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3232 results about "Liquid solid" patented technology
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Full-component resource reclamation method for waste positive electrode materials of lithium ion batteries
ActiveCN102751549AAvoid secondary pollutionImprove separation efficiencyWaste accumulators reclaimingBattery recyclingRecovery methodDistillation
The invention provides a full-component resource reclamation method for waste positive electrode materials of lithium ion batteries. The method comprises the following steps: 1) separating active substances and aluminum foils in waste positive electrode materials of lithium ion batteries by using an aqueous solution of fluorine-containing organic acid and carrying out liquid-solid-solid separation so as to obtain leachate, the lithium-containing active substances and the aluminum foils; 2) respectively carrying out high temperature roasting and impurity removal with alkali liquor on the lithium-containing active substances; 3) respectively carrying out recovery of the fluorine-containing organic acid through addition of acid and distillation, deposition of impurity ions through addition of alkali and ammonium carbonate coprecipitation on the leachate so as to prepare nickel-cobalt-manganese carbonate ternary precursor; and 4) carrying out component regulation on a mixture of the treated active substances and the nickel-cobalt-manganese carbonate ternary precursor, adding lithium carbonate in a certain proportion and carrying out high temperature solid phase sintering so as to prepare a lithium nickel cobalt manganese oxide ternary positive electrode material. The method provided in the invention has the following advantages: the application scope of the method is wide; separation efficiency of the lithium-containing active substances and the aluminum foils is high; short-flow direct re-preparation of positive electrode materials in waste lithium ion batteries is realized; and the method is applicable to large-scale resource reclamation of waste lithium ion batteries.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI
Protein Microspheres Retaining Pharmacokinetic and Pharmacodynamic Properties
ActiveUS20070207210A1Reduce solubilityImmunoglobulins against blood coagulation factorsPowder deliveryHigh concentrationMicrosphere
The present disclosure relates to compositions of methods of making and compositions small compositions of particles of an active agent. In accordance with the method of production, the active agent is dissolved in an aqueous or aqueous-miscible solvent containing a dissolved phase-separation enhancing agent (PSEA) to form a solution in a single liquid phase. The solution is subjected to a liquid-solid phase separation to cause the active agent to form small spherical particles that are substantially amorphous or non-crystalline and are injectable through fine bore needles at high concentrations. The particles exhibit the pharmacokinetic and pharmacodynamnic properties of the active agent. The disclosure has special application for higher molecular weight proteins such as antibodies.
Owner:BAXTER INT INC +1
Pretreatment method of wood fiber raw materials
InactiveCN101864683ARealize comprehensive utilizationRealize full-price developmentPretreatment with acid reacting compoundsCelluloseFiber
The invention relates to a pretreatment method of wood fiber raw materials, which belongs to the technical field of biomass chemical engineering. The process comprises the following steps: carrying out the first-step treatment after the wood fiber raw materials are mixed with mixed liquid of an organic acid solution and catalysts to obtain a liquid-solid mixture; separating the obtained liquid-solid mixture to obtain pretreatment black liquid and cellulose solids; washing the obtained cellulose solids by the organic acid solution to obtain washing black liquid and cellulose solids; adopting diluted acid or alkali for carrying out the second-step treatment on the obtained cellulose solids; mixing the obtained pretreatment black liquid and the obtained black liquid to obtain mixed black liquid; circularly using the mixed black liquid in the first-step treatment process; and recovering organic acids, lignin products and syrup solutions from the black liquid in the cyclic use for at least three times. The invention has the advantages that the full-rate development of raw materials can be realized, in addition, the environment-friendly effect can be realized, and the invention conforms to the requirement of modern biorefinery development.
Owner:TSINGHUA UNIV
Nanostructured material transport devices and their fabrication by application of molecular coatings to nanoscale channels
InactiveUS20050023156A1Reduced cross-sectional dimensionReduce the cross-sectional areaMaterial nanotechnologyFixed microstructural devicesEngineeringNanostructured materials
Owner:RAMSEY J MICHAEL +3
Batch-continuous process and reactor
InactiveUS20060081533A1Precise positioningTreatment using aerobic processesMultistage water/sewage treatmentRetention timeWastewater
This is a method of batch-continuous operation for treatment and separation of liquid-solid mixtures in a reactor with reactive solids comprising steps of continuously feeding the liquid in the reactor, contacting (possibly, mixing) liquid with the solids in at least a portion of the reactor, periodically separating the liquid from the solids in unmixed, or predominantly unmixed, portion of the reactor, discharging at least a portion of the separated liquid from the reactor, and retaining the separated solids in the unmixed portion of the reactor, and periodically resuspending the solids in the unmixed portion of the reactor and transferring the resuspended soilds into the portion of the reactor for contacting liquid with the solids. The contacting and / or mixing of the liquid with the solids in the mixed portion of the reactor can be continuous or periodic mixing. The unmixed zone differs from the quiescent zone in conventional clarifiers. It is a flow-through zone with a noticeably high velocity of flow as in aeration tanks of biological treatment systems. The retention time in unmixed zones is much shorter than in clarifiers. The method and apparatus can be used to treat water and wastewater, and in various chemical, biochemical, and pharmaceutical processing operations.
Owner:KHUDENKO BORIS M
Gas-liquid-solid three-phase suspension bed reactor for fischer-tropsch synthesis and its applications
ActiveUS20100216896A1High activitySimple structureHydrocarbon from carbon oxidesPhysical/chemical process catalystsGas phaseFiltration
A Fischer-Tropsch synthesis three-phase suspension bed reactor (“suspension bed” also called “slurry bed”) and its supplemental systems, may include: 1) structure and dimension design of F-T synthesis reactor, 2) a gas distributor located at the bottom of the reactor, 3) structure and arrangement of a heat exchanger members inside the reactor, 4) a liquid-solid filtration separation device inside reactor, 5) a flow guidance device inside reactor, 6) a condensate flux and separation member located in the gas phase space at the top of reactor, 7) a pressure stabilizer, a cleaning system for the separation device; an online cleaning system for the gas distributor; an ancillary system for slurry deposition and a pre-condensate and mist separation system located at the outlet of upper reactor. This reactor is suitable for industrial scale application of Fischer-Tropsch synthesis.
Owner:SYNFUELS CHINA TECH CO LTD
Preparation method of high-purity vanadium pentoxide
InactiveCN102923775AEfficient removalReduce pollutionVanadium oxidesMetal impuritiesAmmonium metavanadate
The invention discloses a preparation method of high-purity vanadium pentoxide. The preparation method comprises the following steps of: returning and dissolving coarse vanadium in aqueous alkali, and filtering the solution to remove metal impurities, which are subjected to precipitation reaction with the aqueous alkali, in the coarse vanadium, thus obtaining a primary returned solution; slowly pouring the primary returned solution into a sulfuric acid solution, adjusting the pH value of the solution to be 1.0-2.0 to obtain a liquid-solid mixture, and performing solid-liquid separation on the liquid-solid mixture; filtering and washing precipitates obtained from the solid-liquid separation of the mixture, and returning and dissolving the mixture into the aqueous alkali, thus obtaining a secondary returned solution; adding ammonium sulfate into the secondary returned solution for precipitating vanadium, and filtering the solution to obtain ammonium metavanadate; and processing the ammonium metavanadate to obtain the high-purity vanadium pentoxide. The preparation method adopting multiple stages of returned dissolving can be used for effectively removing the metal canon impurities of the vanadium pentoxide, and further obtaining the high-purity vanadium pentoxide with the metal canon impurity contents of less than 0.001% and the vanadium pentoxide content of 99.99%.
Owner:PANZHIHUA IRON & STEEL RES INST OF PANGANG GROUP
Encapsulated phase change materials in seed coatings
InactiveUS20090227451A1Good flexibilityIncrease productionBiocideFertilising methodsSeed dormancyPhase change
The present invention is directed to improved seed coatings which facilitate fall or early spring planting while maintaining seed dormancy until soil temperatures are appropriate for successful germination. The improved seed coatings contain encapsulated phase change materials within a polymeric shell which preserve the dormancy of the seed during early planting by slowing the rate at which the seed temperature rises in the event of a temperature spike thus preventing premature germination. The encapsulated phase change material is a material characterized by a solid / liquid or liquid / solid phase change which occurs at a temperature which ranges from about −5 to about 20° C., preferably between about 0 to about 19° C., most preferably between about 5 to about 15° C. The solid / liquid or liquid / solid phase change is further characterized by an effective enthalpy of fusion / crystallization for the solid-liquid / liquid-solid phase change equal to or greater than 20 J / g when determined by Differential Scanning Calorimetry.
Owner:CIBA CORP
Liquid-solid mixed lipid nano-slow release system for cosmetic and preparation method thereof
InactiveCN102793628AParticle size controllablePlay its due roleCosmetic preparationsBody powdersWater bathsLipid formation
The present invention relates to a liquid-solid mixed lipid nano-slow release system for cosmetics and a preparation method thereof. The release system is composed of nanoparticles constituted by liquid lipid and solid lipid and at least one active ingredient coated in the nanoparticles. The preparation method includes: (1) dispersing a mixing carrier of the solid lipid and the liquid lipid to an organic solvent, adding the active ingredient, and heating in a water bath to dissolve the solid lipid to get an organic phase solution; (2) formulating polyvinyl alcohol into an aqueous phase solution, and adjusting the pH to be acidic to get an aqueous phase solution; and (3) adding the organic phase solution to the aqueous phase solution under the conditions of mechanical agitation with stirring to get a mixed lipid dispersion liquid which is then centrifuged and separated to obtain the nano-slow release system. The nano-slow release system is simple in preparation method and high in stability. The dimensions of the particles are in nanoscale, and the particle size is controllable. The entrapment efficiency of the liquid-solid mixed lipid nanoparticles has been greatly improved than simple solid nanoparticles.
Owner:DONGHUA UNIV
Anaerobic biological wastewater treatment system and process
ActiveUS20060131231A1Improve volume efficiencyLower initial installation costsTreatment with anaerobic digestion processesTreatment with aerobic and anaerobic processesAnaerobic microorganismsTreatment system
The present invention discloses an anaerobic biological wastewater treatment system for treating wastewater containing organic contaminants, which includes an anaerobic sludge bed reactor and a dissolved-air flotation tank. The anaerobic sludge bed reactor is used to decompose organic contaminants by way of an anaerobic biological treatment. The dissolved-air flotation tank is used to carry out liquid-solid separation on effluent from the anaerobic sludge bed reactor, so that anaerobic microorganisms entrained in the effluent can be recovered and recycled to the anaerobic sludge bed reactor, thereby enhancing the hydraulic loading of the anaerobic sludge bed reactor.
Owner:IND TECH RES INST
Pre-treatment liquid for use in preparation of an offset printing plate using direct inkjet CTP
InactiveUS6906019B2Improve image qualityFast plating speedSurface-active detergent compositionsDuplicating/marking methodsPre treatmentSurface chemical
A method of making a printing plate in which the uncoated surface of a substrate is treated with a pre-treatment solution prior to the deposition of ink on the surface. The pre-treatment liquid comprises a polyvalent metal salt, and at least one of an organic swelling reagent and / or a coalescence reagent. The pre-treatment liquid is applied to form a thin, homogenous layer of approximately 4 μm to the entire upper surface of the recording plate. The swelling reagent and / or the coalescence reagent and the polyvalent metal cations are physically well localized in the porous structure of the plate's surface. After partial drying of the pretreated anodized aluminum plate, CTP liquid is deposited onto the surface to form an image. The CTP liquid solids react with the pre-treatment liquid and are, therefore, chemically bound to the surface. This allows all data to be deposited in a single pass of the inkjet head without the problem of clustering.
Owner:HEWLETT PACKARD IND PRINTING LTD
Method for preparing load type rhodium catalyst for making high-carbon aldehyde using hydroformylation of higher olefins
InactiveCN101116816AImprove stabilityCatalyst activation/preparationPreparation by carbon monoxide reactionAlkaline earth metalFormylation reaction
A modified activated carbon supported rhodium type catalyst for high carbene hydrocarbon hydrogen formylation reaction is provided. The preparation of the catalyst comprises the techniques such as carrier pretreatment-activity rhodium solid-phase bound reagent combination, and used for gas-liquid-solid three phase catalyst system, which is characterized in that: a certain amount of alkali or alkaline earth metal hydroxide and salt modification activated carbon is used as a carrier, and the supported rhodium catalyst is prepared by using multiple impregnation method. The catalyst of the present invention is high in activity and selectivity. The catalyst is easy to be separated from products after reaction, capable of being used repeatedly, stable in performance, and suitable for the production process of high carbene hydrocarbon or mixed olefin hydrogen formylation made high carbon aldehyde, which has good industrial application value.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)
Method for synchronously extracting hemicellulose, cellulose and lignin and reclaiming phenolic acid compounds
InactiveCN101143881AProtect chemical structureReduce generationLignin derivativesPaper material treatmentOrganic solventChemical composition
The present invention provides a technique method which separates lignose, hemicellulose, cellulose and phenolic acid from lignocellulosic biomass. Under the selected pH value and temperature, the lignocellulosic biomass is processed by hot water, so that the hemicellulose and the phenolic acid are preferentially resolved in aqueous solution, delignification processing is carried out, organic solvent or alkaline solution is applied to carry out high-temperature cooking, the generated liquid-solid phase product can be easily and effectively separated, and thus the hemicellulose, the cellulose and the phenolic acid can be respectively obtained. Moreover, enzymatic treatment can be selectively added, and a solid phase product is obtained at the first stage of a group of enzymatic treatment with a cooperative effect. Because the ferulic acid linkage between the hemicellulose and the lignose can be selectively broken, the separation of the chemical components has a high yield rate and high purity.
Owner:孔延华
Combined treatment method for oilfield solid waste
InactiveCN101963358AHigh recovery rateLess investmentIncinerator apparatusCombustion chamberOil sludge
The invention provides a new combined treatment process for oilfield solid waste (oil sludge, industrial solid waste and household garbage). In the process, liquid-solid separation is performed on the oil sludge of an oilfield by adopting a conditioning-centrifugal separation process; the separated liquid enters oil-water separation equipment constructed on the oilfield for recovering crude oil; the oil recovery rate is up to 65 to 90 percent; after drying separated solid residue, the separated solid residue and pre-crushed industrial solid waste and household garbage are mixed and enter a countercurrent-type rotary gasification incinerator; combustible components in the oilfield solid waste are decomposed and gasified into combustible gases which are combusted partially in the incinerator; the combustible gases are combusted completely in a secondary combustion chamber; high-temperature smoke gas afterheat is recovered by a conduction oil afterheat boiler and air preheating equipment; and low-temperature smoke gas of which the afterheat is recovered is harmlessly exhausted after being treated by a sharp-quenching deacidification tower, an activated carbon adsorption tower and a bag-type dust remover. The process realizes the purposes of decrement, harmlessness and resources of oilfield solid waste treatment.
Owner:KUNMING UNIV OF SCI & TECH
Toughened hard alloy and preparation method thereof
The invention discloses a high-toughness toughened hard alloy which comprises 10%-30% of Co or Co and Ni serving as a binding phase, 0-1.5% of Cr3C2 serving as an inhibitor, and the balance of hard phase WC, wherein the hard phase consists of WC crystalline grains with coarse, medium and fine grain sizes, the grain size of coarse grains is 9-15 mu m, the grain size of medium grains is 4-7 mu m, the grain size of the fine grains is less than 2 mu m, and the mean grain size of the hard phase WC is 1.6-3.2 mu m. The preparation method of the toughened hard alloy comprises the following steps of: preparing materials including 10%-30% of cobalt powder or cobalt powder and nickel powder, 0-1.5% of chromium carbide powder, and the balance of tungsten carbide powder, wherein Fsss grain size of the coarse grains WC is 9.0-11.0 mu m, the coarse grains WC account for 20%-42% of the prepared powder, the Fsss grain size of the medium grains WC is 4.0-6.0 mu m, the medium grains account for 10%-25% of the prepared powder, the Fsss grain size of the fine grains WC is 1.0-2.0 mu m, and the fine grains account for 20%-40% of the prepared powder; grinding, wherein a liquid paraffin forming agent which accounts for 2% of the prepared materials is added, mixed with absolute ethyl alcohol in a liquid-solid ratio of 300 ml / kg-350ml / kg, wet-ground for 20-28 hours according to the condition that the ratio of grinding media to material is 4:1, and sprayed and dried to obtain mixed materials; pressing; vacuum-sintering and isostatic-pressing and sintering. According to the invention, the toughness is improved on the premise of ensuring the hardness of the alloy, so that the operation field is expanded, special requirements of a cold-heating and cold-punching mould and a holt-rolling hard alloy roller ring are satisfied, and the service life of the high-toughness toughened hard alloy is prolonged.
Owner:ZHUZHOU HARD ALLOY GRP CO LTD
Method for separating antimony and arsenic from antimony and arsenic-containing ash through oxidation and alkaline leaching
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI +1
Liquid-solid circulating fluidized bed waste water treatment system for simultaneous carbon, nitrogen and phosphorus removal
InactiveUS20040178132A1Easy to adaptIncrease contactTreatment using aerobic processesIon-exchanger regenerationActivated sludgeOxygen
Biological nutrient removal (BNR) in municipal wastewater treatment to remove carbonaceous substrates, nutrients and phosphorus, has recently become increasingly popular worldwide due to increasingly stringent regulations. Biological fluidized bed (BFB) technology, which could be potentially used for BNR processes, can provide some advantages such as high efficiency and compact structure. This present invention incorporates the fixed-film biological fluidized bed technology with the biological nutrient removal in a liquid-solid circulating fluidized bed, which has achieved the simultaneous elimination of organic carbon, nitrogen and phosphorus, in a very efficient manner and with very compact space requirements. The BNR-LSCFB has two fluidized beds, running as anoxic / anaerobic and aerobic processes to accomplish simultaneous nitrification and denitrification and to remove carbonaceous substrates, nutrients and phosphorus, with continuous liquid and solids recirculation through the anoxic / anaerobic bed and the aerobic bed. The new BNR-LSCFB system is not only an excellent alternative for conventional activated sludge type BNR technologies but is also capable of processing much higher loadings and suitable for industrial applications.
Owner:UNIV OF WESTERN ONTARIO
Green mining system of natural gas hydrate from non-lithified stratums of deep-sea seabed superficial layers
ActiveCN103628880ANo change in temperature and pressure conditionsEnabling in-situ solid-state developmentMineral miningParticulatesForming gas
The invention discloses a green mining system of natural gas hydrate. The green mining system is used for mining natural gas hydrate from non-lithified stratums of deep-sea seabed superficial layers. The green mining system comprises a seabed tunneling-fluidifying-lifting pry, a closed fluidifying gathering pipeline and a sea surface separating and processing system, wherein the seabed tunneling-fluidifying-lifting pry is used for excavating a natural gas hydrate reservoir in a solid state in a storage region of the natural gas hydrate by virtue of the temperature and pressure in a natural environment, collecting solid matter of the natural gas hydrate, and crushing the solid matters of the natural gas hydrate into particulate matters, and seawater and the particulate matters are mixed through injection to form gas-liquid-solid multiphase mixture flow; the closed fluidifying gathering pipeline comprises a closed pipeline which is connected with the seabed tunneling-fluidifying-lifting pry so as to lift the gas-liquid-solid multiphase mixture flow to the sea surface; the sea surface separating and processing system is arranged at a sea surface support system and comprises a separating device and a processing device, the separating device is used for separating a gas-liquid-solid multiphase mixture lifted to the sea surface through the closed pipeline, and the processing device is used for processing separated matters. According to the green mining system, the safe and green mining of the deep-sea natural gas hydrate is realized, and potential hazards in multiple aspects are avoided.
Owner:CHINA NAT OFFSHORE OIL CORP
DSP-based electromagnetic flowmeter signal processing system
ActiveCN101893465AHigh precisionAvoid interferenceVolume/mass flow by electromagnetic flowmetersSoftware systemHandling system
The invention discloses a DSP-based electromagnetic flowmeter signal processing system, which comprises a hardware system and a software system. The hardware system consists of an excitation driving module, a signal modulation and acquisition module, a signal processing control module, a man-machine interface module, a communication module and a power supply management module. The signal control module uses DSP as a core. In the system, a high frequency square wave excitation control scheme is adopted, and the DSP generates an excitation time sequence to control the excitation driving module to perform high frequency square wave excitation of a magnet exciting coil; the signal modulation and acquisition module amplifies and filters an output signal of an electromagnetic flowmeter, performs the analog-to-digital conversion of the output signal and outputs the output signal to the DSP; the software system processes an acquired signal to obtain a flowmeter measurement result and send the result to a liquid crystal display; and the parameters of the flowmeter are set by keyboard operation or by the interaction between a master computer and the flowmeter by the communication module. The system can realize the high-accuracy and high-speed measurement of fluid flow, particularly the measurement of flow of liquid-solid two-phase fluid such as pulp.
Owner:HEFEI UNIV OF TECH +1
Method for producing nanowires using porous glass template, and multi-probe, field emission tip and devices employing the nanowires
InactiveUS20090045720A1Easy to controlMaterial nanotechnologyDischarge tube luminescnet screensVapor liquidNanowire
Disclosed herein is a method for producing nanowires, which features the use of a porous glass template in combination with a solid-liquid-solid or vapor-liquid-solid process for growing nanowires which are highly straight and have nanoparticles precisely arranged therein. The nanowires can be grown into composite structures of superlattices and hybrids by modulating the composition of the materials provided thereto. Also disclosed is the use of the nanowires in multi-probes, field emission tips, and devices.
Owner:SAMSUNG ELECTRONICS CO LTD
Dual stage centrifugal liquid-solids separator
InactiveUS7025890B2Reduce cavitationEasy to disassembleWater/sewage treatment by centrifugal separationLiquid degasificationDual stageSpins
Disclosed is a vortex-based centrifugal separator for removing solids from a liquid / solids fluid stream in two stages. A fluid stream under pressure is introduced at the top of the cylindrical separator at a tangential angle forming helical downward flow. The first stage uses a centrally-located spin plate for reversing the cleaner interior flow of the vortex back upward, while the heavier solids settle at the bottom of the chamber for periodic removal. In the second stage, a plurality of louvered slots in an upper discharge pipe remove finer solids from the exiting upward fluid flow prior to discharge.
Owner:GRISWOLD CONTROLS LLC
Entrained flow gasifier used for co-gasification of various forms of raw materials
The invention provides an entrained flow gasifier used for the co-gasification of various forms of raw materials. The gasifier is formed by overlaying a gasification chamber and a cooling and washing chamber in a pressure-resisting shell. By adjusting a nozzle configuration scheme, the gasification of a single raw material and the co-gasification of gas-liquid-solid raw materials can be realized and the demands of different sizes of gasification systems can be satisfied. For a medium or small system, an overhead nozzle scheme is adopted for 50-1000 tons of coal per day. For a single serie of large-scale system, a multi-nozzle scheme is adopted for 1000-6000 tons of coal per day; the gasification furnace adopts impinging stream (oppesed multi-nozzle) and cross jet stream (overhead nozzle) to efficiently mix the raw materials and efficiently mix the raw materials and gasifying agents (oxygen and steam). The gasification furnace has excellent high flexibility, large load-adjusting range, high raw material utilization rate which is up to more than 98% and low specific oxygen consumption and specific raw material consumption, and the raw material is convenient to change.
Owner:EAST CHINA UNIV OF SCI & TECH
Harmless and comprehensive utilization method of secondary aluminum dross
InactiveCN107555447ARealize harmless treatmentTo achieve the purpose of "zero emission" utilizationChloride preparationFluoride preparationSlurryLiquid solid
The invention provides a harmless and comprehensive utilization method of secondary aluminum dross and relates to a harmless and comprehensive utilization method of secondary aluminum dross produced in an aluminum dross treating process. The harmless and comprehensive utilization method is characterized in that slurry is prepared from the secondary aluminum dross produced in the aluminum dross treating process and water, a stirring deamination reaction is performed, and ammonia gas formed through the reaction is condensed or absorbed by water; slurry after the reaction is subjected to liquid-solid separation, separated liquid phase is subjected to evaporative crystallization, and a chlorate and fluoride salt mixture is obtained; separated solid phase is used for producing a calcium aluminate material. With adoption of the method, the aluminum dross can be treated harmlessly, useful components in the aluminum dross are recovered efficiently, the harmless secondary aluminum dross can replace high-alumina bauxite for preparing a calcium aluminate product, production cost is reduced greatly, zero-release utilization of the aluminum dross is realized, the process is simple, the operation is convenient, the cost is low, environmental protection is realized, and the method has wide applicability.
Owner:GUIZHOU BRANCH CHINA ALUMINUM IND
Clean production method for preparing sodium chromate from chromite
InactiveCN101659444AObvious superiorityLow reaction temperatureChromates/bichromatesSlagSodium nitrate
The invention relates to a clean production method for preparing sodium chromate from chromite, which comprises the following steps of: reacting the chromite with an oxidizing gas in a medium of NaOH-NaNO3-H2O, wherein sodium nitrate serves as a catalytic medium and is not consumed in the reaction; obtaining a mixed reaction product of an alkali liquor, the sodium chromate and iron slag after thereaction; leaching the mixed reaction product, performing liquid-solid separation of the alkali liquor and a crystal slag mixture (a mixture of a sodium chromate crystal and the iron slag), dissolvingthe mixture of the iron slag and the sodium chromate crystal, performing liquid-solid separation of the solution of the iron slag and the sodium chromate crystal, performing evaporative crystallization of the sodium chromate solution, rinsing and drying the obtained sodium chromate solution, obtaining qualified sodium chromate products; and circulating the crystallized mother liquor and the alkali liquor together to decompose the chromite. In the method, the chromium conversion ratio is above 99 percent and the chromium content ratio in the slag is less than 0.5 percent.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI
Method used for preparing ammonium metavanadate from vanadium slag via ammonium salt leaching
ActiveCN103952565AImprove leaching rateLow impurity contentProcess efficiency improvementSlagAmmonium metavanadate
The invention discloses a method used for preparing ammonium metavanadate from vanadium slag via ammonium salt leaching. The method comprises following steps: (1) vanadium slag is subjected to pre-oxidation so as to obtain a calcined product; (2) the calcined product is subjected to leaching with an ammonium salt aqueous solution, and liquid-solid separation is carried out; and (3) a liquid obtained via step (2) is subjected to cooling crystallization and separation so as to obtain ammonium metavanadate crystals. The method is high in vanadium leaching efficiency; leaching solution impurity content is low; ammonium metavanadate can be obtained via cooling crystallization; waste water contains no mirabilite; subsequent processes, such as purifying, vanadium precipitation, and waste water treatment, are simplified; technical cost is low; operation is simple; and the method is clean, and no pollution is caused.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI
Ultragravity field rotary bed mass transfer and conversion unit
ActiveCN1611293ASmall sizeSmall footprintChemical/physical/physico-chemical moving reactorsFractional distillationLine tubingMetal
The present invention discloses an ultragravitational field rotation bed mass transfer and reaction equipment. Said equipment comprises machine shell, rotor, rotary foam-catching device and transmission device. The described machine shell comprises gas inlet end cover, straight cylinder section and gas outlet end cover; the described transmission device is formed from motor, transmission shaft, supporting bearing and seal system, and the described rotor is formed from dual rotors, and is consisted of two metal frames with shared bottom plate, two phases of gas and liquid can be parallelly-flowed and contacted on one rotor, and on another rotor they are counter-current-wise contacted, and the rotors are fixed on the shaft by means of shared bottom plate. Said invented equipment can be extensively used in the mass transfer and reaction process of multiphase material system of gas-liquid, gas-liquid-solid and gas-liquid-liquid.
Owner:CHINA PETROLEUM & CHEM CORP +2
Process for continuous preparation of trimellitic anhydride by step catalytic oxidation process
The invention provides a process for continuous preparation of trimellitic anhydride by step catalytic oxidation process by using pseudocumene as raw material, fatty group carboxylic acid as dissolvent, cobalt, manganese and bromine as catalyst, the preparing process comprises the steps of, (1) stepwise continuous catalysis oxidizing process, (2) crystallization and liquid-solid separation, (3) anhydride forming procedure, (4) subtractive process, and (5) solvent reclamation.
Owner:CHINA PETROLEUM & CHEM CORP +2
Method and device for producing thiamine from sulfur dioxide in recorered smoke
InactiveCN1648049ANo secondary pollutionDispersed particle separationAmmonium sulfatesPollutionAmmonium sulfate
The present invention discloses method and apparatus for recovering SO2 from fume to produce ammonium sulfate. The present invention has ammonia recovering section over the absorbing section to avoid loss of ammonia and independent fume cooling and humidifying section to produce ammonium sulfate crystal in a saturation and crystallization process in lowered steam energy consumption. Hydraulic staged cyclonic unit is used as effective liquid-solid separator to raise the crystallization degree of the ammonium sulfate product. The whole desulfurizing system produces no waste and has no secondary pollution. The desulfurizing tower has high eliminating efficiency of harmful SO2, SO3, NOx, HCl, HF and dust.
Owner:EAST CHINA UNIV OF SCI & TECH
Device and method for combined use of molecular imprinting solid phase microextraction and hollow fiber liquid phase microextraction, and application thereof
InactiveCN101637668AHigh enrichment factorAnalysis fitIon-exchange process apparatusIon-exchanger regenerationHollow fibre membraneFiber
The invention discloses a device and a method for the combined use of molecular imprinting solid phase microextraction and hollow fiber liquid phase microextraction, and the application thereof. The device consists of a solid phase microextraction device, a molecular imprinting solid phase microextraction probe, a hollow fiber membrane, an extraction bottle and a stirrer. The molecular imprintingsolid phase microextraction probe is inserted in to a hollow fiber membrane cavity containing organic solvent, fixed and then directly positioned into a sample solution to be measured for purpose of liquid-solid phase synchronous microextraction. During the microextraction, analytes permeate the hollow fiber membrane, are then enriched in the organic solvent and then undergo secondary extraction and enrichment under the action of the molecular imprinting solid phase microextraction probe. The device is simple, operates conveniently, facilitates the combined use with an analyzer, is suitable for the separation and enrichment of organics with trace amounts in complex water phase samples obtained from the fields such as environment, food, medicine, biology and the like.
Owner:SUN YAT SEN UNIV
Three-phase energy storage method of solar air conditioner
ActiveCN104374025ATake advantage ofEasy to adjustClimate change adaptationEnergy efficient heating/coolingHigh energyVolumetric Mass Density
The invention provides a three-phase energy storage method of a solar air conditioner, and belongs to the field of solar air conditioners. An absorbing type refrigerating working pair serves as an energy storage medium, a three-phase energy storage device is connected with a generator in a solar absorbing type refrigerating system in parallel, a solar heat collecting medium provides heat for the three-phase energy storage device and the generator, surplus solar collected heat is stored in the three-phase storage device in an energy storage medium chemical potential energy mode by adjusting the flow of the heating collecting medium entering the three-phase energy storage device in real time, and good matching of a drive heat source and an air conditioner load is achieved. The three-phase energy storage method avoids the dangers brought by crystallization during serial connection of a two-phase energy storage device and a generator in the prior art, the load adjusting function of the solar air conditioner can be achieved through an energy storage system by means of gas-liquid-solid three-phase high energy storage density, and the crystallization rate of 50% enables the size of the energy storage device to be reduced by more than a half than the size of an energy storage device in a two-phase energy storage mode. The system is simple, adjustment is convenient and flexible, the amount of released cold is stable, and a common solar air conditioning system can be easily improved into an energy storage air conditioning system.
Owner:BEIJING UNIV OF TECH
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