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341 results about "Hydrolytic Process" patented technology

Hydrolytic process. A reaction of both organic and inorganic chemistry wherein water effects a double decomposition with another compound, hydrogen going to one compound and hydroxyl to another.

High-magnetic heavy-metal ion adsorbent carrying conductive high molecules and preparation method thereof

The invention discloses a high-magnetic heavy-metal ion adsorbent carrying conductive high molecules and a preparation method thereof. The adsorbent comprises high-magnetic microspheres carrying conductive high molecules, each of which comprises a Fe3O4 polycrystal sphere cluster, an amorphous SiO2 protective layer and a polypyrrole adsorption outer layer from inside to outside. The preparation method of the adsorbent is realized in a way that: carrying out a solvent thermal reduction reaction on soluble ferrites to obtain the Fe3O4 magnetic sphere cluster; carrying out the basic hydrolysis by using tetraethoxysilane to obtain the Fe3O4-SiO2 nuclear shell sphere cluster; and finally, carrying out the free radical polymerization reaction on the pyrrole monomers to obtain the Fe3O4-SiO2-polypyrrole functional particles. The heavy-metal ion adsorbent has the characteristics of stable property, high adsorption rate and reproducibility, has favorable adsorption and recovery properties on dichromic ions, and has the advantages of simple preparation process, low material price and no environmental pollution. Compared with the normal chemical absorbent, the product of the invention is convenient to use and achieves the effects of waste water treatment, pollution abatement and environment protection.
Owner:NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI

Process for preparing furfural by using agricultural by-products of high and crude fiber plants

The invention discloses a process for preparing furfural by using agricultural by-products of high and crude fiber plants. The process includes the steps of 1) conducting pretreatment of raw materials; 2) hydrolyzing pretreated raw materials in a hydrolyzing tank, and using an acid catalyst formed by mixing sulfuric acid and phosphoric acid during the hydrolytic process; 3) introducing high-temperature steam into the hydrolyzing tank, heating up the hydrolyzing tank, and conducting gap stripping for hydrolysis products of furfural; and 4) feeding gas stripped furfural to into a furfural phase splitter to obtain coarse furfural and furfural residues. According to the process, the acid catalyst combining the sulfuric acid and the phosphoric acid is used for hydrolyzing the raw materials, and the hydrolytic process is assisted by ultrasonic treatment simultaneously, so that the productivity of the furfural is improved, the residue amount of the sulfuric acid is a little, the production of sulfur oxides in the subsequent activating process of furfural residues is reduced, and the environmental pollution is reduced. Besides, the invention also provides a process for producing activated carbon adsorbents by using the furfural residues. The process includes the steps of drying the furfural residues, screening, roasting, hardening activating and steam curing, the obtained activated carbon specific surface is large, the iodine value is high and the adsorption capacity is high.
Owner:北京博能康成科技有限公司

Medium temperature carbon bisulfide hydrolytic catalyst and preparation method and application thereof

InactiveCN101121123AHigh hydrolysis catalytic rateMetal/metal-oxides/metal-hydroxide catalystsIndustrial gasSocial benefits
A medium-temperature carbon disulfide hydrolysis catalyst and its preparation method and application belong to a catalyst for removing organic sulfur in raw material gas, and the purpose is to solve the problem that CS2 is difficult to remove compared with COS in the catalytic hydrolysis of carbon disulfide. It is characterized in that by adding catalyst modifiers ZrO2 and La2O3, a catalyst with high CS2 hydrolysis catalytic rate, anti-coking and no conversion side reactions is obtained at medium temperature, and its preparation method is that the modifier and the activity accelerator are divided into two steps Loading is done by isometric impregnation. Under normal pressure, temperature 200-400°C, space velocity 2000-8000h-1, CO volume content 0-30%, CS2 concentration less than 500mgS / m3, the carbon disulfide hydrolysis conversion rate is above 95%. It is mainly developed for medium-temperature purification of carbon disulfide in industrial gases containing carbon monoxide, and has considerable application value, economic benefits and social benefits.
Owner:TAIYUAN UNIV OF TECH

Sludge pyrohydrolysis method and sludge pyrohydrolysis system

The invention relates to a sludge pyrohydrolysis method and a sludge pyrohydrolysis system, belongs to the field of treatment of a sewage plant, and particularly relates to the field of treatment of sludge of a sewage treatment product. To solve the problem that most of organic matters are not removed with an existing method, the invention provides the sludge pyrohydrolysis method and the sludge pyrohydrolysis system. The method comprises the processes of sludge slurrying, sludge pyrohydrolysis, sludge decompressed flash, sludge digestion, and centrifugal dewatering, wherein the process of sludge slurrying adopts a pump stirring mode, the temperature in a slurrying tank is kept at 97 DEG C; saturated steam heats a pyrohydrolysis tank to rapidly rise the temperature to be 165-190 DEG C in the process of sludge pyrohydrolysis, the pyrohydrolysis process lasts for 90 min, wherein the time for sludge charge is 15 min, the time for sludge discharge is 15 min, the steam is introduced for about 15 min, the pyrohydrolysis reaction is about 30 min, and the air is exhausted for 15 min; in the flash process, the pressure of a flash tank is kept at 0.1-0.3 MPa and the balance temperature is 102 DEG C; the time for sludge digestion is 15 days. The method and the system use the modes of pyrohydrolysis and flash, the organic matters in the sludge are effectively removed, meanwhile, the time for sludge digestion is shortened, and the sludge treatment efficiency is improved.
Owner:XIAN HUALU ENVIRONMENTAL PROTECTION EQUIP

Method for preparing strong antioxidative peptide by using peanut meal

The invention discloses a method for preparing strong antioxidative peptide by using peanut meal. The method comprises the following steps of: (1) uniformly mixing the peanut meal and an acidic buffer, carrying out microwave heating, and placing in a powdering machine, thus obtaining powder peanut meal; (2) adding water, protease and cellulase, then adding a surface active agent, hydrolyzing at 45-60 DEG C, and carrying out centrifugal separation to obtain liquid supernatant which is peanut meal enzymatic hydrolysate; and (3) adding an ethanol solution to the peanut meal enzymatic hydrolysate, carrying out ultra-filtration, collecting trapped fluid, and carrying out spray drying to obtain the strong antioxidative peptide. According to the method, the peanut meal is pretreated by adopting microwave heating and the acidic buffer, so that disulfide bonds in peanut meal proteins are converted into sulfydryl bonds, more enzymolysis sites are exposed, and the enzymatic hydrolysis is facilitated. The surface active agent is used for cooperating with the enzymatic hydrolysis, changing the characteristics of an enzymolysis substrate, enlarging a surface on which celluloses can be adsorbed, and sequentially simulating reaction sites to be adsorbed on enzymes; and meanwhile, the surface active agent has stablizing effect on the enzymes, effectively stops the denaturation of enzymes in a hydrolytic process and is beneficial to the improvement of hydrolysis efficiency of the proteases.
Owner:广东华肽生物科技有限公司

Method for rapidly converting animal-poultry faeces into high-efficiency fertilizer

The invention discloses a method for rapidly converting animal-poultry faeces into high-efficiency fertilizer, which comprises the following steps: hydrolyzing animal-poultry faeces under the acidity condition and producing amino acid (ova and germina are all killed in the process) to obtain crop synergia fertilizer; adding hydrolyticre agent into dispersant, odor absorbent, adhesive-maintaining agent, coating agent and bulking agent. The fertilizer not only has good fertilizer efficiency, but also has good effects on the proliferation of microbes in soil, can avoid occurrence of the following situations that microbes in soil die out, salt is accumulated and soil is hardened as chemical fertilizer is misused; and the implementation of the method plays a positive role in agricultural non-pollution ecological production and industrial production.
Owner:广西北国生物科技有限公司

Method of using TiCl4 to prepare high-activity double-effect crystal seed and control titanium dioxide particle size

The invention provides a method of using TiCl4 to prepare a high-activity double-effect crystal seed and control titanium dioxide particle size. Specifically, the method employs TiCl4 as a raw material, a precipitate is prepared through a certain proportion and rapid neutralization of a dilute base solution, the precipitate is subjected to peptizing, curing and quenching and then is adjusted to have a proper pH value, then soluble salt compositions are removed through washing, so that the high-activity double-effect crystal seed, which is applied to hydrolysis process and calcining process of production of sulfuric-acid-process titanium dioxide, is prepared. The prepared crystal seed is uniform in particle size and high in activity, and also during application of hydrolysis of a titanium solution, by adjusting the addition amount of the seed crystal and cooperating with addition of a proper salt treating agent and control on calcining intensity, rutile type titanium dioxide with different particle sizes can be prepared, and thus the particle size demands on different products are satisfied. The preparation technology is simple, not high in equipment investment and high in operation controllability, and the prepared double-effect crystal seed is capable of producing titanium dioxide hydrate primary particles with uniform particle size, so that the uniformity of calcined product particle size is guaranteed, and optical performances and pigment performances of titanium dioxide are perfectly exhibited.
Owner:SICHUAN LOMON TITANIUM IND CO LTD

Method of forming a dielectric film

A method of forming a dielectric film on a Si substrate comprises the steps of adsorbing a gaseous molecular compound of a metal element constituting a dielectric material on a Si substrate, and causing a decomposition of the gaseous molecular compound thus adsorbed by a hydrolysis process or pyrolytic decomposition process or an oxidation process.
Owner:TOKYO ELECTRON LTD

Harmless treatment method for secondary aluminum ash

A harmless treatment method for secondary aluminum ash comprises the following five process steps: (1) preparing raw materials, namely preparing the secondary aluminum ash; (2) carrying out hydrolysis in a hydrolytic tank; (3) carrying out filter pressing by using a filter press and washing; (4) fixing fluorine by using calcium hydroxide; and (5) washing ammonia gas generated by reaction in a third-stage leaching tower. The method disclosed by the invention has the following advantages: firstly, aiming at the ammonia gas and hydrogen gas generated in a secondary aluminum ash hydrolysis process, a hydrolytic tank sealing form is adopted to prevent air from being mixed in, and a continuous feeding form and a continuous discharging form are adopted, so that explosion accidents of a large amount of ammonia gas and hydrogen gas generated instantly are effectively avoided, and the method is a safe and reliable recovery process; secondly, the whole technological process consumes less equipment, so that the energy consumption is low; the production cost of the method is lower than that of calcination, acid leaching and other processes, the product high-aluminum material, the by-product fluorite calcium fluoride and dilute ammonia water can be comprehensively utilized, and the economic benefit is high. The method is suitable for treating aluminum ash by-products in the electrolytic aluminum industry.
Owner:邵冰 +1

Novel method of producing strontium ranelate heptahydrate

The invention relates to a new preparation method of strontium ranelate heptahydrate. The products produced by the method have water content of 19.0 per cent to 20.4 per cent and the relevant substances are lower than 0.5 per cent. The strontium ranelate heptahydrate produced by the method is stable under room temperature, has little water content differences between batches and is kept for a long time under natural environment with unchangeable moisture, content and relevant substances. The method is characterized in that: (1) the reflux of the 2-[N, N- 2(carboxymethyl)amino]-3-cyano-group-4-thiopheneacetic-5-carboxylic acid tetra ester (b) is carried out in the proper sodium hydroxide aqueous solution of alcohol for 5h to 6h and the pH value is kept over 10 during hydrolysis; (2) the ethanol of 20 per cent to 60 per cent is added and then the strontium chloride aqueous solution with 2times to 2.5times molal weight is directly added, precipitates the crystal, is filtered and dried; (3) water is added to carry out the reflux and the little salt packed in the crude product is removed, and the product is collected through heat filtration. The invention discloses the drug combination containing the strontium ranelate heptahydrate which is used for the treatment of osteoporosis of women after menopause.
Owner:TIANJIN INSTITUTE OF PHARMA RESEARCH

CaCu3Ti4O12 micro nano sized fiber and its preparation method

InactiveCN102515744AControl the hydrolysis processThe electrospinning process went smoothlyFilament/thread formingSpinning solutions preparationFiberCalcium nitrate tetrahydrate
The invention discloses a CaCu3Ti4O12 micro nano sized fiber and its preparation method, which belongs to the inorganic material technical field. The CaCu3Ti4O12 micro nano sized fiber comprises the elements of Ca, Cu, Ti and O with the mol ratio of 13412, and the diameter is 200-300 nanometers. The preparation method comprises the following steps mixing anhydrous ethyl alcohol, calcium nitrate tetrahydrate and copper acetate monohydrate to obtain a solution A; mixing anhydrous ethanol, butyl titanate and a spinning auxiliary agent to obtain a solution B; slowly adding the solution B in the solution A, and using a static spinning technology to prepare the CaCu3Ti4O12 micro nano sized fiber. The method of the invention can effectively control the hydrolysis process of the raw materials by selecting and adjusting the ratio of raw materials and the spinning auxiliary agent, the obtained static spinning solution possesses spinnability, and the method of the invention provides the novel CaCu3Ti4O12 micro nano sized fiber. The preparation method has the advantages of simple process, mild condition, easy control and wide applicability.
Owner:SUZHOU UNIV

Method for preparing glucosamine hydrochloride

The invention relates to a method for preparing glucosamine hydrochloride, which is characterized by comprising the following steps: 1) treatment of chitin in a gas explosion expanding method: feeding chitin as a raw material into a gas explosion expanding tank, and injecting a gas explosion expanding medium into the gas explosion expanding tank, wherein the gas explosion expanding medium is one of the four substances, namely, steam, water, ammonium hydroxide and ethanol; and instantly releasing the pressure of the gas explosion expanding tank, and discharging the raw material chitin into an atmospheric vessel, thereby obtaining chitin concentrate; 2) hydrolysis with hydrochloric acid; 3) decolorization; 4) filtration; 5) concentration and crystallization; and 6) secondary crystallization. Compared with the prior art, the invention has the following advantages that: 1) the chitin pretreated in the gas explosion expanding method is used as the raw material, and due to the high chemical activity thereof, the invention can achieve a higher product yield; 2) almost no 'coking' can be caused in the process of hydrolysis; 3) the extraction of GAH can be completed at one step during the technological process of technology, thereby simplifying the preparation of GAH; and 4) the hydrochloric acid can be recycled, thereby realizing the clean production of GAH.
Owner:汪昔奇 +1
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