The invention relates to a preparation method of mesoporous beta-TCP (
tricalcium phosphate)
powder. The preparation method comprises steps as follows: 1), two parts of transparent solutions containing surfactants, cosurfactants and water are prepared; 2), a
calcium-containing inorganic
salt solution and a
phosphorus-containing inorganic
salt solution are added to the transparent solutions respectively and stirred, a
phosphorus-containing inorganic salt
mixed solution is added to a
calcium-containing inorganic salt
mixed solution, the pH value is adjusted, and the mixture is stirred to obtain an
emulsion; and 3), the mixture is left to stand, subjected to
ageing,
centrifugation, washing and
drying, placed in a high-temperature furnace, heated and subjected to heat preservation, and mesoporous beta-TCP
powder is obtained. The preparation method has the benefits as follows: 1, the operation is simple,
energy consumption is low, the cost is low, the reaction condition is mild, and harmful substances are not generated in the preparation process; and 2, the obtained mesoporous beta-TCP
powder has smaller
pore diameter and has a three-dimensional pore structure, the average
pore diameter of the mesoporous beta-TCP powder is 8.80-21.36 nm, and the specific surface area is 10.11-153.43 m<2> / g.