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1610results about How to "Mild process conditions" patented technology

Integral recycling method of lithium iron phosphate positive electrode material

The invention provides an integral recycling method of a lithium iron phosphate positive electrode material. The integral recycling method comprises the steps of (1) preparing paste from the lithium iron phosphate positive electrode material, mixing the paste and an acid for leaching reaction, and performing liquid-solid separation to obtain a leaching liquid and residue; (2) adjusting a pH valueof the leaching liquid to 1.5-3, and performing solid-liquid separation to obtain iron phosphate and a deironing acid liquid; (3) adjusting a pH value of the deironing acid liquid to 5-8, and performing solid-liquid separation to obtain a precipitant of aluminum and iron and a lithium-containing purification liquid; and (4) and performing post-treatment on the purification liquid to obtain a lithium product and a precipitation mother liquid. By the method, the recycling rates of lithium, iron and phosphate all are larger than 95wt%, the purity of the obtained lithium carbonate product is larger than 98.5wt%, the impurity content conforms to the requirement of GB/T11075-2013, the iron phosphate product conforms to the quality requirement (HG/T 4701-2014) of battery-level iron phosphate, theresidue discharging quantity is reduced by 85wt%, the flow is simple, and the process is clean.
Owner:北京中科百特科技有限公司

Method and system for denitrifying low-carbon high-nitrogen sewage by utilizing plant carbon source-enhanced artificial wetland

The invention discloses a method and a system for denitrifying low-carbon high-nitrogen sewage by utilizing a plant carbon source-enhanced artificial wetland. The method comprises the following steps: hydrolyzing by taking waste crops or wetland plant straws as carbon sources, and charging hydrolysate into an artificial wetland so as to improve the denitrification efficiency of the low-carbon high-nitrogen sewage. The invention simultaneously provides a treatment system, which is simple in structure, and scientific and reasonable in carbon source charging mode, and the denitrification effect of the low-carbon high-nitrogen sewage can be well realized by enhancing the artificial wetland through utilizing the plant carbon source. According to the method, the adopted plant carbon sources are cheap and easily available, the carbon release capability is strong, the bio-denitrification effect is good, and the hydrolysate is simple and practical to prepare, the carbon source charging mode is strong in continuous running capability, and the method is simple to maintain, less in secondary pollution, low in production cost, and capable of solving the technical difficulty of treating tail water in a sewage treatment plant with low carbon nitrogen ratio through artificial wetland by utilizing a simple method.
Owner:JINAN UNIVERSITY

Method for removing sulfur in petroleum coke and desulfurizer thereof

The invention relates to a method for removing sulfur in petroleum coke and a desulfurizer thereof. The method adopts two types of mixed acid with a fixed ratio controlled as the desulfurizer, and comprises the following steps: placing fine petroleum coke with a high S content (the S content being 3-7 percent) in the mixed acid under the atmospheric pressure and the temperature of 0-60 DEG C, soaking the petroleum coke for reaction for a certain time, separating the petroleum coke and the soaking solution, washing and drying. The desulfurization percent of the obtained petroleum coke is 45-60 percent, the microstructure of the petroleum coke is not changed obviously, and the separated soaking solution of mixed acid can be repeatedly used when being mixed with the newly prepared liquid. The method has the advantages of low desulfurization cost, simple operation and significant desulfurization effect.
Owner:CENT SOUTH UNIV

Carbon dot/carbon nitride/titanium dioxide composite material as well as preparation method and application of the composite material

The invention discloses a carbon dot / carbon nitride / titanium dioxide composite material which is formed by compounding of three-phase carbon dots, graphene-like carbon nitride and titanium dioxide, wherein carbon nitride has a large surface area so as to just provide a depositing space for titanium dioxide nanosheets, so that titanium dioxide cannot cluster; and meanwhile, carbon nitride has relatively narrow energy gap and can increase the light response range. Furthermore, compounding of photo-induced electrons can be further inhibited by utilizing the unique electron transfer capacity of carbon dots, so as to increase the photocatalytic capacity. Moreover, the preparation method is mild in process conditions and low in cost, and the composite material is suitable for large-scale production, and has wide application prospect.
Owner:HUAZHONG AGRICULTURAL UNIVERSITY

Enzymatic extraction method for auricularia auricula polysaccharides

The invention discloses an enzymatic extraction method for auricularia auricula polysaccharides, which comprises the following steps of: mechanically and coarsely grinding dried auricularia auricula, sieving, mixing according to a material-to-water ratio of 1:(50-200), and extracting at the temperature of between 35 and 50 DEG C and the pH of between 5.0 and 9.0 under the action of chitinase for 60 to 180 minutes, wherein the addition amount of the chitinase is 100 to 600U/g; raising the extraction temperature to be between 80 and 95 DEG C, extracting for 60 to 180 minutes to obtain extract, and centrifuging to obtain supernatant and precipitates; and adding ethanol into the supernatant to precipitate polysaccharides, performing centrifugal separation to obtain precipitates, dissolving the precipitates in water, concentrating to remove residual ethanol, adding a mixture of diatomite and activated carbon into concentrated solution, mixing, fully stirring, filtering, performing membrane filtration on filtrate by using a polysulfone membrane of 30 to 100kD, collecting macromolecular concentrated solution which does not filter through the membrane, and drying the macromolecular concentrated solution to obtain the auricularia auricula polysaccharides. The prepared products have high purity and bioactivity; and the polysaccharide content is over 40 percent.
Owner:CHINA JILIANG UNIV

Biochemical joint preparation method and application of absolute rose oil

The invention provides a biochemical joint preparation method and application of absolute rose oil. The preparation method comprises the steps that coarse rose powder is prefermented by beta-glucosidase, amylase and cellulase to generate aroma, reflux extraction is conducted for 3-5 h with an aqueous solution the pH value is regulated to be 9-14, a Maillard reaction is conducted for 3-5 h, suction filtration is conducted, filtrate is retained, an ethanol solution is added into filter residues for secondary reflux extraction, suction filtration is conducted, filtrate is retained, the filtrates obtained in two times of suction filtration are mixed, concentration and alcohol precipitation are sequentially conducted, and a rose extract is obtained; the rose extract is purified through molecular distillation, light components are retained, heavy components are purified through molecular distillation again, the light components are mixed, and the purified absolute rose oil is obtained. The absolute rose oil has purer and richer aroma and fewer impurities, and the irritation is reduced. When the absolute rose oil is applied to reconstituted tobaccos, the color and luster of the reconstituted tobaccos is more natural and uniform, the aroma can be enriched, irritation and offensive odor can be reduced, and the sensory quality can be improved; when the absolute rose oil is applied to a novel tobacco product atomizing agent, the aroma is enriched, the noble rose note is improved, and the tobacco aroma is increased.
Owner:HUBEI CHINA TOBACCO IND

Natural fiber reinforced polylactic acid composite material having functionalized DOPO flame retardant and method for preparing same

The invention belongs to the technical field of material, and specially relates to a functionalized DOPO flame retardant polylactic acid and a method for preparing the same. The preparation method comprises a step of preparing the functionalized DOPO, a step of mixing the functionalized DOPO, the polylactic acid, a anti-oxidant and a anti-dripping agent, and a step of extruding the mixture and a natural fiber with blending in a twin-screw extruder to get the biodegradable natural fiber reinforced polylactic acid composite material having the functionalized DOPO flame retardant. The composite material has relatively good flame retardation performance, and can maintain or improve mechanical properties of materials with respect to pure polylactic acid. The preparation method is simple and effective, mild in technology condition and suitable for mass production.
Owner:TONGJI UNIV +1
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