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33results about How to "Cross-linking reaction is sufficient" patented technology

Preparation method of cellulose microsphere adsorbent

The invention discloses a preparation method of a cellulose microsphere adsorbent, and relates to the field of chemical engineering and environmental protection. The preparation method of the cellulose microsphere adsorbent comprises the steps that cotton straw is cleaned, drying and smashing are performed and then mixed liquid of xylene and ethyl alcohol is added, the mixture reacts in a boiled water bath, and is subjected to washing and suction filtration, a hydrochloric acid solution is added to treat the product, deionized water is added to conduct a water bath reaction, suction filtrationis conducted, and the product is dried for stand-by application; a solution A is added into the pre-treated cotton straw powder to react mutually, after suction filtration and drying are conducted, asolution B is added to react with the product, the product is washed and dried to obtain cotton straw cellulose, the cotton straw cellulose is prepared to be a water solution for stand-by application; semen ricini oil and twain 80 are added into a beaker and stirred for 20 minutes, the cotton straw cellulose water solution is added into the beaker to react with the semen ricini oil and twain 80,and then epoxy chloropropane is added into the beaker to react with mixture; and the oil phase is removed from the reacted system, the product is washed and dried, and the cellulose microsphere adsorbent is obtained. The prepared cellulose microsphere adsorbent has the good adsorption effect on active blue M and metal ions Cr<6+> and Cu<2+> in the wastewater, and has the wide application prospect.
Owner:管敏富

Non-ironing fabric with high hang-dry appearance and manufacturing method thereof

ActiveCN110219172AImprove moisture wrinkle resistanceImproves wrinkle recovery performanceSucessive textile treatmentsWrinkle resistant fibresBuffering agentEngineering
The invention provides non-ironing fabric with a high hang-dry appearance and a manufacturing method thereof. The manufacturing method includes padding the fabric in non-ironing finishing liquid, andstoring the padded fabric in an environment with the temperature of 28-40 DEG C and the humidity of 20-70% for 6-15 hours, wherein the non-ironing finishing liquid comprises a resin crosslinking agentand an acid-base buffering agent; performing steaming treatment at 80-150 DEG C for 2-8 minutes to obtain the non-ironing fabric with the high hang-dry appearance. The non-ironing fabric produced bythe manufacturing method has the high hang-dry appearance under the condition of enough power.
Owner:GUANGDONG ESQUEL TEXTILES

Nylon 66 composite material for connecting rod sleeve and preparation method thereof

The invention discloses a nylon 66 composite material for a connecting rod sleeve. The nylon 66 composite material is prepared from raw material components such as a PA66 base material, carbon fiber,an interfacial compatibilizer, a dispersant, a chain extender, carbon black, an anti-wear agent and an additive; the obtained nylon 66 composite material is light in specific weight, has very strong designability, not only is easy to mould, but also is uniform in material after moulding, and has various significantly improved properties in lubricity, wear resistance, impact resistance, high temperature resistance, corrosion resistance, ageing resistance and the like. In addition, by a preparation method of the nylon 66 composite material, provided by the invention, the raw material mixing sequence is clarified, and especially after the carbon fiber is mixed with the specific interfacial compatibilizer and the matching dispersant in a dry state, melt extrusion is performed through a single-screw extruder and then feeding is performed through a side feed port, so that processing damage such as surface burring and easy tearing and layering due to addition of the carbon fiber is solved, performance advantages of the carbon fiber are fully played, the preparation limitation is broken through, and thus the high strength and the high performance of the nylon 66 composite material are guaranteed.
Owner:烟台恒大聚合体有限公司

High-stability micelle type water-soluble quantum dot for coupling of macromolecular proteins

The invention relates to a high-stability micelle type water-soluble quantum dot for coupling of macromolecular proteins. The high-stability micelle type water-soluble quantum dot has a typical core-shell structure, a hydrophobic inner core of the high-stability micelle type water-soluble quantum dot is composed of an oil-soluble quantum dot and a hydrophobic block of a tri-block amphiphilic polymer, and a crosslinking layer and a hydrophilic layer of the tri-block amphiphilic polymer are respectively composed of a crosslinking block and a hydrophilic block of the tri-block amphiphilic polymer. Since the crosslinking block contains a hydroxyl group and has hydrophily before crosslinking, crosslinking reaction can be generated in a water-phase environment after micelle formation, and a covalent bond network surrounding the hydrophobic inner core is formed, so that the stability of the high-stability micelle type water-soluble quantum dot is comprehensively increased; meanwhile, the tailend of a hydrophilic segment of the tri-block amphiphilic polymer is terminated by functional groups except the hydroxyl group, and the high-stability micelle type water-soluble quantum dot can be used for coupling of various macromolecular proteins. Since the high-stability micelle type water-soluble quantum dot has extremely high stability, the high-stability micelle type water-soluble quantumdot is particularly suitable for coupling and fluorescent labeling of the macromolecular proteins.
Owner:刘宏飞

A kind of preparation method of surface metallized aramid fiber

The invention provides a method for preparing surface metallization aramid fibers. The method includes steps of 1, carrying out aramid surface treatment, to be more specific, removing oil from aramidfibers, cleaning the aramid fibers, then placing the aramid fibers in melamine formaldehyde resin prepolymer solution, treating the aramid fibers at the temperatures of 20-80 DEG C for 5-60 s, then taking out the aramid fibers, mangling moisture on the surfaces of the aramid fibers and drying the aramid fibers; 2, carrying out activation, to be more specific, immersing the aramid fibers, which aretreated at the step 1, in activation solution, carrying out surface activation treatment on the aramid fibers and then removing residual solution on the surfaces of the aramid fibers by water; 3, carrying out reduction, to be more specific, placing the aramid fibers in reducing agents capable of reducing metal ions in the activation solution after the activation treatment is carried out on the aramid fibers, carrying out room-temperature reaction for 1-5 min, then rinsing the aramid fibers by water and drying the aramid fibers; 4, carrying out chemical plating, to be more specific, placing the reduced aramid fibers in plating solution, carrying out chemical plating on the aramid fibers, taking out the aramid fibers after the chemical plating is completely carried out on the aramid fibersand washing and drying the aramid fibers. The method has the advantages that the method is simple, feasible, safe, reliable, ecological and environmentally friendly and is convenient to operate, and large-scale production can be facilitated; the surface metallization aramid fibers prepared by the aid of the method are small in density, high in strength and good in electric conductivity, and the like.
Owner:CHINA BLUESTAR CHENGRAND CO LTD

Zinc oxide resistor disc end surface welding agent

The invention relates to the field of welding auxiliaries, in particular to a zinc oxide resistor disc end surface welding agent which comprises the following components in parts by weight: 20-30 parts of polyaniline nanofibers, 100-180 parts of an organic solvent, 20-25 parts of conductive inorganic nonmetal filler, 20-25 parts of conductive metal filler, 100-150 parts of thermosetting resin, 10-60 parts of a curing agent and 5-30 parts of an accelerant. By utilizing the synergistic effect between the polyaniline nanofibers and the graphene, the graphene can provide a conductive skeleton for the polyaniline nanofibers, and the polyaniline can improve the stability of the graphene; the thermosetting resin has good processability and is easily mixed with the curing agent, the conductive filler and the like, so that the conductive filler is uniformly distributed in the welding agent and is tightly attached to the surface of an aluminum layer of a resistor disc after being cured, and thus, the aluminum layer of a resistor surface is protected; and the welding agent has the advantages of good conductivity, strong adhesiveness, good chemical stability and better mechanical properties.
Owner:NANYANG JINNIU ELECTRIC

Processing method for interface of molded joint of high-voltage cable

The invention discloses a high-voltage cable molded joint interface treatment method, which comprises the following specific operations: (1) treating a crosslinked cable insulation body by using plasma, and immediately performing insulation material extrusion molding after treatment; (2) after full filling, a vulcanization process is carried out, a cross-linking reaction is carried out, and the vulcanization process comprises three heating and heat preservation stage processes; and (3) after the reaction is finished, cooling and preserving heat to eliminate internal stress. According to the method, the cable insulation surface is treated through plasma, so that a cross-linked network structure on the surface is cracked, steric hindrance is reduced, meanwhile, a large number of free radicals are generated, firm binding force between the cable insulation surface and a newly injected insulation material is promoted, and the performance of a body cannot be affected by over-crosslinking; and the electrical and mechanical properties of the molded joint under high-pressure work are improved.
Owner:HENGTONG SUBMARINE POWER CABLE CO LTD

A kind of alkaline battery negative electrode preparation method

The invention discloses an alkaline battery cathode preparation method, and aims to improve the uniform dispersity of a gelatinizing agent for preparing gel electrolyte. The alkaline battery cathode preparation method comprises the following steps: (1) metering and feeding an electrolyte into a stirring tank of a gel electrolyte stirring device, and starting a stirring motor of the gel electrolyte stirring device to enable the gel electrolyte stirring device to firstly stir the electrolyte for time A; (2) after the electrolyte is stirred for the time A, metering the gelatinizing agent, then dispersively feeding the gelatinizing agent into the stirring tank of the gel electrolyte stirring device, completing the feeding of the gelatinizing agent within time B, and keeping the stirring motor of the gel electrolyte stirring device working during the feeding of the gelatinizing agent; (3) continuously enabling the stirring motor of the gel electrolyte stirring device to work for time C; (4) aging a product obtained in the step (3) for time D to swell the gelatinizing agent; (5) metering the gel electrolyte obtained in the step (4), then feeding the gel electrolyte into a stirring container of zinc paste stirring equipment, adding metered zinc powder, and uniformly mixing the zinc powder and the gel electrolyte through the zinc paste stirring equipment; (6) feeding zinc paste obtained in the step (5) into a zinc paste transfer container.
Owner:浙江长虹飞狮电器工业有限公司
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