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1537 results about "Coupling reagent" patented technology

To facilitate the coupling of the two amino acids, a peptide coupling reagent is used. There are several different kinds of coupling reagents, including carbodiimides, aminium, phosphonium, uronium and others. The most successful and widely used peptide synthesis methods use uronium or guandidium salts as their peptide coupling reagents.

Methods for refolding of recombinant antibodies

ActiveUS20060194280A1Efficient and economic productionImproved pharmaceuticalImmunological disordersFermentationRecombinant antibodiesCoupling reagent
The present invention is generally directed to methods of producing an increase in the enrichment or recovery of preferred forms of IgG proteins. More particularly, the invention relates to subjecting preparations of such recombinant IgG proteins with a reduction / oxidation coupling reagent and optionally a chaotropic agent.
Owner:AMGEN INC

Apparatus and method for easing use of a spectrophotometric based noninvasive analyzer

A placement guide apparatus with an improved hydration inducing plug used in coupling a noninvasive analyzer to a sampling site to determine analyte in the human body is disclosed. The hydration inducing plug includes at least one fluoropolymer that may be used as a coupling agent. The guide apparatus may further include an automated or semi-automated coupling fluid delivery system. Use of either of these couplers mitigates issues associated with related technology and enhances noninvasive analyte measurements, such as a near-IR diffuse reflectance based noninvasive glucose concentration analyzer.
Owner:GLT ACQUISITION

Tetrazine-based bio-orthogonal coupling reagents and methods

Coupling reactions, suitable for use in organic or aqueous media, are performed by contacting a 1,2,4,5-tetrazine with a dienophile. The dienophile may be covalently bonded to a protein, and the coupling reaction may be performed in biological media such as those containing cells or cell lysates. The reactions may be performed in the presence of primary amines, thiols, acetylenes, azides, phosphines, and products of Staudinger and / or Sharpless-Huisgen reactions Novel 3-substituted cyclopropene compounds and trans-cyclooctenes are exemplary dienophiles for these reactions.
Owner:UNIVERSITY OF DELAWARE

Blocked mercaptosilane coupling agents for filled rubbers

Disclosed herein is a blocked mercaptosilane selected from the group consisting of[[(ROC(═O))p—(G)j]k—Y—S]r—G—(SiX3)s; and  (1)[(X3Si)q—G]a—[Y—[S—G—SiX3]b]c  (2)whereinY is a polyvalent species (Q)zA(═E) selected from the group consisting of —C(═NR)—; —SC(═NR)—; —SC(═O)—; —OC(═O)—; —S(═O)—; —S(═O)2—; —OS(═O)2—; (—NR)S(═O)2—; —SS(═O)—; —OS(═O)—; (—NR)S(═O)—; —SS(═O)2—; (—S)2P(═O)—; —(—S)P(═O)—; —P(═O)(—)2; (—S)2P(═S)—; —(—S)P(═S)—; —P(═S)(—)2; (—NR)2P(═O)—; (—NR)(—S)P(═O)—; (—O)(—NR)P(═O)—; (—O)(—S)P(═O)—; (—O)2P(═O)—; —(—O)P(═O)—; —(—NR)P(═O)—; (—NR)2P(═S)—; (—NR)(—S)P(═S)—; (—O)(—NR)P(═S)—; (—O)(—S)P(═S)—; (—O)2P(═S)—; —(—O)P(═S)—; and —(—NR)P(═S)—; wherein the atom A attached to unsaturated heteroatom E is attached to the sulfur which in turn is linked via a group G to the silicon atom;each R is chosen independently from hydrogen, straight, cyclic, or branched alkyl that may or may not contain unsaturation, alkenyl groups, aryl groups, and aralkyl groups, with each R containing from 1 to 18 carbon atoms;each G is independently a monovalent or polyvalent group derived by substitution of alkyl, alkenyl, aryl, or aralkyl, wherein G can contain from 1 to 18 carbon atoms, with the proviso that G is not such that the blocked mercaptosilane would contain an α,β-unsaturated carbonyl that can undergo polymerization reactions, and if G is univalent, G can be a hydrogen atom;X is independently selected from the group consisting of —Cl, —Br, RO—, RC(═O)O—, R2C═NO—, R2NO—, R2N—, —R, and —(OSiR2)t(OSiR3) wherein each R is as above and at least one X is not —R;p is 0 to 5; r is 1 to 3; z is 0 to 2; q is 0 to 6; a is 0 to 7; b is 1 to 3; j is 0 to 1, but it may be 0 only if p is 1; c is 1 to 6; t is 0 to 5; s is 1 to 3; k is 1 to 2; with the provisos that (I) if A is carbon, sulfur or sulfonyl, then (i) a+b is 2 and (ii) k is 1; (II) if A is phosphorus, then a+b is 3 unless both (i) c is greater than 1 and (ii) b is 1, in which case a is c+1; and (III) if A is phosphorus, then k is 2.
Owner:GENERAL ELECTRIC CO

New macromolecule fiber composite material

The invention discloses a new macromolecule fiber composite material which is prepared by the following components in parts by weight, 40-100 parts of plant fiberfill, 60-100 parts of plastic base material, 3.5-5 parts of heat stabilizer, 1-2 parts of plasticizer, 1.6-2 parts of lubricating agent, 4-8 parts of modifying agent, 1-3 parts of compatilizer, 2-3 parts of coupling reagent, 1-5 parts of super dispersing agent, 1-4 parts of positive ion surface active agent, 1-1.8 parts of foaming agent, 1-5 parts of blowing promoter, 0.3-1.2 parts of antioxygen, 1-10 parts of cross-linking agent, 1-20 parts of nucleating agent, 0.8-1 part of viscosity reducer, 0.8-1 part of tackifier and 3.2-13.4 parts of other auxiliaries. The new composite material can not easily cause wet swelling and air shrinkage, and is low in expansibility and water absorbability, so that the prepared product has good stability.
Owner:GUILIN SHUKANG BUILDING MATERIAL

Piercing needle

A piercing needle having a low piercing resistance even if repeatedly caused to pierce is provided. The piercing needle has an undercoat of a silane coupling agent, preferably, an amino group-containing alkoxysilane or an epoxy group-containing alkoxysilane, and an outer surface of a mixture of a (1) reactive silicone such as a reaction product of an amino group-containing alkoxysilane, an epoxy group-containing alkoxysilane and a silicone having silanol groups at both terminal ends, with (2) a non-reactive silicone.
Owner:NIPRO CORP

Blocked mercaptosilane hydrolyzates as coupling agents for mineral-filled elastomer compositions

Rubber composition intended for the manufacture of tire casings which have improved hysteretic properties and scorch safety, based on at least one elastomer and silica by way of reinforcing filler enclosing a reinforcing additive consisting of the mixture and / or the product of in situ reaction of at least one functionalized polyorganosiloxane compound containing, per molecule, at least one functional siloxy unit capable of bonding chemically and / or physically to the surface hydroxyl sites of the silica particles and at least one functionalized organosilane compound containing, per molecule, at least one functional group capable of bonding chemically and / or physically to the polyorganosiloxane and / or the hydroxyl sites of the silica particles and at least one other functional group capable of bonding chemically and / or physically to the polymer chains.
Owner:GENERAL ELECTRIC CO

Methods for refolding of recombinant antibodies

The present invention is generally directed to methods of producing an increase in the enrichment or recovery of preferred forms of IgG proteins. More particularly, the invention relates to subjecting preparations of such recombinant IgG proteins with a reduction / oxidation coupling reagent and optionally a chaotropic agent.
Owner:AMGEN INC

Magnetic nanometer ion liquid composite particles as well as preparation method and application thereof

The invention discloses magnetic nanometer ion liquid composite particles as well as a preparation method and application of the magnetic nanometer ion liquid composite particles in removing pollutants in water bodies. The preparation method of the magnetic nanometer ion liquid composite particle comprises the following steps of: firstly synthesizing ferric oleate into magnetic Fe3O4 nanometer particles by taking ferric oleate as an iron source and adopting a chemical precipitation method; preparing nanometer nuclear shell type magnetic silicon dioxide with surface amino-functionalization by utilizing the nanometer magnetic particles as a kern, taking ethyl orthosilicate and a silane coupling agent as silicon sources, and utilizing a colloidal sol-gel method; and synthesizing a functionalized ion liquid by utilizing reaction between N, N-carbonyldimidazole (CDI) and an ion liquid containing carboxyl, and thus preparing the magnetic nanometer ion liquid composite particle by utilizing reaction between the functionalized ion liquid and amino on the surface of the magnetic nanometer silicon dioxide; and the method is used for removing pollutants in the water bodies. The method provided by the invention has the advantages that the operation is simple and convenient, the cost is low, the treatment process is simple, and the removal efficiency is high.
Owner:SOUTH CHINA UNIV OF TECH

Preparation method and usage of modified attapulgite adsorption material

The invention discloses a preparation method and usage of a modified attapulgite adsorption material. The method comprises the following steps: modifying attapulgite which has undergone purification and acid activation with an amino-silane coupling agent so as to introduce amino onto the surface of attapulgite; subjecting amino and excess acrylic acid ester to a Michael addition reaction so as tointroduce ester groups, subjecting introduced ester groups and polyethylene polyamine to a Michael addition reaction, carrying out underpressure distillation to remove a solvent and excess reactants,and carrying out vacuum drying, grinding and sieving to obtain a finished product. According to the invention, polyethylene polyamine or alcamine compounds are bonded to the surface of attapulgite through covalent bonds, thereby substantially improving adsorption performance of attapulgite to metal ions.
Owner:江苏麦阁吸附剂有限公司

Processes for producing coated magnetic microparticles and uses thereof

This invention relates generally to the field of production of coated magnetizable microparticles and uses thereof. In particular, the invention provides a process for producing coated magnetizable microparticles with active functional groups, which process uses, inter alia, conducting polymerization of said coating monomers on the surface of magnetic particle to form coated magnetizable microparticles with active functional groups in the presence of a coupling agent, coating monomers, a functionalization reagent, a cross-linking agent and an initiator in an organic solvent containing a surfactant. The coated magnetizable microparticles produced according to the present processes and uses of the coated magnetizable microparticles, e.g., in isolating and / or manipulating various moieties are also provided.
Owner:AVIVA BIOSCI

Moistureproof type low-smoke halogen-free flame-retarding wire and cable insulation material used for building

The invention discloses a moistureproof type low-smoke halogen-free flame-retarding wire and cable insulation material used for building. The insulation material comprises components, by weight, 100 parts of vinyl copolymer and / or ethylene propylene rubber, 100-250 parts of halogen-free flame retardants, 1-20 parts of compatilizer, 0.3-5 parts of antioxygen, 0.5-5 parts of lubricants, 0-3 parts of coupling reagents, 0-2 parts of dispersing agents, and 2-20 parts of one or more of vinyl silicone oil, silicone, silicone grease, silicone rubber, and mineral oil. Wires made of the material is low in smoke, free of halogen, incapable of releasing poisonous gas. Flames can be retarded due to the fact that a single stick of wire can vertically combust at combusting time. Moreover, some special addition agents are added in materials of insulation layers or protective sleeve layers, so that the surface hydrophobic property of products is increased and can be used in a high-temperature humid environment for a long time, and short circuit accidents caused by moisture absorption of the wire insulation layers are avoided.
Owner:SHENZHEN WOER HEAT SHRINKABLE MATERIAL +1

Hydrophilic block polyether amino silicone oil with amino branched chain, and preparation method and application thereof

InactiveCN104031269AStable working fluidThe reaction steps are simpleVegetal fibresDisiloxaneEpoxy
The invention discloses hydrophilic block polyether amino silicone oil with an amino branched chain and a preparation method thereof. The hydrophilic block polyether amino silicone oil with the amino branched chain has the following structure as shown in the specification, wherein R1 is represented by formulas shown in the specification. The preparation method comprises the following steps: carrying out mixing reaction of tetramethyl dihydro disiloxane, polysiloxane and concentrated sulfuric acid, neutralizing with anhydrous sodium carbonate, carrying out reduced pressure pumping to remove a low-boiling-point substance, and thus obtaining silicone oil with the end containing hydrogen; carrying out mixing reaction of the silicone oil with the end containing hydrogen, allyl epoxy polyether and a catalyst, and thus obtaining epoxy silicone oil; carrying out mixing reaction of the epoxy silicone oil, polyether amine and a solvent, and thus obtaining block polyether amino silicone oil; and carrying out mixing reaction of the block polyether amino silicone oil, a silane coupling agent hydrolysate and an alkali catalyst, neutralizing with glacial acetic acid, and thus obtaining the hydrophilic polyether amino silicone oil with the amino branched chain.
Owner:江阴市诺科科技有限公司

Preparation method of polyamide fiber with uvioresistant function

The invention relates to a preparation method of polyamide fiber with a uvioresistant function. The method comprises the following process steps: (1) grinding and mixing titanium dioxide, silicon dioxide and zinc oxide to obtain a mixture, and modifying the mixture by adopting a titanate coupling reagent so as to obtain a modified uvioresistant screening agent; (2) mixing the modified uvioresistant screening agent and polyamide slices, and performing melt extrusion pelleting in a twin-screw extruder so as to obtain uvioresistant master batches; (3) blending the uvioresistant master batches and the polyamide slices to obtain a mixture I, performing heating melting on the mixture I in the twin-screw extruder, and forming long polyamide yarns in an extruding manner from a yarn spraying port of a spinning manifold; (4) quenching and bundling the long polyamide yarns, so as to obtain yarn bundles, and performing primary tensioning, annealing and secondary tensioning on the yarn bundles so as to obtain the polyamide fiber. The polyamide fiber obtained by adopting the method has the good uvioresistant performance, and has the high wearing resisting performance.
Owner:WUXI TAIBO GARMENT

Preparation method of inorganic/organic hybridization antibacterial film

The invention relates to a preparation method of an inorganic / organic hybridization antibacterial film. The preparation method mainly comprises the steps of: (1) preparing a nano-silver-loaded molecular sieve germicide with stronger stability by ion exchange and a chemical reduction method; and preparing a molecular sieve / polymer hybridization antibacterial film loaded with nano-silver particles by a phase transformation film preparation process; and (2) taking N,N-dimethylformamide as a solvent and a reducing agent simultaneously, reducing silver ions to nano-silver serving as an antibacterial function body in a film casting liquid system in situ, and firmly loading the nano-silver in a polymer porous matrix material by a dispersion action and a coupling action of a coupling agent so as to form a nano-silver-loaded polymer porous film. The hybridization antibacterial film, provided by the invention, keeps excellent water flux, high retention rate and tough mechanical intensity, and has excellent antibacterial function, and can effectively solve the problems of loss of the silver ions of the silver-ion-loaded molecular sieve in the membrane filtration, loss of the nanometer inorganic particles in the polymer porous matrix, easy pollution of a separation film by microorganisms, and the like.
Owner:天津鼎芯膜科技有限公司

Textured surfaces for polynucleotide synthesis

Methods, devices and systems are provided herein for surfaces for de novo polynucleotide synthesis that provide for increased polynucleotide yield. Surfaces described herein comprise a texture that increases surface area provide for increased polynucleotide yield compared to non-textured surfaces. In addition, the patterned placement of nucleoside coupling reagent spanning such surfaces provides for improved synthesis yield, representation, and a reduction in contamination on the surface between different polynucleotide species.
Owner:TWIST BIOSCI

Magnetic nanoparticle-based immobilized laccase and ionic liquid composite particle and application thereof

The invention discloses a magnetic nanoparticle-based immobilized laccase and an ionic liquid composite particle, a preparation method thereof and application in removal of contaminants in water. The preparation method comprises the steps that carbonyl iron is taken as an iron source and is synthesized to be gamma-Fe2O3 nano-particles through a chemical precipitation method; the magnetic nanoparticles are taken as cores, tetraethoxysilane and a silane coupling agent are taken as a silicon source, and by means of a sol-gel method, surface amino-functionalized nano core-shell type magnetic silicon dioxide is prepared; 1-ethyl-(3-dimethyllaminopropyl) carbodiie hydrochlide is taken as a coupling agent, and laccase is bonded on the surface of the nano core-shell type magnetic silicon dioxide in a covalent bond manner to obtain the immobilized laccase of the magnetic nanoparticle silicon dioxide particles; and then the immobilized laccase is reacted with a functionalized ionic liquid which is synthesized by reacting N,N-carbonyldiimidazole and an ionic carboxy contained liquid to prepare the magnetic nanoparticle immobilized laccase and ionic liquid composite particle, and the composite particle is applied to the removal of the contaminants in water.
Owner:SOUTH CHINA UNIV OF TECH

Self-repairing microcapsule used for metal anticorrosive paint and preparation method thereof

The invention relates to the technical field of self-repairing anticorrosive paints and particularly relates to a self-repairing microcapsule used for a metal anticorrosive paint and a preparation method of the self-repairing microcapsule. The self-repairing microcapsule sequentially comprises a capsule core material and double layers of wall materials from inside to outside, a corrosion-inhibiting material is loaded between the double layers of wall materials, a coupling reagent is adhered on an outer wall of the double layers of wall materials, wherein the capsule core material is a reactant of a polyhydroxyl or multiamino compound and isocyanate, an inner wall of the double layers of wall materials is polyurethane, the outer wall of the double layers of wall materials is melamine formaldehyde resin, and the corrosion-inhibiting material is a nanoparticle and a metal corrosion inhibitor. The microcapsule is high in repairing efficiency, stable in mechanical property and simple in process, is matched with a matrix, has extensive applications, and can be widely applied to the fields of metal anti-corrosion and self-repairing materials like the petrochemical engineering, the marine industry and the automobile industry.
Owner:SHENYANG RES INST OF CHEM IND +1

Adsorbing substance for absorbing heavy metal ion and preparation method thereof

The invention discloses an adsorbent for adsorbing heavy metal ions, and the preparation method of the adsorbent. The invention is characterized in that a silane coupling agent and acid anhydride are in epoxy ring cleavage reaction in inert atmosphere or air at the temperature of minus 78 to 200 DEG C, wherein the mol ratio of the silane coupling agent to the acid anhydride is 1 : 2 to 20; after the reaction product is dissolved by a solvent, halogenated alkane is added to the solution according to the mol ratio of two to ten times of the silane coupling agent, the amination reaction is carried out at the temperature of 0 to 200 DEG C, and then, the product generated by the amination reaction is cleaned with water or ethanol and is dried to obtain the adsorbent for adsorbing the heavy metal ions. In the adsorbent, acidic groups are arranged on both sides of a molecular backbone, and basic groups are positioned on the molecular backbone. The adsorbent has stronger capability for adsorbing heavy metal ions, such as Pb2+, Cu2+ and the like in the solution, and can be used for adsorption separation and purification treatment of waste water containing heavy metal ions.
Owner:HEFEI UNIV

Apparatus and method for easing use of a spectrophotometric based noninvasive analyzer

A placement guide apparatus with an improved hydration inducing plug used in coupling a noninvasive analyzer to a sampling site to determine analyte in the human body is disclosed. The hydration inducing plug includes at least one fluoropolymer that may be used as a coupling agent. The guide apparatus may further include an automated or semi-automated coupling fluid delivery system. Use of either of these couplers mitigates issues associated with related technology and enhances noninvasive analyte measurements, such as a near-IR diffuse reflectance based noninvasive glucose concentration analyzer.
Owner:GLT ACQUISITION

Long glass fiber enhanced polypropylene composite material with low shrinkage and low warpage and preparation method and application thereof

The invention discloses a long glass fiber enhanced polypropylene composite material with low shrinkage and low warpage, a preparation method thereof, and application of the long glass fiber enhanced polypropylene composite material in manufacturing an automobile tail door sheet. The composite material is prepared from the following raw materials in parts by weight: 30-80% of polypropylene, 10-60% of continuous glass fiber, 3-10% of compatilizer, 0.1-1.5% of antioxidant, 0.1-1% of lubricating agent, 0.5-3% of coupling reagent, 0.1-2% of nucleating agent, 5-20% of zinc oxide whisker and 0.5-3% of glass bead. The zinc oxide whisker, the nucleating agent and the glass bead are compounded, so that the composite material achieves an ideal enhancement effect, the differential degree of glass fiber along a fiber glass orientation between a flowing direction and a vertical flowing direction in a polypropylene matrix is reduced, and the shrinking percentage and the warping degree of the composite material can be obviously lowered. The long glass fiber enhanced polypropylene composite material can be used for manufacturing the automobile tail door sheet.
Owner:CGN JUNER NEW MATERIALS +1

Quaternary amino cation modified polysiloxane softening agent and preparation method thereof

The invention relates to a quaternary amino cation modified polysiloxane softening agent and a preparation method thereof. The structural formula of the softening agent is A1BA2. The preparation method comprises the following steps: (1) mixing hydroxy silicone oil and silane coupling agent according to a molar ratio of 1:1-1:4, and carrying out reaction on the mixture for 4 to 24 hours at the temperature of between 25 and 105 DEG C to obtain an amino terminated siloxane intermediate; (2) carrying out reaction on the amino terminated siloxane intermediate and epoxy quaternary ammonium salt for 2 to 10 hours in a solvent under the protection of nitrogen during the whole reaction, and finally vacuumizing the mixture and removing partial solvent to obtain a sticky transparent modified polysiloxane product; and (3) diluting the modified polysiloxane product by water and organic acid to obtain transparent emulsion, and adding an emulsifying agent which is 5 to 10 percent of weight of the emulsion into the emulsion to obtain a product. Compared with the prior art, the softening agent has the advantages of good softness, fluffy feeling, hydrophilicity, extremely low yellowing property, and the like.
Owner:上海氟聚化学产品股份有限公司

Sulfoperoxycarboxylic acids, their preparation and methods of use as bleaching and antimicrobial agents

The present invention relates to novel sulfoperoxycarboxylic acid compounds, and methods for making and using them. The sulfoperoxycarboxylic compounds of the invention are storage stable, water soluble and have low to no odor. Further, the compounds of the present invention can be formed from non-petroleum based renewable materials. The compounds of the present invention can be used as antimicrobials, and bleaching agents. The compounds of the present invention are also suitable for use as coupling agents.
Owner:ECOLAB USA INC

Nanometer carboxylated polystyrene microsphere with spacer arm and preparation method thereof

The invention relates to a nanometer carboxylated polystyrene microsphere with a spacer arm and a preparation method thereof. A nanometer carboxylated polystyrene microsphere A is prepared by taking styrene and acrylic acid as a mixed monomer, taking water as a reaction medium, taking potassium persulfate as an initiator and taking sodium dodecyl sulfate as an emulsifier with an emulsion polymerization method. In the presence of EDC (Ethylidene Dichloride) serving as a coupling agent and Sulfo NHS, 4-aminobutyric acid, 6-amidocaproic acid or 8-aminocaprylic acid is connected to the surface of the microsphere, so that the nanometer carboxylated polystyrene microsphere with the spacer arm is prepared. The spacer arm is introduced into the surface of the nanometer microsphere, so that the steric hindrance of a coupling macromolecule is lowered, the activity and utilization ratio of the macromolecule are increased, and a nonspecific interaction between the macromolecule and the polystyrene microsphere is reduced. Meanwhile, the grain diameter of the microsphere can be adjusted by adjusting the using amount of the emulsifier, the length of the space arm and surface density, so that the nanometer microsphere has a wide application prospect in the fields of immune diagnosis, solid phase extraction and the like when serving as a carrier as well as a template.
Owner:TIANJIN MEDICAL UNIV

Preparation method and application of ionic liquid bonded silica adsorbent

The invention discloses a preparation method and an application of an ionic liquid bonded silica adsorbent. The preparation method takes silica as a carrier, takes 3-aminopropyltriethoxysilane as a coupling agent to synthesize alkylsilane epoxy silica, and reacted with ionic liquid like 1,3-di-n-butyl imidazole hexafluoride phosphate to obtain the ionic liquid bonded silica adsorbent; the ionic liquid is fixed on the solid phase carrier silica through a chemical modification mode, characteristics of the ionic liquid can be maintained, and the stability during the usage process can be substantially enhanced; thereby the analysis cost can be reduced, and the precision of the determination result can be improved. The ionic liquid adsorbent by the chemical modification possesses good adsorption function to the hydrophobic substances such as a heavy metal ion chelate, and is suitable for separation and enrichment of trace hydrophobic compounds in a water phase sample in the fields of environment, food and the like.
Owner:GUANGDONG UNIV OF TECH

Cold-stirring cold-paving type epoxy modified asphalt material and preparation method thereof

The invention discloses a cold-stirring cold-paving type epoxy modified asphalt material and a preparation method thereof. The cold-stirring cold-paving type epoxy modified asphalt material is composed of a main ingredient A and a curing agent B; the main ingredient A comprises the following components in parts by weight: 0-50 parts of epoxy resin, 40-90 parts of flexibilizer, 5-15 parts of reactive diluent, 10-40 parts of asphalt, 10-40 parts of active bulking agent and 0-5 parts of coupling reagent; the curing agent B comprises the following components in parts by weight: 0-100 parts of flexible curing agent, 0-100 parts of alicyclic amine curing agent and 0-10 parts of accelerant; and the ratio of the main ingredient A to the curing agent B is (1-5):1. The invention utilizes a self-assembly behavior of the active bulking agent on the surface of asphalt particles to solve the problem of compatibility between weak polar asphalt and strong polar epoxy resin. A flexible chain segment is introduced into an epoxy asphalt three-dimensional structure network by the flexibilizer and the flexible curing agent, so that the fatigue toughness of the epoxy asphalt material is greatly promoted and the secondary cracking phenomenon caused by insufficient toughness is effectively restrained.
Owner:JIANGSU SINOROAD TRANSPORTATION SCI & TECH CO LTD

Method for synthesizing silicon dioxide cladded organic-inorganic perovskite structure quantum dot and application of quantum dot synthesized by method

The invention relates to a method for synthesizing a silicon dioxide cladded organic-inorganic perovskite structure quantum dot and application of the quantum dot synthesized by the method, and belongs to the field of nano-material synthesis. The method comprises the following steps: taking methylammonium halide and lead halide as raw materials and taking oleic acid and an amino-containing silane coupling agent as ligands to synthesize the stable and efficient silicon dioxide cladded organic-inorganic perovskite structure quantum dot, which is capable of being processed in a solution, in one step through a solution method at room temperature. According to the method provided by the invention, the stability of the quantum dot is greatly increased through silicon dioxide cladding; meanwhile, high fluorescent quantum efficiency of the quantum dot is ensured and can reach 95 percent at maximum. Meanwhile, the quantum dot prepared by the method can be dispersed into solvents including toluene and the like to form a stable solution. A quantum dot solution and a toluene solution of polystyrene are mixed and can be used for preparing a warm white-light light emitting diode; the prepared white-light light emitting diode has a color coordinate (0.38, 0.43) and color temperature of 4500K, and can be applied to various fields including information storage, information encryption, counterfeiting prevention, illumination display and the like.
Owner:CHANGCHUN INST OF OPTICS FINE MECHANICS & PHYSICS CHINESE ACAD OF SCI

Preparation method for self-suspension propping agent in laboratory

The invention belongs to the technical field of yield increasing and fracturing of petroleum engineering and provides a method for preparing a self-suspension propping agent in a laboratory. The method comprises the following steps: taking quartz sand / ceramsite / propping agent as aggregates; pre-treating with an organic solvent and treating the surface with a coupling reagent; polymerizing and coating; and crushing, drying, pelletizing and then packaging. A coating polymerizing product (as shown in the figure) is acquired through the polybasic polymerization of the reactant and acrylamide / sodium acrylate / functional monomer / cross-linking agent. The expansion times of the prepared self-suspension propping agent is 3-12 times; the self-suspension propping agent can be completely hydrated within 1min-2min; the hydrated layer is stably expanded at 2 DEG C to 193 DEG C; the self-suspension propping agent swells once encountering with water, the volume density is reduced from 2.4g / cm3 to 1.3g / cm3 and the excellent self-suspension characteristic after the clean water system swelling is presented. The self-suspension propping agent prepared in the laboratory can realize the onsite mixing for hydraulic fracturing construction, the water for fracturing is greatly reduced, the labor cost is lowered and the application prospect is wide.
Owner:王展旭
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