Preparation method of ZnO/g-C3N4 composite photocatalyst
A photocatalyst, g-c3n4 technology, applied in the direction of physical/chemical process catalysts, chemical instruments and methods, chemical/physical processes, etc., can solve the problem of not being able to fully play the role of energy level matching, easily forming agglomerated structures, reducing catalyst activity, etc. problem, achieve the effect of improving crystallinity, increasing dispersion and inhibiting agglomeration
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Embodiment 1
[0019] ZnO / g-C 3 N 4 The preparation adopts two-stage solvothermal-ultrasonic method. According to zinc acetate, ethanol, diethanolamine, g-C 3 N 4 Mass ratio = 1:10:20:1.5, mixed vigorously for 6 hours; then transferred the mixed system into a polytetrafluoroethylene-lined high-pressure reactor, reacted at 150°C for 24h, and at 190°C for 24h; after that, filtered, Ultrasonic dispersion (frequency 40KH Z , the power is 300W), washing, and repeating four times, the filter cake is dried and calcined at 500° C. for 2 h in an air atmosphere; it is ground into powder after cooling.
Embodiment 2
[0021] ZnO / g-C 3 N 4 The preparation adopts two-stage solvothermal-ultrasonic method. ZnO / g-C 3 N 4 Preparation according to zinc acetate, ethanol, diethanolamine, g-C 3 N 4 Mass ratio = 1:15:20:2.0, mixed vigorously for 8 hours; then transferred the mixed system into a polytetrafluoroethylene-lined high-pressure reactor, reacted at 130°C for 30h, and reacted at 180°C for 18h; then filtered, Ultrasonic dispersion (frequency 40KH Z , the power is 600W), washing, and repeating four times, the filter cake is dried and calcined at 500° C. for 1 h in an air atmosphere; it is ground into powder after cooling.
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