The invention discloses a preparation method of a
graphene /
nickel-aluminum bi-
metal hydroxide composite material and an application thereof, belonging to the technical field of
electrochemistry. The preparation method comprises the following steps of: preparing a
mixed solution by a stripping
enhancer, oxidized
graphene and deionized water, dispersing the
mixed solution by ultrasonic wave; decompressing and filtering the
mixed solution to obtain a filtering cake, and arranging the filtering cake into a household
microwave oven to radiate; placing a
graphene filtering cake into a tubular furnace, charging Ar / H2
mixed gas, and executing high-temperature thermal
cracking; and adding an alkali source compound,
nickel and aluminum salt precursors, a medium regulating agent and the deionized water to prepare a reactant mixing solution, and transferring the reactant mixing solution to a high-pressure reaction kettle to carry out a
hydrothermal reaction, and finally obtaining the graphene /
nickel-aluminum bi-
metal hydroxide composite material. According to the preparation method of the graphene / nickel-aluminum bi-
metal hydroxide composite material, disclosed by the invention,
toxic chemical agents are not used at two steps of reduction of the graphene, thus damage on the health of a
human body and environmental
pollution because a large number of harmful
chemical agents such as hydrazine
hydrate and the like are taken as a strong
reducing agent in a
chemical reduction method can be eliminated fundamentally.