The invention discloses a low-temperature
sintering temperature stabilization type
zirconate microwave dielectric ceramic material, which comprises Li2Mg3ZrO6, CaZrO3 and ZrO2. The preparation methodcomprises: S1, weighing raw materials MgO, Li2CO3 and ZrO2, completely mixing the raw materials, agate balls and absolute
ethanol, carrying out ball milling for 6-10 h,
drying, and pre-firing to obtain Li2Mg3ZrO6 pre-fired
powder; S2, weighing raw materials CaCO3 and TiO2, mixing the raw materials, agate balls and absolute
ethanol, carrying out ball milling for 6-10 h,
drying, and pre-firing to obtain CaTiO3 pre-fired
powder; and S3, adding the Li2Mg3ZrO6 pre-fired
powder obtained in the step S1, the CaTiO3 pre-fired powder obtained in the step S2, and LiF into a container, adding agate ballsand absolute
ethanol, mixing, carrying out ball milling for 6-10 h,
drying, adding a
polyvinyl alcohol aqueous solution, granulating, sieving, forming a billet by a sheet pressing
machine, and
sintering to obtain the low-temperature
sintering temperature stabilization type
zirconate microwave dielectric ceramic. According to the present invention, the disadvantages of large
resonance frequency
temperature coefficient and high sintering temperature of the
ceramic material are overcome, and the temperature stability of the material is ensured.