The invention discloses a production method for high-concentration defluorinate nitro
nitrogen phosphorus and
potassium compound
fertilizer, which is based on the conventional process
route of
nitric acid phosphatic
manure production, an acid-insoluble substance deep desorbing procedure is added in an acid-insoluble substance
precipitation separation procedure so as to radically separate the acid-insoluble substance; a
mother liquor defluorinating procedure is added between
calcium nitrate filtration and
mother liquor neutralization, by adding
potassium nitrate into
mother liquor, fluosilicic acid ions in mother liquor is reacted with
potassium ion to generate potassium fluorosilicate product, after defluorinating reaction, potassium fluorosilicate is separated from
slurry through filtering and separating, and
ammonia neutralization,
evaporation, pelletization,
drying and cooling treatment are performed on defluorinated mother liquor by adding
potassium nitrate and
ammonium nitrate, namely, high-concentration nitro
nitrogen phosphorus and potassium compound
fertilizer is obtained. In the invention, mid low grade
phosphate rock is used for preparing compound
fertilizer, namely
fluorine resource is recycled, and by-product potassium fluorosilicate is obtained, pollutions to the environment are reduced, the obtained product has an excellent performance,
chlorine is not contained, the application range is broad, the probability of
caking is low, and the market competitiveness is strong.