Preparation method of inorganic/organic hybridization antibacterial film
An organic hybrid, antibacterial membrane technology, applied in chemical instruments and methods, membrane technology, semi-permeable membrane separation, etc. The effect of simple processing technology and less usage
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Embodiment 1
[0043] Common A-type (3A, 4A or 5A), X-type, and Y-type molecular sieves are used as silver-loaded substrates, with a particle size of 0.5-7 μm, and silver nitrate (AgNO 3 ) or silver perchlorate (AgClO 4 ) is the silver ion donor. The silver salt is configured as a 0.025mol / L aqueous solution, and a certain amount of any one of the above-mentioned molecular sieves is added to the silver salt aqueous solution, stirred mechanically at 50°C for 2h, and the obtained molecular sieve is washed with pure water, and dried at 80°C for 4h. Repeat the above steps twice to obtain the molecular sieve loaded with silver ions.
[0044] Configure 0.04mol / L sodium borohydride (NaBH 4 ) aqueous solution, the molecular sieve loaded with silver ions that takes a certain amount of preparation adds NaBH 4 In the aqueous solution, stir at 0°C for 20 minutes, wash the obtained molecular sieve with pure water, and dry at 80°C for 8 hours to obtain the molecular sieve loaded with nano-silver partic...
Embodiment 2
[0046] Polyvinylidene fluoride (PVDF) is used as the film-forming substrate (the mass fraction of PVDF in the casting solution system is 17%), and dimethylacetamide (DMAc) is used as the solvent (the mass fraction of DMAC in the casting solution system is 77%) , polyvinylpyrrolidone (PVP, the mass fraction in the casting solution system is 5%), the nano-silver 3A molecular sieve antibacterial agent prepared by example 1 and the silane coupling agent (KH550) are additives (the mass fraction in the casting solution system is respectively 0.5% and 0.5%), prepared as a spinning solution at room temperature. Using dry-wet spinning process, spinning through a circular porous spinneret with an air gap of 10 cm, passing through a coagulation bath at a certain temperature, and then guiding to the winding wheel through a guide wheel; after the film is cut into sections, it is bundled and immersed Wash with ultra-filtered water and store in 30% glycerol aqueous solution. The prepared an...
Embodiment 3
[0048] Polyacrylonitrile (PAN) is used as the film-forming substrate (mass fraction in the casting solution system is 17%), dimethylformamide (DMF) is the solvent (the mass fraction of DMF in the casting solution system is 76%), polyacrylonitrile Ethylene glycol (PEG, the mass fraction in the casting solution system is 5%), the nano-silver 4A molecular sieve antibacterial agent prepared by example 1 and the silane coupling agent (KH540) are additives (the mass fraction in the casting solution system is respectively 1% and 1%), prepared as a spinning solution at room temperature. With reference to the spinning process in Example 2, the prepared antibacterial hollow fiber membrane is an asymmetric structure, and the water flux is 200L / m at 0.1MPa operating pressure 2 h, the antibacterial rate against Escherichia coli and Staphylococcus aureus both reached 97%.
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