Patents
Literature
Hiro is an intelligent assistant for R&D personnel, combined with Patent DNA, to facilitate innovative research.
Hiro

75 results about "Ethyl cyanoacrylate" patented technology

Ethyl cyanoacrylate (ECA), a cyanoacrylate ester, is an ethyl ester of 2-cyano-2-propenoic acid. It is a colorless liquid with low viscosity and a faint sweet smell in pure form. It is the main component of cyanoacrylate glues and can be encountered under many trade names. It is soluble in acetone, methyl ethyl ketone, nitromethane, and methylene chloride. ECA polymerizes rapidly in presence of moisture.

Guanine one-pot synthesis method

The invention discloses a synthesis method for guanine, which includes the following steps: carrying out a cyclization reaction of guanidine nitrate and ethyl cyanoacrylate to obtain the compound of 2, 4-diamino-6-hydroxypyrimidine in formamide solvent, adding sodium nitrite, formamide and concentrated formic acid in turn, and carrying out nitrosation and reduction reaction with reducing agent and cyclization reaction to obtain the final product. The invention is the use of ''one-pot'', and the raw materials are fat chain ethyl cyanoacrylate and guanidine nitrate, which are directly from market, cheap and easy to get, without need of separation and purification of pyrimidine intermediates. Guanine is prepared by one step through effective control of reaction conditions, feeding sequence and ratio. The product is purified through adjusting pH, which has high yield and is easy to operate.
Owner:SHANGHAI INST OF PHARMA IND

Polyethylene terephthalate composite material for 3D printing and preparation method thereof

The invention provides a polyethylene terephthalate composite material for 3D printing and a preparation method thereof. The preparation method of the composite material comprises the following steps of: dissolving polyethylene glycol into isopropanol; adding benzyl triethylamine bromide, and standing at room temperature; then sequentially adding benzoic anhydride and ethyl alpha-cyanoacrylate, and stirring at room temperature; then adding polyethylene terephthalate granules, heating, stirring, and cooling to room temperature to obtain the polyethylene terephthalate composite material for 3D printing, wherein the content of polyethylene terephthalate is 40%-50%, the content of ethyl alpha-cyanoacrylate is 5%-25%, the content of polyethylene glycol 4000 is 5%-20%, the content of isopropanol is 15%-30%, the content of benzyl triethylamine bromide is 1%-5%, and the content of benzoic anhydride is 1%-5%. The polyethylene terephthalate composite material prepared through the method provided by the invention can be used for 3D printing within a temperature range of 40-60 DEG C without plugging a spray head of a 3D printer.
Owner:TAICANG BIQI NEW MATERIAL RES & DEV

Heat resistance instant dry adhesive and preparation method thereof

The invention discloses a heat resistance instant dry adhesive and a preparation method thereof. The heat resistance instant dry adhesive comprises the following components in parts by weight: 80 to 90 parts of ethyl cyanoacrylate, 2 to 8 parts of ethyl cyanoacrylate, 2 to 6 parts of silica, 0.3 to 1 part of nitrobenzene, 0.5 to 2 parts of polyethylene glycol, 0.5 to 1 part of hydroquinone, 5 to 10 parts of polyvinyl acetate, 0.1 to 0.5 part of methanesulfonic acid and 0.05 to 0.1 part of sulfur dioxide. The preparation method comprises the following steps: adding the ethyl cyanoacrylate, the ethyl cyanoacrylate, the nitrobenzene, the hydroquinone, the polyvinyl acetate, the silica, the polyethylene glycol, the methanesulfonic acid and the sulfur dioxide into a reaction kettle; sufficiently stirring and uniformly mixing; heating to a temperature of 70 to 80 DEG C and performing the reaction for 50 to 80 minutes to be a paste state. The heat resistance instant dry adhesive provided by the invention can be rapidly gelled and meanwhile, also can achieve a good binding effect under high temperature conditions of 80 DEG C and 120 DEG C.
Owner:NANTONG REPAIR AIR CHEM BIOENG

Preparation method of hydrotalcite composite material for repairing soil of farmland with copper ions exceeding standard

The invention belongs to the field of soil repairing materials and relates to a preparation method of a hydrotalcite composite material for repairing soil of farmland with copper ions exceeding the standard. According to the preparation method, modified hydrotalcite is composited into holes of ammoniated bagasse, and the preparation method comprises specific processes such as cleaning of bagasse, ammoniation of the bagasse, modification of hydrotalcite, preparation of the composite material and the like. The bagasse and hydrotalcite composite material prepared with the method has the advantages as follows: (1) the hydrotalcite is fixed in the bagasse by the aid of ethyl cyanoacrylate, the characteristics of low density and large specific surface area of the bagasse can be realized, and the advantage that the modified hydrotalcite has high adsorption capacity for the heavy metal copper ions can also be utilized; (2) compared with hydrotalcite powder, the composite material solves problems of agglomeration of the hydrotalcite powder and reduction of adsorption capacity for the copper ions and can also solve the problem of secondary soil pollution due to the fact that the hydrotalcite adsorbing the copper ions is difficult to recover; (3) compared with the bagasse, the composite material has the advantage that the copper ion saturated adsorption amount of the soil repairing material is substantially increased.
Owner:TAICANG BIQI NEW MATERIAL RES & DEV

Preparation method for nano particle-modified polypropylene composite sheet

The invention discloses a preparation method for a nano particle-modified polypropylene composite sheet. The preparation method comprises the following steps: adding a modifying composition into a first extruding machine, and extruding at 90 to 120 DEG C to obtain a modified thin film; adding a polypropylene composition into a second extruding machine, and extruding at 220 to 240 DEG C to obtain a polypropylene foamed sheet; compounding the modified thin film and the polypropylene foamed sheet to obtain the nano particle-modified polypropylene composite sheet, wherein the modifying composition consists of ethyl cyanoacrylate, phenyl benzoate, sodium dodecyl sulphate, nano porous nickel oxide and tributyl phosphate; the polypropylene composition consists of homo-polypropylene, N-acyl-N-methyl glucamine, nanosilicon dioxide of which the surface is coupled with triethylamine, and a foaming agent. According to the preparation method, the compositions are molten by adopting simple extruding machines and are extruded to obtain a main body and a modifying body material; a composite plastic sheet is prepared by utilizing a multilayer compounding manufacturing method; the operation is easy and convenient; the produced composite sheet has the characteristics of good heat resistance, mechanical properties and the like.
Owner:JIN BAOLI TECH SUZHOU

Method for producing alpha-cyanoacrylate adhesive by continuous feeding

The invention relates to a method for producing an alpha-cyanoacrylate adhesive by continuous feeding, which comprises the following steps: pumping ethyl cyanoacetate and an organic solvent into a first mixer by a feeding pump respectively, conducting uniform mixing, and preheating the mixed material 1 by a heat exchanger to obtain a preheated material 1; and converging and mixing the preheated material 1 with formaldehyde and a basic catalyst entering through a feeding pump in a second mixer to obtain a mixed material 2, performing primary polycondensation reaction on the mixed material 2, and then performing polycondensation reaction to obtain an ethyl alpha-cyanoacrylate prepolymer with centralized molecular weight distribution. The method provided by the invention maintains a constantmolar ratio of ethyl cyanoacetate to formaldehyde in the reaction process. According to the invention, continuous feeding of raw materials in the synthesis stage of the ethyl alpha-cyanoacrylate prepolymer is realized, the homogeneity of the polymerization degree of the ethyl alpha-cyanoacrylate prepolymer is improved, the depolymerization temperature range of the ethyl alpha-cyanoacrylate prepolymer is reduced, the energy consumption in the production process is reduced, and the yield and the production efficiency of the product are improved.
Owner:山东禹王和天下新材料有限公司

Composite medical pressure-sensitive adhesive and preparation method thereof

The invention provides a composite medical pressure-sensitive adhesive and a preparation method thereof. The composite medical pressure-sensitive adhesive comprises the following components: alpha-cyan ethyl acrylate, dibutyl phthalate, methacrylic acid, alginate, a cissampelos pareira extract and sweetgum resin, wherein the cissampelos pareira extract is extracted by adding water into a crude cissampelos pareira material to extract, concentrating, adding ethanol until the volume concentration of ethanol is 40-60%, filtering to obtain the supernate, and by recycling the ethanol until the volume concentration of the ethanol is less than 2-5%. The preparation method comprises the following steps: mixing and smelting alpha-cyan ethyl acrylate, dibutyl phthalate and methacrylic acid in an open mill, adding alginate, the cissampelos pareira extract and the sweetgum resin, continuously smelting until the components are uniformly dispersed, and vulcanizing by using a press vulcanizer, thereby obtaining the composite medical pressure-sensitive adhesive of requested thickness. Compared with the prior art, the composite medical pressure-sensitive adhesive has the advantages of good mechanical property, good biocompatibility, good injury heal promotion effect and the like.
Owner:SUZHOU BEC BIOLOGICAL TECH

Building insulation coating and its preparing method

InactiveCN104725912AImprove insulation effectExcellent other physical and chemical propertiesCoatingsSarcosineEthyl acetate
The invention discloses building insulation coating. The building insulation coating comprises diatomite, light calcium carbonate, bentonite, ethylene carbonate, 2-cyanoacrylate, triethyleneglycolmonoethylether, hydroxypropyl methyl cellulose, N-oleo sarcosine octadecyl amine, silicon dioxide, and ethyl acetate. The preparing method includes: adding the diatomite, the bentonite, the hydroxypropyl methyl cellulose, the N-oleo sarcosine octadecyl amine and the silicon dioxide into water, performing periodic heating and stirring, drying mixed liquid to obtain solid, crushing the solid, adding the crushed solid into mixed liquid of the ethylene carbonate, the 2-cyanoacrylate and the ethyl acetate, performing heating and stirring in a reflow device, and allowing cooling to room temperature after reflowing; adding the remaining components, and performing stirring at the room temperature before grinding so as to obtain the building insulation coating. The building insulation coating has good thermal insulation, good impact strength and good other physical and chemical characteristics and is widely applicable to the field of coating insulation.
Owner:李孟平

Sample preparation method and mold for peel strength test on coated fabric

ActiveCN107389399ASolve the shortcomings that cannot reflect the real strengthPreparing sample for investigationEthyl cyanoacrylateAdhesive
The invention discloses a sample preparation method and a sample preparation mold for a peel strength test on coated fabric. An adhesive adopted in a gluing and conglutination step in a sample preparation process is a single-componnet moisture-cured adhesive; ethyl cyanoacrylate is contained in the single-componnet moisture-cured adhesive; the compaction and the curing are carried out by adopting a sample preparation compaction mold in a compaction and curing step in the sample preparation process; the sample preparation compaction mold comprises a base and a gland which can be put together in a covering manner; multiple compaction grooves which are arranged in parallel are processed in the upper surface of the base; the tops of the compaction grooves are open; certain end surfaces of the compaction grooves are open; the lower surface of the gland is provided with multiple press heads correspondingly matched with the compaction grooves in a one-to-one correspondence manner. The sample preparation method provided by the invention can effectively keep the peel strength of a coating changeless, can be further used for the test, is applicable to the preparation of a test sample for the T-shaped peel strength of most coated fabric, and is especially applicable to PU (Polyurethane) and PVC (Polyvinyl Chloride) coated fabric.
Owner:中央军委后勤保障部建筑工程研究所

Method for sealing tenon on instrument shell

The invention provides a method for sealing a tenon on an instrument shell. According to the method, a quick dry adhesive with Alpha-ethyl cyanoacrylate as a main component is applied into a gap between a flight parameter recorder shell and the tenon so as to achieve the aims of sealing and preventing liquid wax from flowing out. After the method is adopted, even if burning happens, since an adhesive layer in the gap is rapidly carbonized to form a solid blockage, the sealing function does not fail, so that electronic elements are effectively protected; the adhesive layer is not corroded when being soaked in seawater, therefore the protection time is prolonged and consequently the precious time is prolonged for search and rescue work.
Owner:SHAANXI BAOCHENG AVIATION INSTR
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products