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130results about How to "Porous structure" patented technology

Method for preparing superabsorbent polymer

ActiveUS20180037686A1Excellent gel strengthHigh absorption rateSuperabsorbent polymerWater soluble
The present invention provides a method for preparing a superabsorbent polymer, the method comprising the steps of: forming a function gel polymer by cross-linked polymerization of a monomer mixture under the presence of an internal cross-linking agent, the monomer mixture including a water-soluble ethylene-based unsaturated monomer having an acid group at least part of which is neutralized, a carbonate, a volatile organic solvent, a surfactant, and a bubble promoting agent; forming a base resin powder by drying, grinding, and classifying the function gel polymer; and forming a surface cross-linked layer by additional cross-linking of the surface of the base resin powder under the presence of a surface cross-linking agent. The method for preparing a superabsorbent polymer may provide a superabsorbent polymer which has a porous structure, thereby exhibiting an excellent absorption rate while exhibiting excellent gel strength. Such a superabsorbent polymer may have excellent physical properties such as water retention capacity, absorbency under pressure, and flowage.
Owner:LG CHEM LTD

Preparation method of novel high-selectivity positively-charged nanofiltration composite membrane

The invention discloses a preparation method of a novel high-selectivity positively-charged nanofiltration composite membrane. The preparation method comprises the following steps: taking positively-charged polyethylenimine as a functional layer material of the composite membrane, taking aromatic polybasic acid as a crosslinking agent and modifying, and coating and crosslinking on a nanofiltrationmembrane supporting layer to obtain the high-selectivity positively-charged nanofiltration membrane. By adopting a gradient crosslinking technology, the pore diameter of a prepared composite membranecrosslinking layer is gradually increased from bottom to top; and the water flux is greatly improved under the condition of keeping high desalting performance. The preparation method disclosed by theinvention is simple in technology and easy to operate; and the prepared composite membrane can be operated under a low-pressure condition, so that the cost is reduced and the composite membrane is easy to popularize and apply. The nanofiltration membrane prepared by the preparation method has relatively high selectivity on multivalent cations and monovalent cations and can be used for the fieldsincluding water softening, medicines, dyestuffs, lithium extraction of salt lakes, industrial wastewater and the like.
Owner:ZHEJIANG UNIV OF TECH

Preparation method of membrane adsorbent for removing ammonia nitrogen in wastewater

The invention provides a preparation method of a membrane adsorbent for removing ammonia nitrogen in wastewater. The preparation method comprises the following steps: treating modified pure water sludge; adding polyvinylpyrrolidone into a tapered bottle containing dimethyl acetamide; adding polyvinylidene fluoride after uniformly stirring; re-adding pure water sludge after dissolution; after fully stirring, sealing the bottle mouth and leaving the mixture to stand for defoaming to prepare a casting solution, wherein the addition of polyvinylpyrrolidone accounts for 2-4% of the mass of the casting solution, the total mass of polyvinylidene fluoride and sludge particles accounts for 17-20% of the mass of the casting solution, the mass ratio of polyvinylidene fluoride to the sludge particles is (3:7)-(7:3), and the rest is dimethyl acetamide; striking the casting solution on a glass plate to manufacture a flat sheet membrane; then placing the flat sheet membrane in a pure water precipitating bath; soaking in deionized water after film forming, and then taking out; placing the membrane in anhydrous ethyl alcohol to be soaked; taking out the membrane; naturally cooling to obtain the membrane adsorbent. The membrane adsorbent can absorb ammonia nitrogen in water and is renewable.
Owner:SUZHOU UNIV OF SCI & TECH

Multifunctional pesticide fertilizer and production method thereof

The invention relates to a multifunctional pesticide fertilizer and a production method thereof. The raw materials of the multifunctional pesticide fertilizer comprise 0.1-9 parts by weight of a pesticide, 20-60 parts by weight of a macro-element fertilizer, 0.5-4 parts by weight of a trace element fertilizer, 5-15 parts by weight of an acrylamide or starch graft, and 10-20 parts by weight of a carrier, wherein the pesticide comprises at least one of avermectin and polyoxin; the macro-element fertilizer comprises at least one of a nitrogen fertilizer, a phosphorus fertilizer and a potassium fertilizer; the trace element fertilizer comprises at least one of zinc and molybdenum; the carrier is an ore waste residue or a boron sludge; and the multifunctional pesticide fertilizer is prepared through mixing and granulating the raw materials. The pesticide fertilizer production method has the advantages of simple technology, low production cost, water utilization rate increase, and guarantee of the drug effects of the pesticide and the fertilizer efficiencies of the above fertilizers.
Owner:锦州硕丰农药集团有限公司

Lucid ganoderma fruit chiffon cake and preparation method of lucid ganoderma fruit chiffon cake

The invention provides lucid ganoderma fruit chiffon cake, which comprises lucid ganoderma fruit. The invention also provides a preparation method of the cake. According to the preparation method of the cake, lucid ganoderma fruit powder is added on the basis of chiffon cake, the original nutrition ingredients of the lucid ganoderma fruit are maintained, the nutrition value and the health care function of the cake are improved, in addition, good mouth feeling, flavor and tissue structures of the chiffon cake are ensured, meanwhile, the bitter taste and the astringent taste caused by lucid ganoderma are completely shielded by the flavor of the chiffon cake through an optimized recipe.
Owner:JIANGSU POLYTECHNIC COLLEGE OF AGRI & FORESTRY

Preparation method for core-shell perovskite-type catalyst for preparing methanol through methane

The invention relates to a preparation method for a core-shell perovskite-type catalyst for preparing methanol through methane. The general formula of the core-shell perovskite-type catalyst is Fe2O3@A(1-m)A'mB(1-n)B'nO3. The preparation method for the core-shell perovskite-type catalyst comprises the following steps: adding nano-sized or micron-sized Fe2O3 into ethanol; dispersing under the effect of ultrasonic waves; removing the supernatant after complete precipitation; using ultrasonic waves to disperse Fe2O3 into deionized water to obtain a Fe2O3 suspension; adding soluble salts corresponding to A, A', B and B' to deionized water; stirring to allow the soluble salts to dissolve completely; adding a complexing agent; after heating and stirring for complexing, adding to the Fe2O3 suspension; stirring evenly; adding glycol; after thorough stirring, evaporating to obtain a colloidal mixture; drying and roasting to obtain the core-shell perovskite-type catalyst. The core-shell perovskite-type catalyst is a perovskite-type oxide catalyst of a core-shell structure; the active constituent, namely Fe2O3 is wrapped in the perovskite oxide, so that the phenomenon that the Fe2O3 is reduced to elementary substance Fe in the catalytic oxidation process, and the activity of the core-shell perovskite-type catalyst declines due to the sintering and accumulation of the Fe, is effectively prevented.
Owner:NORTHEAST GASOLINEEUM UNIV

Method for preparing high-performance silicon-carbon negative electrode composite material of lithium ion battery

The invention discloses a method for preparing a high-performance silicon-carbon negative electrode composite material of a lithium ion battery, and belongs to the technical field of negative electrodes of the lithium ion batteries. The method comprises the following steps of (1) selecting micron silicon powder as a raw material to prepare nano silicon powder; (2) carrying out high-temperature annealing on carbohydrates under the protection of inert gas to obtain an amorphous carbon material; (3) mixing the nano silicon powder obtained in the step (1) with the amorphous carbon material obtained in the step (2) and then adding into a ball mill to carry out ball milling in order to obtain a binary precursor material; and (4) adding the binary precursor material obtained in the step (3) and graphite into the ball mill to be subjected to ball milling again in order to obtain the silicon-carbon negative electrode composite material. The silicon-carbon negative electrode composite material obtained by the invention has a ternary structure, the volume expansion of silicon particles is buffered, and the pulverization of the material in a lithium de-intercalation process is inhibited; and the specific capacity is improved through multiple compact coating layers, and the first coulombic efficiency and the cycling stability are improved.
Owner:BEIJING JIAOTONG UNIV

Piezoelectric device and method for manufacturing the piezoelectric device

A piezoelectric device includes a piezoelectric substrate having a connection pad, a package having an electrode pad, and a connection member to connect the electrode pad to the connection pad, the connection member being a metal member having a plurality of spherical metal particles connected to each other by sintering.
Owner:SEIKO EPSON CORP

Method for preparing titanium-rich material for fluidizing chlorination from high-calcium-magnesium low-grade titanium slag

The invention belongs to the field of metallurgy and chemical engineering and particularly relates to a method for preparing a titanium-rich material for fluidizing chlorination from high-calcium-magnesium low-grade titanium slag. The method for preparing the titanium-rich material for fluidizing chlorination from the high-calcium-magnesium low-grade titanium slag comprises the following steps that (1) the titanium slag is dried and sieved; (2) a high-temperature strong oxidation reaction is conducted on titanium concentrate under the temperature of 950-1000 DEG C; (3) then a weak reduction reaction is conducted under the temperature of 800-850 DEG C; (4) hydrochloric acid is added, and pressure leaching is conducted under heating rotation conditions; and (5) solids and liquids are separated, and the titanium-rich material finished product is obtained through washing and drying. Through the method, the titanium slag similar to Panzhihua high-calcium-magnesium low-grade titanium slag can be treated successfully, thereby being updated for preparing high-quality titanium-rich raw materials meeting the needs of fluidizing chlorination, and significance is achieved for utilizing complextitanium resources of the west of Panzhihua and for developing titanium chloride dioxide.
Owner:PANZHIHUA IRON & STEEL RES INST OF PANGANG GROUP +1

Positive electrode for nonaqueous electrolyte secondary battery, and nonaqueous electrolyte secondary battery

InactiveUS20170244096A1Promote reactionReaction surface of be increaseFinal product manufactureSecondary cellsPore diameterElectrolyte
A positive electrode for a nonaqueous electrolyte secondary battery according to the present invention is provided with a porous positive electrode active material layer that contains a positive electrode active material. The positive electrode active material layer is formed so that a logarithmic differential pore volume distribution curve thereof, which shows the relation between pore diameter and pore volume of pores in the positive electrode active material layer, is a single-peak type curve. The distribution curve has a main peak having a full width at half maximum of from 0.001 μm to 0.05 μm inclusive, and the sum of the pore volumes of the pores within a pore diameter range corresponding to the full width at half maximum is 70% or more of the total pore volume.
Owner:ELIIY POWER

Heavy metal contaminated soil improving coated fertilizer and preparation method thereof

The invention discloses heavy metal contaminated soil improving coated fertilizer and a preparation method thereof. The preparation method includes the steps of 1), preheating fertilizer granules; 2),mixing ammonium magnesium phosphate with grease by blending to obtain coated slurry; 3), evenly spraying the coated slurry to surfaces of the fertilizer granules preheated in the step 1); 4), evenlymixing biochar powder with wormcast powder and coating the mixture on a product to obtain the coated fertilizer after performing cooling and drying. The surface of the fertilizer is coated with a layer of a film-forming material, heavy metals in the active state in soil can be passivated, pollution caused by the heavy metals to the ecosystem is reduced, and fattening release cycle of the fertilizer can be delayed; the prepared coated fertilizer meets requirements of the state for the coating fertilizer, the fertilizer is decomposed gradually under the action of chemical and biological factorsafter applied to the soil, nutrients are released slowly, and requirements of crops in the whole growing period on the nutrients can be met.
Owner:WUHAN POLYTECHNIC UNIVERSITY

Preparation method of small-size abalone shell hydroxyapatite porous microspheres

The invention discloses a preparation method of small-size abalone shell hydroxyapatite porous microspheres. The preparation method comprises the following steps: taking abalone shells as a main raw material, cleaning substances on the surface layers of the abalone shells, conducting naturally drying, crushing and sieving the substances by 200 meshes to obtain abalone shell powder, dissolving abalone shell powder, and then dripping a phosphoric acid solution at a constant speed according to the molar ratio of Ca to P of 1.67 to 1, then adding sodium citrate and a poly aspartic acid template agent, simultaneously adding urea to adjust the pH, and synthesizing uniformly stirred precursor reaction solution into the hydroxyapatite porous microspheres by a hydrothermal method. The preparation method is simple, wide in raw material source, low in cost and easy to popularize.
Owner:SHANDONG UNIV

Processing method of coarse cereal products convenient to compound

The invention relates to a processing method of coarse cereal products convenient to compound, and belongs to the field of grain processing. The products consist of the following raw materials in parts by weight: 60-80 parts of rice and 20-40 parts of precooked coarse cereals, wherein the precooked coarse cereals consist of the following ingredients in parts by weight: 15-20 parts of brown rice, 10-14 parts of oat, 10-14 parts of black rice, 12-15 parts of small red beans, 8-10 parts of mung beans, 10-15 parts of millet, 5-10 parts of corn grits, 3-5 parts of walnuts, 1-3 parts of black sesameseeds and 5-8 parts of red jujubes. The brown rice, the oat, the black rice, the small red beans and the mung beans in the ingredients are processed into the precooked coarse cereals through steps ofimpurity removal, soaking with NaHCO3, screening, microwave noncontinuous type heating and the like. Compared with a traditional technology, the processing method disclosed by the invention is simpler, fewer in operating procedures, shorter in precooking time and lower in energy consumption; and the products are rich in nutrients and convenient and swift, and have the efficacy of nourishing the kidney, boosting essence, nourishing the liver to improve visual acuity, replenishing blood, soothing the nerves, moistening lung for arresting a cough and the like.
Owner:TIANJIN UNIV OF SCI & TECH

Detection method for protein with nucleic acid aptamer target gathering and laser enzymolysis

The invention belongs to the field of chemicobiology and relates to a detection method for protein with nucleic acid aptamer target gathering and laser enzymolysis. Firstly, nanogold with the diameter of 13nm and a target board are in epoxy dripping mode, the anogold is dryed and calcined, and even and thick gold films are formed on the target board. With the method, the gold films which are with a loose hole-type structure are formed on the surface finish of the target board, large specific surface area is provided, excellent stability and biocompatibility are achieved, and the method for protein with nucleic acid aptamer target gathering and laser enzymolysis can be applied to various functionalized modifications. Secondly, nucleic acid aptamers of mercapto modification is fixed on the target board. Thirdly, target protein is gathered and target quick laser enzymolysis is supplemented, and samples are sent to matrix-assisted laser desorption ionization (MALDI)-time-off-flight mass spectrometer (TOFMS) to accept qualitative and quantitative analysis. The whole experiment process is simple, quick, accurate and can be widely applied into high-throughput qualitative and quantitative analysis of important protein.
Owner:FUDAN UNIV

Preparation method and application of a biological composite artificial trachea

The present invention provides a biological composite artificial trachea and its preparation method in combination with 3D printing technology. The material used in the present invention has both flexibility and certain mechanical strength, which meets the physical and mechanical properties of the trachea as a hollow organ in the thoracic cavity; secondly, The artificial trachea of ​​the present invention has a porous and loose structure, which is conducive to the diffusion of nutrients and the growth of autologous blood vessels; in addition, the present invention prints the seed cells obtained from the expansion of the recipient's own airway epithelial cells and chondrocytes in the trachea wall, The patient's rejection of the cells is avoided; moreover, the seed cells are composed of terminally differentiated mature cells, which avoids the problem of inducing differentiation and the risk of tumor formation caused by the use of stem cells; at the same time, the spatial distribution of the cells in the present invention is The printing is precise and controllable, and the distribution according to histological laws accelerates the repair process; finally, the tracheal stent can be degraded in the body, reducing the complications caused by foreign body residues in the body, and avoiding the risk of secondary surgical removal.
Owner:SHANGHAI PULMONARY HOSPITAL +1

Salt-containing oyster powder decontamination antibacterial material and preparation method and use method

The present invention discloses a salt-containing oyster powder decontamination antibacterial material and a preparation method and a use method, the salt-containing oyster powder decontamination antibacterial material is a mixture of oyster shell powder with teh particle diameter of 50mum or less, food grade sodium bicarbonate powder and sodium chloride powder in a weight ratio of 1:0.45-0.55:0.45-0.55; wherein the oyster shell powder has a porous structure, and is high activity powder obtained by calcinations and grinding of oyster shell as a raw material. According to the preparation method, clinker is prepared by three-level stepped heating calcining method to obtain the porous structure and high chemical activity; and the use method of the salt-containing oyster powder decontamination antibacterial material used for removing agricultural pesticide residues is simple, safe and efficient, and free of secondary pollution. Compared with the prior art, the salt-containing oyster powder decontamination antibacterial material has low cost, energy saving, safe and efficient use, green environmental protection and other characteristics, is suitable for all kinds of fruit and vegetable washing treatment, can effectively eliminate residual agricultural chemicals deposited on the surface, and can kill escherichia coli.
Owner:QINGDAO UNIV

Flexible fire-proof and explosion-proof blanket for cable intermediate joint

The invention relates to a flexible fire-proof and explosion-proof blanket for a cable intermediate joint, which comprises a fire-proof heat-insulation outer sheath, a fire-proof heat-insulation inner sheath, and a fire-proof cotton layer, an expandable graphite particle layer, a graphite-based flexible blanket, an explosion-proof fiber layer and a waterproof fiber layer which are clamped between the fire-proof heat-insulation inner sheath and the fire-proof heat-insulation outer sheath and are sequentially laminated, the peripheral edges of the fire-proof heat-insulating outer skin and the fire-proof heat-insulating inner skin are sewn together, a plurality of strapping tapes are sewn on the fire-proof heat-insulating outer skin side by side, and the fire-proof explosion-proof blanket is wrapped at the intermediate joint of the cable through the strapping tapes. The flexible fire-proof and explosion-proof blanket has excellent comprehensive protection performance, especially fire-proof and explosion-proof performance, the intermediate joint of the cable is coated through the strapping tapes in the using process, and the flexible fire-proof and explosion-proof blanket is convenient to use and install and can be repeatedly used.
Owner:XUCHANG SIDA ELECTRIC POWER EQUIP
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