The invention relates to a
graphene preparation method, which comprises: 1, preparing a
working electrode, wherein
graphite is pressed on a stainless steel
current collector so as to be adopted as a
working electrode of a three-
electrode system, 2, preparing intercalation
graphite, wherein the three-
electrode system is adopted to prepare intercalation
graphite, 3, washing, wherein deionized water is adopted to wash the intercalation graphite, 4, carrying out
vacuum drying, 5, carrying out
microwave stripping, wherein the dried intercalation graphite is taken and added to an
ion liquid according to a certain
mass volume ratio, and the obtained mixture is placed into a
microwave oven to carry out stripping, 6, washing, wherein
filtration is performed by using
organic solvent, and washing is performed by using deionized water until the pH value is neutral, and 7, carrying out
vacuum drying. According to the present invention, the
graphene preparation method has characteristics of simple operation and easy industrialization achievement, the yield of the
graphene prepared by using the graphene preparation method is high, and the single layer rate of the graphene is up to more than 60%.