The invention provides a method for controlling
sintering densification and grain sizes of
metal materials. The method includes the steps that firstly,
raw material powder is deagglomerated, and deagglomerated
powder with good
dispersity is obtained. The deagglomerated
powder is subjected to
spray granulation, so that the flow performance of the powder and the density uniformity of a pressing blank are improved. The granulated powder is subjected to high-pressure pressing and cold isostatic forming. After the pressing blank is subjected to two steps of
pressureless sintering, high-density fine-grain
refractory metal is obtained. According to the first step of
sintering, the pressing blank is rapidly heated to the temperature T1, heat preservation is carried out, the density is controlled at 75-85%, then the pressing blank is reduced to the temperature T2, then time heat preservation is carried out, and residual holes are further eliminated. By means of the two steps of
sintering, the sintering temperature can be greatly reduced, almost full densification of the
metal blank can be achieved at low temperature, rapid growth of grains in the densification later period in the conventional sintering process can be effectively restrained, the prepared
refractory metal product is almost fully dense, the grains are fine, the grain sizes are evenly distributed, and the mechanical performance is excellent.