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64results about How to "Achieve superhydrophobic effect" patented technology

Method for preparing good-stability super-hydrophobic fabrics

The invention discloses a method for preparing good-stability super-hydrophobic fabrics, which comprises the following steps: dispersing organosilane polymers into an organic solvent so as to obtain 2-50 mg / mL of an organosilane polymer solution; coating the organosilane polymer solution on the surface of a fabric in a dip-coating or spray-coating mode; and carrying out curing processing on the fabric in an ultrasonic and / or heat treatment mode so as to obtain a super-hydrophobic fabric. The super-hydrophobic fabric prepared by using the method disclosed by the invention is excellent in super-hydrophobicity and hydrophobic stability, and keeps the natural mechanical properties and luster and the like of fabrics, therefore, the fabric has wide application in the fields of self-cleaning fibers and fabrics. In addition, the method disclosed by the invention is simple in preparation process, mild in reaction conditions, low in cost, and convenient for mass production.
Owner:LANZHOU INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Making method of single-face-super-hydrophobic and single-face-hydrophilic Janus-type fabric

The invention relates to a making method of a fabric, in particular to a making method of a single-face-super-hydrophobic and single-face-hydrophilic Janus-type fabric and belongs to the field of textile function arrangement. The method comprises the following steps that 1, the fabric is cleaned and then dried for use; 2, the single face of the fabric is protected, under the condition of constantoxygen pressure intensity, plasma glow discharge treatment is conducted on the single face of the fabric, after oxygen is switched off, under the condition of constant steam pressure intensity of a grafting monomer, plasma glow discharge treatment is conducted again, and the single-face-super-hydrophobic and single-face-hydrophilic Janus-type fabric is obtained. According to plasma glow dischargetreatment, a cold plasma treatment instrument is used for generating plasma glow, the plasma treatment power is within 30-120 W, and the time is within 1-10 min. According to the method, the technology is simple and easy to control, the method is suitable for single-face treatment of various cotton fabrics and acetate fiber non-woven fabrics, the functionality demand is met, and the method also has good wearing performance.
Owner:ZHEJIANG SCI-TECH UNIV

Preparation method and application of super-hydrophobic antibacterial finishing agent for cotton fabrics

InactiveCN104131468AAchieve superhydrophobic effectExcellent antibacterial and anti-mildew functionVegetal fibresPolymer scienceOrganosolv
The invention relates to a super-hydrophobic antibacterial finishing agent for cotton fabrics. The super-hydrophobic antibacterial finishing agent comprises following components: long-chain alkyl alkoxy siloxane, nano zinc oxide and silane behenyl trimethyl ammonium chloride used as an emulsifier antibacterial agent. Long-chain alkyl alkoxy siloxane and nano zinc oxide are used as super-hydrophobic raw materials and silane behenyl trimethyl ammonium chloride is used as the emulsifier antibacterial agent to prepare the super-hydrophobic antibacterial finishing agent for fabrics, particularly the cotton fabrics; water is used as a dispersion medium so that the disadvantage of existing patented technologies at home and abroad that an organic solvent is taken as a carrier to prepare the super-hydrophobic fabrics is overcome; the contact angle between the cotton fabrics treated by the super-hydrophobic antibacterial finishing agent and water drops is larger than 150 degrees and the super-hydrophobic effect of a lotus leaf is realized; the water drops roll on the surfaces of the cotton fabrics and are not absorbed by the cotton fabrics for long time; meanwhile, the super-hydrophobic antibacterial finishing agent has good antibacterial and mould-proof functions.
Owner:NANXIONG DING CHENG NEW MATERIAL TECH CO LTD

Strawberry-shaped super-hydrophobic composite microsphere and application thereof

The invention relates to a strawberry-shaped super-hydrophobic composite microsphere and application thereof. The microsphere is prepared through the following steps that (1) an amino polystyrene microsphere, ethyl alcohol, ethyl orthosilicate and distilled water are added into a reactor, and take a reaction for 24h at room temperature; the product is washed with ethyl alcohol; after vacuum drying is performed, a strawberry-shaped composite microsphere is obtained; (2) the strawberry-shaped composite microsphere, a solvent and a silane coupling agent are added into the reactor; the reaction is performed for 5 to 15h under the condition of 25 DEG C to 100 DEG C; the product is centrifuged to obtain the strawberry-shaped super-hydrophobic composite microsphere. The strawberry-shaped super-hydrophobic composite microsphere and epoxy resin are matched to be used as a super-hydrophobic coating; the excellent and stable super-hydrophobic performance is realized; muddy water is splashed on the prepared super-hydrophobic surface; the super-hydrophobic surface cannot be polluted by the muddy water, so that the self cleaning function of the surface is realized.
Owner:天津傲卓菲科技有限公司

Preparation method for fluoride-free super-hydrophobic cotton fabric

The invention discloses a preparation method for a fluoride-free super-hydrophobic cotton fabric, and belongs to the field of textile function finishing and processing. The preparation method comprises the steps that rolling-drying-baking finishing is performed on a cotton fabric by adopting nano titanium dioxide sol to improve the roughness of the surface of the fabric, and then hydrophobic modification is performed on the fabric by adopting a low-surface-energy substance-molten wax substance; the contact angle of the prepared cotton fabric and a water drop is larger than 150 degrees. According to the method, through a chemical reaction between hydroxyl of cotton fiber and hydroxyl in the nano TiO2 hydrosol, the constructed rough surface has the good firmness; through the structural characteristics of the bionic lotus leaf surface, the molten wax substance is adopted to be cured and crystallized on the rough surface of an oxide for organic modification, not only can the super-hydrophobic effect can achieved, but also the influences of introducing a fluorine-containing organic modifier and other organic solvent or a surfactant on the hydrophobicity of the fabric can be avoided, and therefore the super hydrophobicity of the prepared fabric has the excellent stability.
Owner:ZHONGYUAN ENGINEERING COLLEGE

Fluorine-free super-hydrophobic Zn-MOF composite coating on surface of magnesium alloy and preparation method thereof

The invention discloses a fluorine-free super-hydrophobic Zn-MOF composite coating on the surface of a magnesium alloy and a preparation method thereof. The fluoride-free super-hydrophobic Zn-MOF composite coating on the surface of the magnesium alloy specifically comprises a micro-arc oxidation layer, a Zn-MOF layer and a stearic acid layer which are sequentially attached to the surface of the magnesium alloy. A magnesium alloy matrix is sequentially subjected to grinding and polishing, oil removal and ultrasonic cleaning, then micro-arc oxidation treatment is carried out, after a micro-arc oxidation film is formed on the surface of the magnesium alloy matrix, the micro-arc oxidation film is placed in a polytetrafluoroethylene reaction kettle for high-temperature and high-pressure reaction to form the Zn-MOF coating, and finally the Zn-MOF coating is treated with a low-surface-energy substance stearic acid, and the fluorine-free super-hydrophobic Zn-MOF composite coating on the surface of the magnesium alloy is obtained after drying. The method is simple in preparation process and free of fluorine, the composite coating and a magnesium alloy base material have good binding force,the composite coating can be evenly distributed on the surface of the magnesium alloy, the corrosion current density is low, the super-hydrophobic effect is achieved, and good corrosion resistance isshown.
Owner:GUILIN UNIVERSITY OF TECHNOLOGY

Boron-doped diamond film and preparation method thereof, oil-water separation element, water treatment electrode and preparation method thereof and water treatment device

The invention provides a boron-doped diamond film and a preparation method thereof, an oil-water separation element, a water treatment electrode and a preparation method thereof and a water treatmentdevice, and relates to the technical field of diamond films. The boron-doped diamond film comprise a boron-doped diamond micrometer layer and a boron-doped diamond nanometer layer; the surface of theboron-doped diamond micrometer layer is provided with convex micrometer particles; the boron-doped diamond nanometer layer is formed on the surface of the boron-doped diamond micrometer layer, and thesurface of the boron-doped diamond nanometer layer is provided with nanometer particles; and the boron-doped diamond micrometer layer and the boron-doped diamond nanometer layer form a lotus leaf-like multilevel micro-nano structure. The boron-doped diamond film has the lotus leaf-like multilevel micro-nano structure, a bionic superhydrophobic surface is formed, the filtering function and the electrocatalytic water purification function are taken into account concurrently, and a foundation is laid for development of a new-generation field living water supply system.
Owner:SHENZHEN INST OF ADVANCED TECH

Superhydrophobic coating and preparation method thereof

The invention belongs to the field of material surface and inorganic porous material and specifically relates to a superhydrophobic coating and its preparation method. The preparation method comprises the following steps: a, adding 1-5 parts by weight of natural zeolite into 50-100 parts by weight of ethanol, carrying out ultrasonic dispersion for 10-30 min, adding 0.15-0.85 part by weight of perfluorodecyltrichlorosilane, and continuously carrying out ultrasonic dispersion for 10-30 min to obtain a dispersion liquid; b, immersing a base material into the dispersion liquid obtained in the step a for 3-5 min, taking out the base material and drying the base material at 50-70 DEG C for more than 30 min; and c, repeating the step b for two to three times so as to form the superhydrophobic coating on the surface of the base material. Natural zeolite belongs to an inorganic porous material and is easy to form a micro-nano structure in the coating. Meanwhile, there exist many hydroxide radicals on the surface of zeolite, and its surface energy is reduced after condensation between perfluorodecyltrichlorosilane and hydroxide radicals. Thus, the superhydrophobic effect is achieved. The natural zeolite is cheap and easily available. The preparation method is simple and easy for industrialization. The coating of the invention has a self-cleaning ability, is applicable to many base materials and is widely applied.
Owner:HUBEI UNIV

Method for modifying microporous membrane wettability by utilizing low pressure-forced Cassie state effect

The invention discloses a method for modifying microporous membrane wettability by utilizing a low pressure-forced Cassie state effect. The method comprises the step of: inducing a liquid drop on a microporous membrane with the aperture of 10-100 mu m to be changed from a Wenzel state to a Cassie state at the room temperature by utilizing relative pressure of 100-300 Pa, so as to modify interfacial wettability property of the microporous membrane. Before the implementation of the above-mentioned step, preferably, surface finish is performed on the microporous membrane by adopting a surface modification technology. Under a same micropore structure, the larger the contact angle of the liquid drop on the surface of the modified microporous membrane is, the smaller the critical pressure of the forced Cassie state of the microporous membrane is. The invention provides a novel approach for designing a superhydrophobic surface. Compared with the common superhydrophobic surface, the microporous membrane has the advantages of reducing the degree of dependence on a low surface energy substance and a surface micro-nano fine structure, and decreasing the probability of failure of the surface superhydrophobic function when external pressure and the surface fine structure are damaged, therefore wide application prospect is obtained.
Owner:NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI

Hydrophobic bamboo wood with surface being loaded with oxidized graphene and silicon dioxide and production technology thereof

The invention discloses a production technology of hydrophobic bamboo wood with the surface being loaded with oxidized graphene and silicon dioxide, and relates to the technical field of composite materials. The production technology includes the following steps that S1, absolute ethyl alcohol, deionized water and ammonia water are collected to be poured into a beaker for stirring, so that a soak solution is prepared, and TEOS is added into the soak solution to obtain colloid; S2, the bamboo wood loaded with the oxidized graphene and the colloid in the step S1 are transferred into a reaction still to carry out a hydrothermal reaction; S3, after the hydrothermal reaction is completed, a bamboo block is taken out and cleaned with the deionized water, and then the bamboo block is put into a vacuum drying oven to be dried; S4, heptadecafluorodecyl trimethoxy-silane and methyl alcohol are mixed to be evenly stirred, so that mixed liquor is formed; S5, the bamboo block dried in the step S3 is put into the mixed liquor of the step S4 to be stirred; and S6, after stirring is completed, the bamboo block is taken out and is washed with the methyl alcohol, and then the bamboo block is put into the vacuum drying oven to be dried so that a product can be prepared. By the adoption of the production technology, the technical problem that bamboo wood prepared in the prior art cannot meet the hydrophobic requirement is solved.
Owner:ZHEJIANG FORESTRY ACAD

A preparation method and product of a superhydrophobic polymer composite coating containing nanoparticles

The invention discloses a method for preparing a super hydrophobic polymer composite coating containing nano particles. The method comprises the following steps: firstly, mixing a coupling agent with a hydrolysis promoter and deionized water to carry out hydrolysis at normal temperature; adding the nano particles, reacting at 50-100 DEG C for 0.25-5 hours under magnetic agitation, so as to obtain modified nano particle powder by post-treatment; sieving the modified nano particle powder, and mixing with a fluorine-containing polymer emulsion; and evenly agitating after diluting by a diluent, coating on a metal substrate, and cooling to room temperature after high-temperature solidification and annealing treatment. The invention proposes a simple method for preparing the super hydrophobic polymer composite coating containing the nano particles. The nano particles are modified by the coupling agent, meanwhile, the adjusting process of pH in the hydrophobic treating process of the nano particles is removed, the modified nano particles are added to the polymer composite coating, and the stable target is achieved by interaction of bonding of a nano particle-coupling agent and a fluorine-containing polymer molecular chain.
Owner:中国人民武装警察部队杭州士官学校

Diamond thin film of multi-level micro-nano structure and preparation method and application thereof

The invention discloses a diamond thin film of a multi-level micro-nano structure and a preparation method and application thereof and relates to the technical field of diamond thin films. The diamondthin film comprises a discontinued micron-sized diamond island which is formed from the surface of a substrate to the exterior in sequence and the multi-level micro-nano structure which is similar tothe mastoid process of the lotus leaf and is formed by a nano diamond film layer composed of continuous nano-sized diamond grains. The preparation method of the diamond thin film comprises the following steps that first, low-density crystal implantation is performed on the substrate, and primary growth of diamond is performed through a heat wire chemical vapor deposition method; and then, high-density crystal implantation is performed on the primary growth diamond thin film, and secondary growth of diamond is performed through the heat wire chemical vapor deposition method. The diamond thin film is of the multi-level micro-nano structure similar to the mastoid process of the lotus leaf, forms a bionic super-hydrophobic surface, and is high in hydrophobicity and self-cleaning capacity, resistant to corrosion and long in service life. The preparation method is easy to implement, high in applicability and suitable for industrial production and has a simple and stable process.
Owner:SHENZHEN INST OF ADVANCED TECH

Super-hydrophobic modification method of nanocellulose

InactiveCN113773404ALoose structureReinforced hydrophobic long chainsUltrasonic oscillationCarboxylic group
The invention relates to super-hydrophobic modification of nanocellulose, and provides a super-hydrophobic modification method of nanocellulose. The method comprises the following steps: preparing nanocellulose with different carboxyl contents by utilizing a method of combining a TEMPO / NaClO / NaBr oxidation system and ultrasonic oscillation, and selecting octadecylamine with low surface energy as a hydrophobic modifier, wherein a hydrophobic long chain can be grafted on the surface of the nanocellulose by carboxyl in the nanocellulose and amino in the octadecylamine through complexation reaction; and selecting an adhesive substance polydopamine, and coating the surface of the modified nanofiber with the selected substrate, so that not only can an octadecylamine long chain grafted with the nanocellulose be protected, but also free octadecylamine in a system can be adsorbed on the surface of the nanocellulose. The prepared hydrophobic nano cellulose film is applied to the fields of oil-water separation, waterproof films and the like.
Owner:TIANJIN UNIVERSITY OF SCIENCE AND TECHNOLOGY

Electrolyte for realizing blackening of magnesium alloy surface and blackening process method

The invention provides an electrolyte for realizing blackening of a magnesium alloy surface and a blackening process method. A coloring solution of a silicic acid system is adopted, and the coloring solution comprises additives such as ferric ammonium citrate and the like. In the coloring process, a magnesium alloy is subjected to down-current two-step constant-current micro-arc oxidation treatment in a prepared micro-arc oxidation solution to prepare a black ceramic membrane. In order to further improve the corrosion resistance and the stability of a membrane layer, hole sealing treatment iscarried out in hole sealing liquid. The coloring micro-arc oxidation solution is safe, environmentally friendly and high in stability, by optimizing a micro-arc oxidation manner, positive and negativecurrent density parameters are adjusted, self-repairing hole sealing is carried out on the interior of the membrane layer, the problems that the surface is loose and porous, and the thickness of a compact inner layer is small are solved, membrane layer compactness control is achieved, the membrane layer is thicker and more compact, finally the hole sealing liquid is good in stability, the influence on the color of the membrane layer does not exist, and the corrosion resistance is improved. By means of the technology, blackening treatment of the magnesium alloy is achieved, and the applicationfield of the magnesium alloy is broadened.
Owner:CHANGZHOU UNIV

Super-hydrophobic heat-resistant coating for aluminum alloy and preparation method of super-hydrophobic heat-resistant coating

The invention discloses a super-hydrophobic heat-resistant coating for an aluminum alloy and a preparation method of the super-hydrophobic heat-resistant coating, and relates to the technical field of coatings. The heat-resistant coating is formed on the surface of the aluminum alloy through the spraying pretreatment process and the second-time spraying treatment in sequence, the heat-resistant coating and the aluminum alloy form a firm cross-linked interpenetrating network structure, the heat resistance of the coating is improved, and the phenomenon that the service life of the aluminum alloy is shortened in a high-temperature environment is reduced; and then third spraying treatment is conducted, a corrosion inhibitor serves as an inner core solution, stearic acid serves as a shell solution, a super-hydrophobic coating is formed through coaxial electrostatic spraying, the corrosion inhibitor is prepared from isoquinocarboxylic acid, dipropylene triamine and p-methoxyphenyl thiourea, the surface of the aluminum alloy is isolated from an environment medium, and corrosion of an acid medium and chloride ions is inhibited. The prepared super-hydrophobic heat-resistant coating for the aluminum alloy has the heat-resistant, super-hydrophobic and corrosion-resistant effects.
Owner:严平

A kind of hydrophobic bamboo with graphene oxide and silicon dioxide on its surface and its production process

The invention discloses a production technology of hydrophobic bamboo wood with the surface being loaded with oxidized graphene and silicon dioxide, and relates to the technical field of composite materials. The production technology includes the following steps that S1, absolute ethyl alcohol, deionized water and ammonia water are collected to be poured into a beaker for stirring, so that a soak solution is prepared, and TEOS is added into the soak solution to obtain colloid; S2, the bamboo wood loaded with the oxidized graphene and the colloid in the step S1 are transferred into a reaction still to carry out a hydrothermal reaction; S3, after the hydrothermal reaction is completed, a bamboo block is taken out and cleaned with the deionized water, and then the bamboo block is put into a vacuum drying oven to be dried; S4, heptadecafluorodecyl trimethoxy-silane and methyl alcohol are mixed to be evenly stirred, so that mixed liquor is formed; S5, the bamboo block dried in the step S3 is put into the mixed liquor of the step S4 to be stirred; and S6, after stirring is completed, the bamboo block is taken out and is washed with the methyl alcohol, and then the bamboo block is put into the vacuum drying oven to be dried so that a product can be prepared. By the adoption of the production technology, the technical problem that bamboo wood prepared in the prior art cannot meet the hydrophobic requirement is solved.
Owner:ZHEJIANG FORESTRY ACAD

Preparation method of super-hydrophobic anticorrosive self-assembled three-dimensional nano material

The invention discloses a preparation method of a super-hydrophobic anticorrosive self-assembled three-dimensional nano material. The method comprises the following steps: firstly, preparing dahlia-like carbon nanohorns by adopting an electric arc discharge method, and performing transient oxidation treatment on the carbon nanohorns to obtain an open-cell carbon nanohorn material; and fully mixingnano zinc ethanol slurry and the carbon nanohorn material, and performing self-assembly compounding on the carbon nanohorns and nano zinc by adopting a supercritical fluid method to form the three-dimensional pearl mussel-like structural material. According to the preparation method provided by the invention, the carbon nanohorn-nano zinc composite material prepared by adopting the method has a simple process, synergy of a super-hydrophobic structure of the carbon nanohorns and corrosion resistance of the nano zinc in the coating system can physically block a reaction of a metal surface withan active medium, and effectively protect elemental zinc against corrosion by a liquid and oxidation by the air, thereby greatly improving a zinc utilization rate and corrosion resistant efficiency; and the composite material can be widely used in the fields of architectural coatings and industrial anticorrosive coatings to improve compactness, barrier properties, mechanical properties and corrosion resistance of films.
Owner:上海利物盛纳米科技有限公司

A kind of photocuring coating, ultraviolet light curing hydrophobic anti-adhesion film surface and preparation method thereof

The invention provides a light-cured coating, an ultraviolet light-cured hydrophobic anti-adhesion film surface and a preparation method thereof. The light-cured coating comprises the following components in parts by weight: 15-30 parts of polyurethane acrylate, 10-30 parts of nano Particles, 2-4 parts of photoinitiator, 1-15 parts of perfluoropolyether, 5-15 parts of perfluoro-modified long-chain alkylsilane and 30-50 parts of solvent. The invention uses polyurethane acrylate, perfluoropolyether and perfluoromodified long-chain alkyl silane to compound nanoparticles, so that the photocurable coating is crosslinked through photocuring reaction to form a tight coating, which has wear resistance and forms a cured coating. The super-hydrophobic microstructure of the substance enhances its hydrophobicity. Through the microstructure formation and ultraviolet curing methods, a concave-convex microstructure is produced on the surface of the prepared film, which produces a lotus leaf effect, enhances hydrophobicity, and achieves superhydrophobicity. Production Afterwards, it can be rolled directly without the need for a protective film, saving costs.
Owner:ZHANGJIAGANG KANGDE XIN OPTRONICS MATERIAL
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