1602results about How to "Conducive to large-scale industrial production" patented technology

The invention discloses a gradient-doping positive material of a lithium ion battery and a preparation method of the gradient-doping positive material of the lithium ion battery. The structural formula of the positive material is shown as Li(1+alpha)Ni(x)M(y)M'(1-x-y)O(2), wherein alpha is greater than or equal to 0 and less than or equal to 0.2; x is greater than or equal to 0.3 and less than or equal to 1.0; y is greater than or equal to 0 and less than or equal to 0.475; 1-x-y is greater than 0 and less than or equal to 0.35; the concentration of doping element M' is subjected to gradient change from the surfaces of the material particles; on the surfaces of the material particles, the concentration of the element M' is relatively high, the concentration of element Ni is relatively low, and even the surfaces of the material particles are free of the element Ni; in the material particles, the concentration of the element Ni is relatively high, the concentration of the element M' is relatively low, and even the inside of the material particles are free of the element M'. The positive material is excellent in comprehensive performance and especially has the advantages of high discharge capacity, excellent cycle performance and the like. In addition, the method is simple; the industrial production is easy to implement.

The invention discloses a method for preparing porcelain granules by using fly ash, which comprises the following steps: putting fly ash, potassium feldspar and quartz as raw materials into a ball mill respectively, dry-milling the raw materials, sieving the milled raw materials respectively, removing iron from the sieved fly ash, putting the fly ash after iron removal, the sieved potassium feldspar and quartz and kaolin into the ball mill, and wet-milling and evenly mixing the materials to form mixed slurry; and granulating the mixed slurry by adopting a pressure type spray granulator, putting the granules into an alumina crucible, placing the alumina crucible into a silicon-carbon rod resistance furnace, sintering and naturally cooling the granules, and taking out the granules to obtain the high-strength porcelain granules. The method for preparing the porcelain granules by using the fly ash is not only favorable for saving natural resources and reducing the production cost, but also favorable for environmental protection. The fly ash does not need to be crushed by a high-power crusher, and the fly ash is mixed evenly. The production process is easy to control, and has little energy consumption; the strength of the prepared fly ash porcelain granules can reach 60 to 120MPa; and the porcelain granules have good properties of light weight, high temperature resistance, corrosion resistance and the like, and can be used as a fracturing propping agent for middle and deep layer oil-gas fields.

The invention relates to an automatic frequency tracking method and a system for an ultrasonic transducer. A direct digital frequency synthesizer is used as a signal source, wherein the direct digital frequency synthesizer can be an independent integrated chip and also be achieved by the method that a digital part of a DDS is integrated in a site programmable logical element FPGA and then a digital-analog converter is additionally added. The design of the invention adopts a frequency sweeping and tracking policy, and an automatic frequency controller achieved by the programmable element controls the output frequency of the DDS according to a feedback signal sampled from the self transducer end so as to achieve the full digitization automatic frequency tracking and ensure that the ultrasonic transducer work near a resonance point all the time to obtain the optimal efficiency. A phase comparator utilizes a trigger to give out the arriving time difference of two riser edge signals of two input signals I ph and V ph aiming to the sensitive characteristics of the riser edge signals, and the sequence of the riser edge signals of the two input signals I ph and V ph is given out by a Dirrect pin.

The invention relates to monodisperse large-grain-diameter and high-stability acid silica sol and a preparation method thereof. The silica sol comprises water and silica colloid, wherein the silica colloid is dispersed in the water and has the granularity being 10 to 100 nm, the pH value of a sol system is 1.0 to 6.0, and the solid content is 10 to 35 percent. The preparation method comprises thefollowing steps that: firstly, active silicic acid is prepared through an ion exchange method and is added into boiling water glass to be prepared into basic silica sol with the uniform granularity, organic acid is adopted for surface modification, finally, the acid silica gel is prepared through iron exchange, and the silica sol is concentrated to the required concentration. Small-granularity and low-concentration products are adopted as the mother liquid, the sol grain growth process is controlled through controlling the dripping times of the active silicic acid and simultaneously regulating the pH value and the reaction time of a reaction system, and the monodisperse large-grain-diameter and high-stability acid silica sol products are obtained. The product stability is good, the coagulation and gel phenomena can not occur after the storage for more than six months at the normal temperature, the production period is short, and the mass industrial production is favorably realized.

The invention provides a new taxane derivative and a preparation method thereof as well as a method of preparing antitumor medicaments (cabazitaxel, docetaxel and taxol) by utilizing new taxane isoserine ester.

The invention provides a preparation method of a drug loaded emulsion, which can reduce degradation of a drug in a preparation process. The method comprises the following steps: a, preparing a blank emulsion without drug ingredients; and b, adding an effective treatment amount of the drug in the blank emulsion. The technology process is simple, avoids the use of an organic solvent, and is suitable for industrial production in a large scale.

The invention provides a nickel-iron double hydroxide / foamed nickel catalyst based on a ferric chloride / urea eutectic solvent, and a preparation method and an application thereof. The nickel-iron double hydroxide / foamed nickel catalyst is prepared from the eutectic solvent which is prepared from ferric chloride hexahydrate and urea. The preparation method has the advantages of cheap and easily available raw materials, low cost, extremely simple operating process, easily realized reaction conditions, no high temperature, low energy consumption, short preparation period, and suitableness for industrial production. The obtained catalyst is nickel-iron double hydroxide loaded on foamed nickel, and the catalytic active component is nickel-iron double hydroxide (NiFe-LDH), and has a hierarchicalstructure that is a nanoflower structure composed of nanosheets. The catalyst has a good electrocatalytic electrolysis effect on water and urea.

The invention is concerned with a secondary fermentation method of tea. It takes Yunnan-Dayecha or the camellia related genera plant with large lamina as material to produce Pu'er crude tea, i.e. green tea, through beating, rolling and drying. Repeat the wet, ferment and dry process for some times, and age to get Pu'er ripe tea. Or it takes un-fermentation tea or half fermentation tea as material, through repeating the wet, ferment and dry process for some times, and age to get secondary fermentation tea. During the machining process, the tea does not go moldy and emanates the faint scent smell, and the color is carmine after deep dunking close to the liquor color of Pu'er crude tea stored for long time, and the smell is aromatic and natural, and the flavor is rich and tasty taste. The operation is easy and fits for industry produce in large without losing the nutritional substance.