669results about How to "Improve crystal structure" patented technology

The invention relates to a nickel cobalt manganese lithium oxide material used for an anode of a li-ion battery and a preparation method. The invention belongs to the li-ion battery technical field. The nickel cobalt manganese lithium oxide material used for the anode of the li-ion battery is a li-rich laminated structure with the chemical component of Li1+zM1-x-yNixCoyO2; wherein, z is less than or equal to 0.2 and more than or equal to 0.05, x is less than or equal to 0.8 and more than 0.1, and y is less than or equal to 0.5 and more than 0.1. The preparation method of the invention is that dissoluble salt of the nickel, cobalt and manganese is taken as the raw material; ammonia or ammonium salt is taken as complexing agent; sodium hydroxide is taken as precipitator; water-dissoluble dispersant and water-dissoluble antioxidant or inert gas are added for control and protection; in a cocurrent flow type the solution is added to a reaction vessel for reaction; after alkalescence disposal, aging procedure, solid-liquid separation and washing and drying, the nickel cobalt manganese oxide is uniformly mixed with the lithium raw material; the nickel cobalt manganese lithium oxide powder is obtained by sintering the mixed powder which is divided into three temperature areas. The invention has the advantages of high specific capacity, good circulation performance, ideal crystal texture, short production period, low power loss, and being suitable for industrial production, etc.

The invention provides an Al-Fe-C-RE aluminium alloy and a preparation method thereof. The preparation method comprises the following steps of: a) casting an aluminium alloy cast ingot; b) homogenizing the aluminium alloy cast ingot and rolling the homogenized aluminium alloy cast ingot to obtain an aluminium alloy rod material; c) intermittently annealing the aluminium alloy rod material obtained in the step b); and d) aging the aluminium alloy rod material obtained in the step c), thus obtaining the aluminium alloy. The invention also provides a power cable. The aluminium alloy has better overall performances by selecting and controlling the added elements and adopting a reasonable preparation process.

The invention provides an Al-Fe-Sb-RE aluminum alloy, and a preparation method of the Al-Fe-Sb-RE aluminum alloy. The method comprises the steps that: (a) an aluminum alloy ingot is cast; (b) the aluminum alloy ingot is subjected to a homogenization treatment; and the obtained aluminum alloy ingot is rolled, such that an aluminum alloy rod material is obtained; (c) the aluminum alloy rod material obtained in the step (b) is subjected to a batch-type annealing treatment; and (d) the aluminum alloy rod material obtained in the step (c) is subjected to an aging treatment, such that aluminum alloy is obtained. The invention also provides a power cable. According to the invention, through the selection and control over added elements and the adoption of a reasonable preparation process, the obtained aluminum alloy is provided with good comprehensive performance.

The invention discloses a preparation method of a prussian blue complex / carbon composite material and an application of the composite material as a positive electrode material for lithium ion and sodium ion batteries. The preparation method of the prussian blue complex / carbon composite material comprises at least the steps of uniformly dispersing a transition metal cyano complex, an inorganic acid and a carbon material in water to obtain a reaction solution; and heating the solution for a certain time to obtain the prussian blue complex / carbon composite material. The method is simple in preparation, can be controlled easily and has high practical degree. Crystal water content and coordinated water content in the obtained prussian blue complex / carbon composite material are little, so that the prussian blue complex / carbon composite material presents high capacity and excellent cycle performance when being used as the positive electrode material for the lithium ion and sodium ion batteries.

The invention relates to a method for peeling a laminar inorganic material quickly. The method comprises the following steps of: firstly, preparing laminar inorganic intercalating composite of the laminar inorganic material; secondly, decomposing or evaporating the inter-laminar organic material of the organic intercalating composite solid of the laminar inorganic material in a short time in the presence of microwaves and allowing the inter-laminar organic material to escape from the space between the layers of the laminar inorganic material so as to quickly peal the laminar inorganic material; and finally, performing separation, washing, drying and grinding to obtain the products. The method not only can peal the laminar inorganic material in a short time but also keep a good crystal structure of the laminar inorganic material, so the application of the laminar inorganic material is substantially widened and the use value thereof is multiplied.

Provided is a tantalum sputtering target having a crystal structure in which the (222) orientation is preferential from a position of 10% of the target thickness toward the center face of the target, and a manufacturing method of a tantalum sputtering target, including the steps of forging and recrystallization annealing, and thereafter rolling, a tantalum ingot or billet having been subject to melting and casting, and forming a crystal structure in which the (222) orientation is preferential from a position of 10% of the target thickness toward the center face of the target. As a result, evenness (uniformity) of the film is enhanced, and quality of the sputter deposition is improved.

The invention provides an Al-Fe-Sn-RE aluminum alloy, and a preparation method of the Al-Fe-Sn-RE aluminum alloy. The method comprises the steps that: (a) an aluminum alloy ingot is cast; (b) the aluminum alloy ingot is subjected to a homogenization treatment; and the obtained aluminum alloy ingot is rolled, such that an aluminum alloy rod material is obtained; (c) the aluminum alloy rod material obtained in the step (b) is subjected to a batch-type annealing treatment; and (d) the aluminum alloy rod material obtained in the step (c) is subjected to an aging treatment, such that aluminum alloy is obtained. The invention also provides a power cable. According to the invention, through the selection and control over added elements and the adoption of a reasonable preparation process, the obtained aluminum alloy is provided with good comprehensive performance.

The invention provides an Al-Fe-Re-RE aluminum alloy, and a preparation method of the Al-Fe-Re-RE aluminum alloy. The method comprises the steps that: (a) an aluminum alloy ingot is cast; (b) the aluminum alloy ingot is subjected to a homogenization treatment; and the obtained aluminum alloy ingot is rolled, such that an aluminum alloy rod material is obtained; (c) the aluminum alloy rod material obtained in the step (b) is subjected to a batch-type annealing treatment; and (d) the aluminum alloy rod material obtained in the step (c) is subjected to an aging treatment, such that aluminum alloy is obtained. The invention also provides a power cable. According to the invention, through the selection and control over added elements and the adoption of a reasonable preparation process, the obtained aluminum alloy is provided with good comprehensive performance.

The invention provides Al-Fe-Ir-RE aluminum alloy, and also provides a preparation method of the Al-Fe-Ir-RE aluminum alloy. The preparation method comprises the following steps of: a) casting an aluminum alloy ingot; b) homogenizing the aluminum alloy ingot, and rolling the homogenized aluminum alloy ingot to obtain an aluminum alloy rod; c) intermittently annealing the aluminum alloy rod obtained in the step b); and d) performing aging treatment on the aluminum alloy rod obtained in step c) to obtain the aluminum alloy. The invention further provides a power cable. According to the invention, the aluminum alloy has a good comprehensive performance by choosing and controlling added elements and adopting a reasonable preparation process.

The invention provides a preparation method of a vanadium sodium fluophosphate cathode material of a hybrid ion battery. The method comprises the following steps: 1) grinding of a mixed material: taking trivalent or pentavalent vanadium oxide (V), ammonium dihydrogen phosphate (P), sodium fluoride (F) and a reducing agent carbon source (C) as raw materials, wherein the molar ratio of V to P to F is 2:(1.9-2.3):3, the molar ratio of V to C in the reducing agent carbon source is 1:(1-2), then weighing carbon source accounting for 3-5% of the total weight of the raw materials to serve as a conductive agent, and carrying out mixed grinding to obtain a precursor mixture; 2) precalcination: precalcinating the precursor mixture for 6-10 hours at the temperature of 300-400 DEG C at the warming speed of 3-5 DEG C per minute under the protection of inert gas, cooling the mixture to room temperature and taking out the mixture for secondary grinding; and 3) secondary calcination: carrying out the secondary calcination on the mixture ground in the step 2) for 6-10 hours at the temperature of 550-750 DEG C at the warming speed of 3-5 DEG C per minute under the protection of the inert gas, and naturally cooling to room temperature to obtain the vanadium sodium fluophosphate cathode material. The vanadium sodium fluophosphate cathode material has good electrochemical performance which is obviously improved.