:INST OF RESOURCES UTILIZATION & RARE EARTH DEV GUANGDONG ACAD OF SCI

Sandy silt subgrade filling construction method and application thereof

The The invention relates to the technical field of subgrade engineering, and particularly discloses a sandy silt subgrade filling construction method and application thereof. According to the sandy silt subgrade filling construction method, sandy silt doped with a curing agent serves as a subgrade, the CBR strength of the subgrade can greatly meet the construction requirement after the subgrade is fully compacted under the optimal water content, and theunconfined compressive strength is effectively improved. Meanwhile, the curing agent can generate more gel substances, so that soil sample particles are more compact, the strength and the stability of a cured soil body are greatly improved, the volume shrinkage in the freezing and thawing process is effectively reduced, the phenomena of local pulverization and peeling and corner falling of the soil sample are improved, and then the freezing and thawing cycle resistance can be effectively improved; and the problem that an existing sandy silt subgrade filling construction method cannot effectively improve the freeze-thaw cycle resistance of a sandy silt subgrade is solved, and wide market prospects are achieved.
Owner:CCCC FOURTH HIGHWAY ENG +1

Solidified substrate manufacturing device and process and solidified substrate manufactured through solidified substrate manufacturing device and process

The invention provides a solidified substrate manufacturing device and process and a solidified substrate manufactured through the solidified substrate manufacturing device and process, and belongs tothe field of plant cultivation. The solidified substrate manufacturing process comprises the following steps of raw material preparation; charging; heat curing, wherein a high-energy heat source is started, heat is diffused upwards from the bottom face of a mold to gradually heat raw materials, hot-melt cured fibers are controllably melted, meanwhile, a pressure mechanism is started to control apressing block to move, the raw materials are evenly compressed, and the raw materials are bonded; and cooling molding, wherein the high-energy heat source and the pressure mechanism are closed, heating of the raw materials and moving of the pressing block are stopped, cooling and demolding are carried out to form a cured substrate block. Due to the fact that in the curing forming process, the rawmaterials close to a heat source end obtain more heat, the temperature is higher, heating is more sufficient, the hot-melt fibers are more sufficiently melted, and under the simultaneously-generatedcompression of the pressing block, the raw materials are more easily compressed, raw material particles are tighter relatively, connection is more sufficient, the density is higher relatively, and thewater holding pore ratio is more relatively.
Owner:INST OF URBAN AGRI CHINESE ACADEMY OF AGRI SCI

Microcapsule containing active substance and preparation method thereof

The invention relates to a microcapsule containing an active substance and a preparation method thereof, in particular to a multilayer microcapsule containing an embedded active substance and a preparation method of the multilayer microcapsule. According to the application, the microcapsule particles are prepared by a method of combining extrusion rolling core making (or centrifugal granulation core making) with fluidized spray coating; the preparation method comprises the following steps: firstly, preparing a primary pellet core by adopting an extrusion spheronization granulation method or a centrifugal granulation method, and then uniformly fluidizing a water-blocking coating layer material and a hydrophilic coating layer material to the surface of the pellet core. The prepared microcapsule particles are safe, free of toxic and side effects, small in particle size, rich in active substances and good in stability under the normal temperature condition, and have a slow release effect.
Owner:INNER MONGOLIA MENGNIU DAIRY IND (GRP) CO LTD

Method for continuous and stable preparation of lithium battery high nickel ternary precursor material

InactiveCN108493407AAchieving a porous structureGreenCell electrodesLi-accumulatorsContinuous measurementDischarge rate
Belonging to the technical field of ternary battery preparation, the invention in particular relates to a method for continuous and stable preparation of a lithium battery high nickel ternary precursor. The method for continuous and stable preparation of a lithium battery high nickel ternary precursor provided by the invention carries out stepwise sinking in a high-speed rotating settling chamber,controls the composition of a synthetic precursor by continuous measurement, and sets different rotation rates in each layer of settling chamber so as to ensure the uniformity of settling particle size at each layer, utilizes high-speed rotation to realize spheroidization and controllable particle size of the high nickel ternary material, further realizes coating of low nickel with high nickel continuously, solves the defect of difficult control of the coating process at present, realizes continuous, stable and controllable preparation of high nickel precursor. The finally obtained ternary precursor has the characteristics of uniform particle size distribution, compact particles and high tap density, finally can be sintered and then applied to lithium ion batteries, and under the condition of 0.1C discharge rate, the discharge capacity is up to 296 mAh / g, and the capacity still remains at about 256 mAh / g after 200 cycles.
Owner:CHENDU NEW KELI CHEM SCI CO LTD

Copper salt alkalescent electroplating solution for PCB hole metallization and application of copper salt alkalescent electroplating solution

PendingCN112941575AReduce the total concentrationStrong dispersion abilityPrinted element electric connection formationChemistryCopper salt
The invention discloses a copper salt alkalescent electroplating solution for PCB hole metallization and application of the copper salt alkalescent electroplating solution. The pH is 8-10, the copper salt alkalescent electroplating solution is composed of copper salt, a main coordination agent, an auxiliary coordination agent, a pH buffer agent, a uniform plating agent and an induction activator, the mass concentration of the copper salt is 5-20 g / L, and the uniform plating agent is composed of a selenium compound and a salt compound. The induction activator is composed of a cuprous reduction accelerator and a polyalcohol compound. The copper salt alkalescent electroplating solution is stable, low in total concentration of the solution and high in dispersing capacity; and the current efficiency is high, under the specified electroplating condition, obtained copper layer particles are fine and compact, the dispersion capacity value (TP) is high, and electroplating uniform thickening of PCB through holes can be achieved.
Owner:XIAMEN UNIV

Fluotitanate conversion fluid applied to surface of 6061 aluminum alloy and use method of fluotitanate conversion fluid

The invention belongs to the technical field of metal material surface treatment technology, and particularly relates to a fluotitanate conversion fluid applied to the surface of a 6061 aluminum alloy and a use method of the fluotitanate conversion fluid. Each liter of the conversion fluid comprises raw material by weight as follows: 3 g of sodium fluoride, 4 g of ammonium fluorosilicate, 1.0 g of sodium hexametaphosphate, 1.5 g of titanium salt, 1.5 mg of hydrogen peroxide and the balance of water, wherein titanium salt is one of tetra-n-butyl titanate, titanium sulfate, titanyl sulfate and titanium chloride. Etched aluminum ions on the surface of the 6061 aluminum alloy participate in generation of a fluotitanate conversion coating at the normal temperature, so that particles on the coating are fine and compact, and the conversion coating is firmly combined with an aluminum alloy substrate and has characteristics of good corrosion resistance and high adhesive force when attached to an organic coating, and has the advantages of energy conservation, time saving, high production efficiency, low cost, simple process and stable performance.
Owner:XINXIANG UNIV

Preparation method of medical composite glass fiber strontium containing enhanced bone cement product

Calcium nitrate, diammonium phosphate and urea are mixed and added with strontium phosphate to be mixed, stirred and heated, to prepare strontium containing hydroxyapatite; the hydroxyapatite is added into magnesium chloride and magnesium oxide, added with water to be dissolved, to prepare magnesium oxychloride adhesive; a hand lay-up bone pre-fabricated piece is paved with pulp and glass fiber cloth, flattened, paved uniformly and brushed with glue; and then the prefabricated outer skin is paved and compacted, the seam is sealed by plastic thin film, cured and stripped; the product is trimmed within one day after stripping, and a medical composite glass fiber strontium containing enhanced bone cement product is prepared. The composite material prepared by the invention has the advantages of uniform glass fiber dispersion and good combination of the strontium containing hydroxyapatite and a matrix interface, and biomedical composite material with very good application prospect.
Owner:李胜

Renewable green biomass fuel

The invention discloses renewable green biomass fuel. The biomass fuel is prepared from, by weight, 30-50 parts of wood processing residua, 5-18 parts of crop straw, 2-7 parts of bentonite compounds, 2-4 parts of methyl alcohol, 2-8 parts of isobutanol, 1-2 parts of ammonium nitrate, 1-2 parts of nonionic surfactant and 1-3 parts of fuel additive. The bentonite compounds are prepared as the following process: mixing and stirring bentonite and water, adopting a sulfuric acid solution to adjust pH value of the system to 3.4-4, adding a poly(diallyldimethylammonium chloride), stirring, filtering and cleaning the mixture, adding potassium carbonate and water, continuing to stir, filter and clean the mixture, drying the mixture to constant weight, grinding the dried mixture, adding and evenly blending soy protein and water, adding and evenly stirring sodium hydroxide at room temperature, adding maleic anhydride and then raising temperature and stirring the final mixture to obtain the bentonite compounds.
Owner:铜陵启汇新型能源有限公司

Energy-saving and environment-friendly biomass fuel and preparation method thereof

The invention discloses an energy-saving and environment-friendly biomass fuel and a preparation method thereof, and relates to the technical field of biomass fuels. The problem of environmental pollution is solved. The biomass fuel comprises,s by weight, 80 parts of forestry and agricultural residues, 45 parts of animal waste, 35 parts of coal slime, 7 parts of a combustion improver, 5 parts of a desulfurizer, 6 parts of a denitrification agent, 4 parts of a dechlorinating agent and 8 parts of high clay. The preparation method of the biomass fuel comprises the following steps: taking the forestry and agricultural residues, the animal waste and the coal slime as raw materials, and naturally airing until the moisture content is 8-12%; taking and sequentially crushing the aired agricultural and forestry waste, animal waste and coal slime until the particle size is smaller than or equal to 2 mm; and taking the crushed agricultural and forestry waste and animal waste according to the component proportion. The sulfur content, the nitrogen content and the chlorine content of the fuel are effectively reduced, release of harmful substances such as nitrogen dioxide and carbon dioxide is reduced, potassium ions and chloride ions are removed, pollution to the environment is prevented, and energy conservation and environmental protection are achieved.
Owner:曾淑云
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