Relating to a preparation method and application of a novel
nanocomposite material, the invention provides a preparation method of a
mesoporous silica-restricted gold nanocluster-induced
fluorescence enhanced nano-fluorescent device and application of the same in
copper ion detection, and aims to solve the problems of high cost, complex process and long detection time in existing
copper ion detection methods. The method includes: 1. taking
chloroauric acid as the
raw material, adopting reduced
glutathione as the
reducing agent and stabilizer, and utilizing thermal reduction means to synthesize a gold nanocluster solution A from the bottom up under a high temperature stirring condition, loading the solution A into a centrifugal tube for
centrifugation, taking the precipitate, using a
mixed solution of
acetonitrile and water to perform washing 3 times and performing dissolving in deionized water to obtain a solution B; 2. making TEOS,
ethanol, water and
ammonia water into
solid silica particles by Stober process, washing and
drying the silica particles, then taking NaoH as the etchant, and performing sealed stirring overnight in a flask, then loading the obtained solution into a centrifugal tube for
centrifugation 3 times to remove the precipitate left by the supernatant, and performing washing and
drying to obtain
mesoporous silica; and 3. putting the
mesoporous silica into the solution B under a stirring condition so as to obtain the novel
nanocomposite material with
specific detection application in cooper ions. The
composite material prepared by the method has the characteristics of low cost, simple operation,
rapid detection and high sensitivity, and can be used in the fields of environmental
ion detection and bioimaging.