The invention belongs to the technical field of
chemical separation and relates to a preparation method of a
wetting selective oil-water separation membrane separated according to requirements. The preparation method comprises the following steps: firstly, mixing an
aluminate precursor and a pH
regulator to form a solution, adding 8 to 12 ml of
aluminum ion pH
regulator mixed solution according toa porous
basement membrane per
square centimeter, carrying out
hydrothermal reaction at the temperature of 150 to 200 DEG C for 12 to 24 hours, taking out a reactant, washing and carrying out vacuumdrying to obtain a precursor separation membrane with a hierarchical structure; carrying out high-temperature calcining to obtain a superhydrophilic /
underwater super-oleophobic separation membrane with a hierarchical structure; then adding the superhydrophilic /
underwater super-oleophobic separation membrane into a
sodium laurate solution and carrying out modification reaction at the temperature of40 to 70 DEG C for 5 to 9 hours, and carrying out high-temperature calcining to obtain the superhydrophilic /
underwater super-oleophobic separation membrane with the hierarchical structure; and carrying out repeated calcining and
surface modification to obtain the
wetting selective membrane according to the requirements. The preparation method disclosed by the invention has the advantages of simple process and low cost, solves the problems of poor selectivity, high possibility of
pollution, low separation efficiency and the like of a traditional oil-water separation membrane are solved by utilizing surface superhydrophilic and super-hydrophobic characteristics under different conditions, and has a great application value in the fields of environment friendliness,
chemical engineering and the like.