Application of multifunctional carbon quantum dot taken as fluorescent whitening agent
A fluorescent whitening agent and carbon quantum dot technology, which is applied in the field of fluorescent whitening agents, can solve problems such as poor light resistance, narrow application range, and poor mutual solubility, and achieve simple and effective synthesis methods, wide application fields, and whitening effects Good results
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Embodiment 1
[0045] A preparation of multifunctional carbon quantum dots using corn as a carbon source mainly includes the following steps:
[0046] Put 5 grams of seaweed into a beaker, add 1mL of 0.5mM NaOH aqueous solution, add 1mL of N,N-dimethylformamide, and mix well; transfer the well-mixed reaction solution into a microwave reactor, and control the reaction temperature at 200°C , react for 30 minutes, separate and purify after cooling, and obtain multifunctional water-soluble carbon quantum dots. (absorption spectrum such as figure 1 a, Fluorescence emission spectrum as figure 1 b, TEM as figure 2 ). Further experiments prove that the fluorescence intensity of the water-soluble carbon quantum dots does not change with temperature, illumination time and pH value (such as Figure 3-5 ), showing good heat resistance, light resistance, strong acid and alkali resistance and other excellent characteristics. The carbon quantum dots did not affect the normal growth of HeLa cells when...
Embodiment 2
[0050] A preparation of multifunctional carbon quantum dots using leaves as a carbon source mainly includes the following steps:
[0051] Put 50 grams of fresh green leaves into a beaker and add 50 mL of 10M H 2 SO 4 The aqueous solution is uniformly mixed; the uniformly mixed reaction solution is transferred to an ultrasonic reactor, the reaction temperature is controlled at 100°C, and the ultrasonic reaction is performed for 12 hours, separated and purified after cooling to obtain multifunctional water-soluble carbon quantum dots.
[0052] The application of the above-mentioned multifunctional carbon quantum dots prepared from leaves as a carbon source as a new type of fluorescent whitening agent in the washing industry:
[0053] When preparing detergent, add different amounts of carbon quantum dots (0-10%), according to the method of cycle washing, after washing pure cotton white cloth with detergent containing carbon quantum dots, carry out the test of cotton cloth whiten...
Embodiment 3
[0055] A preparation of multifunctional carbon quantum dots using citrus as a carbon source mainly includes the following steps:
[0056] Put 10 grams of fresh citrus into a beaker, mash it, add 50mL of 1M NaOH aqueous solution, add 10mL of methanol, and mix well; transfer the well-mixed reaction liquid into a hydrothermal reaction kettle, control the reaction temperature at 250°C, and react 1 Hours, separated and purified after cooling to obtain multifunctional water-soluble carbon quantum dots.
[0057] The application of the above-mentioned multifunctional carbon quantum dots prepared from citrus as a carbon source as a new type of fluorescent whitening agent in the textile industry:
[0058] The prepared carbon quantum dots are mixed with other dyeing agents (the mixing ratio is 2%). After the pure white cotton cloth is printed and dyed, the cotton cloth shows a higher whiteness (90%). At the same time, the cotton cloth is exposed to sunlight. Under irradiation, it has a ...
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