Patents
Literature
Hiro is an intelligent assistant for R&D personnel, combined with Patent DNA, to facilitate innovative research.
Hiro

716results about How to "Not easy to hydrolyze" patented technology

Organosilicone modified acrylate emulsion, preparation method thereof and water-based artificial stone prepared from organosilicone modified acrylate emulsion

The invention provides an organosilicon modified acrylate emulsion with a weight-average molecular weight of 201205 and also provides a preparation method of the organosilicon modified acrylate emulsion and an artificial stone prepared from the organosilicon modified acrylate emulsion. According to the specific technical scheme, the preparation method comprises the following steps of: (1) preparing a siloxane intermediate emulsion; (2) preparing a silicon-acrylic copolymer core emulsion; and (3) preparing a silicon-acrylic copolymer shell emulsion. The molecular structure of the organosilicon modified acrylate emulsion has a special core-shell structure design, wherein an innermost core of a particle is made of an organosilicon component, an intermediate layer of the particle is made of a polyacrylate component and the shell of the particle is made of a multi-crosslinked organosilicon and polyacrylate component. The organosilicon modified acrylate emulsion not only has high organosilicon content, but also has high hardness and adhesive force. Compared with a common product, the organosilicon modified acrylate emulsion has higher emulsion hardness and resistance to soiling and water. The artificial stone prepared from the organosilicon modified acrylate emulsion has the advantages of good compatibility, high abrasion resistance, low water absorption, good heat resistance, high fire resistance and low shrinkage rate in an artificial stone formula.
Owner:广东海顺新材料科技有限公司

Process of preparing biological diesel

This invention relates to the preparation method of the biological diesel fuel. It belongs to the composition of biological fuel and green regenerated energy resource technology area. It adopts the Bronsted acid ion as the catalyst, and the biological diesel fuel can be produced under the temperature is from 20DEG C to 300DEG C, the pressure is from 0.1Mpa to 10Mpa, the mole ratio of biological fat (or fat acid) to short chain alcohol is from 1:30 to 1:1300, the mole ratio of biological fat (or fat acid) to ion catalyst solution is from 300:1 to 1:1. Adopting the Bronsted acid iron catalyst to prepare the biological diesel fuel, the activity of the catalyst is high, the stability of it is good and it can reuse. There is no corrosion to the equipment and the process environment is friendly, and the product can be separated easily. The investment of equipment and cost of operation is low.
Owner:TSINGHUA UNIV

Flame-retardant polyamide composite material and preparation method thereof

The invention discloses a flame-retardant polyamide composite material and a method for preparing the flame-retardant polyamide composite material. The flame-retardant polyamide composite material is characterized by comprising 40-80wt% (weight percent) of polyamide resin, 0-30wt% of reinforcing material, 10-25wt% of flame retardant, 2-4wt% of synergistic flame retardant, 2-5wt% of compatibilizer, 0.5-1wt% of heat stabilizer and 0.5-1wt% of processing aid. The method for preparing the flame-retardant polyamide composite material comprises the following steps: adding the polyamide resin, the reinforcing material, the flame retardant, the synergistic flame retardant, the compatibilizer, the heat stabilizer and the processing aid into a twin-screw extruder, melting, mixing, extruding and granulating. The flame-retardant polyamide composite material disclosed by the invention has stable thermal stability and flame-retardant effect, good comprehensive mechanical performance and processing and forming performance and wider application range and field and can be applied to the fields of automotive industry, electronic industry and furniture industry.
Owner:SHANGHAI KINGFA SCI & TECH +1

Dyeing process of pure cotton fabric

The invention discloses a dyeing process of a pure cotton fabric, which comprises the following steps: a. taking one mass part of pure cotton fabric to be dyed; b. grinding a powdery reactive dye occupying 2-8% of the total mass of the fabric in a ball grinding mill for 2h, adding ethanol and grinding for 1h, wherein the mass of ethanol is nine times of that of the powdery reactive dye; c. adding decamethylcyclopentasiloxane, high-speed cutting for 5min at a rotating speed of 600r/min, and preparing a powdery reactive dye/decamethylcyclopentasiloxane suspension system, wherein the mass of the decamethylcyclopentasiloxane is 50 times of the total mass of the fabric; d. pretreating the pure cotton fabric to be dyed in an alkali solution of 1-130g/L so as to enable the pure cotton fabric tofully swell, and controlling the fabric liquid carrying rate to be 100-220% through a rolling machine; and e. immersing the treated fabric into the powdery reactive dye/decamethylcyclopentasiloxane suspension system, dyeing for 40min at normal temperature, slowly rising the temperature to 70-110 DEG C within 15min, fixing color for 10-60 min at the temperature of 70-110 DEG C, and finally reducing the temperature to the normal temperature to finish dyeing. The dyeing process disclosed by the invention has the advantages of high dyeing fixation rate, environmental-protection and no pollution.
Owner:HAINING GREEN UNIVERSE TEXTILE TECH CO LTD

Ruthenium complex capable of inhibiting tumor angiogenesis and preparation method and application thereof

The invention belongs to the field of chemical drugs, and discloses a ruthenium complex capable of inhibiting tumor angiogenesis and a preparation method and application thereof. The ruthenium complex provided by the invention has a structure shown in a formula I or II. The preparation method comprises the following steps of: dropwise adding a silver nitrate solution to a sodium salt solution, stirring and reacting, then filtering, washing and vacuum drying a precipitate, and thereby obtaining a ligand O-O; taking ruthenium chloride, L, and lithium chloride to be dissolved in N-, N-dimethyl formamide, heating and refluxing under the protection of argon atmosphere to obtain an intermeidate Ru (L2) Cl22 +; allowing the ligand O-O and the Ru (L2) Cl22 + to be dissolved in an ethanol/water mixed solvent, heating and refluxing to obtain the ruthenium complex shown in the formula I; and allowing the Ru (L2) Cl22 +, 8- hydroxyquinoline, and ammonium acetate to be dissolved in ethanol, and heating and refluxing under the protection of argon atmosphere to obtain the ruthenium complex shown in the formula II. The ruthenium complex has the advantages of good stability, uneasiness in hydrolysis, good solubility, low toxicity, and the ability to inhibit tumor angiogenesis, and is easily absorbed by the human body.
Owner:JINAN UNIVERSITY

Polytef double-film composite filtering materials

A dual teflon films combined filtering material is prepared from glass fibers through twisting to become glass fiber yarns, coating teflon film by immersing in teflon solution and baking, weaving to obtain raw fabric, and covering a teflon film on its surface.
Owner:江苏正大森源集团有限公司

Poly(ethylene carbonate) type polyurethane water-based adhesive

The invention discloses a poly(ethylene carbonate) type polyurethane water-based adhesive which is prepared through the following method: taking 100 parts of poly(ethylene carbonate) diol according to parts by weight, adding 2-10 parts of dimethylol propionic acid, stirring and slowly raising temperature to 100-120 DEG C under nitrogen protection, reducing the temperature to 50-70 DEG C after dissolution, dropping 20-60 parts of diisocyanate, raising the temperature to 70-80 DEG C, reacting for 2-3 hours, stopping heating when glue solution has viscosity and is transparent, naturally cooling to 40-50 DEG C, stopping introducing nitrogen, adding 100-700 parts of 5-30% of catalyst water solution while stirring intensely, neutralizing, emulsifying and preparing the adhesive. As a large number of carbonate bonds are contained in molecules of poly(ethylene carbonate) polyol, the bonding strength of a product is high; simultaneously, the carbonate bonds are less prone to hydrolysis, the storage stability of the product is high. In addition, the poly(ethylene carbonate) polyol is prepared by copolymerizing carbon dioxide and epoxy ethane, the cost is low, and the poly(ethylene carbonate)type polyurethane water-based adhesive has broad market application space.
Owner:HUIZHOU DAYAWAN DAZHI FINE CHEM

Acrylic acid modified epoxy phosphate resin and aqueous dispersion thereof

The invention belongs to the field of painting, and particularly relates to acrylic acid modified epoxy phosphate resin and an aqueous dispersion thereof. In the formula, the acrylic acid modified epoxy phosphate resin is prepared from 40-45 parts of epoxy resin, 20-30 parts of a solvent, 0.4-0.5 part of phosphoric acid, 8-12 parts of acrylic acid (ester) monomer of which acrylic acid accounts for 1.4-2 parts, 0.5-0.8 part of an initiator, 3.2-5.2 parts of neutralizer and 80-100 parts of water. The resin is prepared by the following steps: modifying epoxy resin with phosphoric acid, and reacting with acrylic acid and ester monomers thereof; adding the neutralizer and deionized water, stirring and emulsifying to obtain the acrylic acid modified epoxy phosphate aqueous dispersion, wherein the acid value of the emulsion is 10-12mgKOH/g, and the solid content is 28-38 percent. The prepared main resin dispersion body is epoxy resin, has a phosphate structure, and has a good adhesive force for metal base materials, thus having good corrosion resistance; acrylic resin is modified, introduced with carboxyl and neutralized by the neutralizer to give aqueous dispersion to resin, so that the resin can be produced into water-borne painting, and the content of VOC is greatly reduced; and multiple hydroxyl radicals are arranged on the main chain of the epoxy resin, and can be crosslinked with amino resin, urea resin and phenolic resin to produce stoving varnish.
Owner:BEIJING JINHWEILI APPLIED CHEM PROD

Fruit anti-cracking nutritional agent and preparation method thereof

The invention discloses a fruit anti-cracking nutritional agent and a preparation method thereof. The fruit anti-cracking nutritional agent comprises the following raw materials in part by weight: 5 to 15 parts of sodium carboxymethylcellulose, 3 to 7 parts of calcium, 1 to 5 parts of ethylene glycol, 0.01 to 0.9 part of plant growth regulator and 10 to 20 parts of water. The preparation method comprises the following steps of: (1) dissolving the sodium carboxymethylcellulose with the water so as to obtain sodium carboxymethylcellulose aqueous solution; (2) adding the calcium into the sodium carboxymethylcellulose aqueous solution and heating to the temperature of between 40 and 50 DEG C; and (3) adding the ethylene glycol into the solution obtained in the step (2), stirring at the temperature of between 40 and 50 DEG C for 30 to 40 minutes, lowering the temperature to the normal temperature, adding the plant growth regulator and stirring uniformly so as to obtain the fruit anti-cracking nutritional agent. The medicinal agent forms a film after being applied by spraying, is difficultly dissolved in the water for the second time after being dried, has a controllable thickness and can effectively lower fruit cracking rate by about 10 percent.
Owner:李开森

Acrylic acid modified epoxy phosphate ester resin and preparation method of aqueous dispersion thereof

The invention belongs to the field of coating and provides acrylic acid modified epoxy phosphate ester resin and a preparation method of aqueous dispersion thereof. The formula comprises 40-45 parts of epoxy resin, 20-30 parts of a solvent, 0.4-0.5 part of phosphoric acid and 8-12 parts of acrylic acid (acrylate) monomer, wherein the acrylic acid monomer accounts for 1.4-2 parts, an initiator accounts for 0.5-0.8 part, a neutralizer accounts for 3.2-5.2 parts and water accounts for 80-100 parts. The preparation method comprises the following steps: modifying the epoxy resin by using the phosphoric acid, reacting the epoxy resin with the acrylic acid and the ester monomer thereof, adding the neutralizer and deionized water, stirring and emulsifying to obtain the aqueous dispersion of the acrylic acid modified epoxy phosphate ester resin, wherein the acid value of the emulsion is 10-12 mg KOH / g, and the solid content is 28-38%. The main body of the obtained resin dispersion is epoxy resin, has a phosphate structure and has a good adhesive force on a metal base material, so that the corrosion resistance is excellent, carboxyls are introduced by the modification of the acrylic resin and provides water dispersibility after being neutralized by the neutralizer, the resin can be made into a water-based paint, the VOC content is greatly reduced, and a plurality of carboxyls are carried on the epoxy main chain to be crosslinked with such resin as amino, urea formaldehyde and phenolic aldehyde to be made into stoving varnish.
Owner:BEIJING JINHWEILI APPLIED CHEM PROD

Aluminum-zirconium-phosphorus master alloy and preparation method thereof

The invention belongs to the field of metal materials, relating to an aluminum-zirconium-phosphorus master alloy used for refining eutectic and primary silicon in hypereutectic Al-siliceous ferroalloy and a preparation method thereof. In a master alloy system, P exists in a mode of a ZrP compound which contains the following components by weight percent 78.0 percent to 94.0 percent of aluminum, 3.0 percent to 20.0 percent of zirconium and 1.0 percent to 6.0 percent of phosphorus. The preparation method comprises the following steps: preparing industrial pure aluminum, aluminum-phosphorus master alloy, sponge zirconium or potassium fluorozirconate according to the ratio; melting the industrial pure aluminum to 900 DEG C to 1300 DEG C in a melting furnace; firstly adding the aluminum-phosphorus master alloy to mix for 10 to 20 min; and then adding the sponge zirconium or the potassium fluorozirconate to fully react and uniformly mix, and directly casting the mixture to form a ingot or prepare a wire. The aluminum-zirconium-phosphorus master alloy has favorable refining effect, and can remarkably improve the high temperature mechanical properties of the alloy.
Owner:SHANDONG UNIV

Vegetable disease prevention and control preparation containing plant inducer

The invention discloses a vegetable disease prevention and control preparation containing a plant inducer. The vegetable disease prevention and control preparation contains the components by weight percent of 30-70% of polyglutamic acid and 30-70% of chitooligo saccharide. The preparation method comprises the step of: evenly mixing the polyglutamic acid with the chitooligo saccharide according to a ratio. The polyglutamic acid and the chitooligo saccharide are mixed according to the ratio, namely 1.5-2g of the mixture of the polyglutamic acid and the chitooligo saccharide is mixed with water with the weight being 15000-20000 times that of the mixture of the polyglutamic acid and the chitooligo saccharide in each 667m<2>; and the vegetable disease prevention and control preparation is sprayed at the surfaces of plants for preventing and controlling fungal diseases such as cucumber downy mildews and botrytis cinereas before a disease appears.
Owner:SUZHOU ACADEMY OF AGRI SCI +1
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products