Preparation method of ZnO / g-C3N4 composite photocatalyst
A photocatalyst, g-c3n4 technology, applied in physical/chemical process catalysts, chemical instruments and methods, chemical/physical processes, etc., can solve problems such as weak composite structure, easy formation of agglomerated structure, and reduced catalyst activity, so as to improve Activity, increased crystallinity, enhanced separation effect
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Embodiment 1
[0019] ZnO / g-C 3 N 4 The preparation adopts two-stage solvothermal-ultrasonic method. According to zinc acetate, ethanol, diethanolamine, g-C 3 N 4 Mass ratio = 1:10:20:1.5, mixed vigorously for 6 hours; then transferred the mixed system into a polytetrafluoroethylene-lined high-pressure reactor, reacted at 150°C for 24h, and at 190°C for 24h; after that, filtered, Ultrasonic dispersion (frequency 40KH Z , the power is 300W), washing, and repeating four times, the filter cake is dried and calcined at 500° C. for 2 h in an air atmosphere; it is ground into powder after cooling.
Embodiment 2
[0021] ZnO / g-C 3 N 4 The preparation adopts two-stage solvothermal-ultrasonic method. ZnO / g-C 3 N 4 Preparation according to zinc acetate, ethanol, diethanolamine, g-C 3 N 4 Mass ratio = 1:15:20:2.0, mixed vigorously for 8 hours; then transferred the mixed system into a polytetrafluoroethylene-lined high-pressure reactor, reacted at 130°C for 30h, and reacted at 180°C for 18h; then filtered, Ultrasonic dispersion (frequency 40KH Z , the power is 600W), washing, and repeating four times, the filter cake is dried and calcined at 500° C. for 1 h in an air atmosphere; it is ground into powder after cooling.
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