The invention relates to the field of preparation of semiconductor elements, and particularly discloses a preparation method of a semiconductor structure, which comprises the following steps: firstly, forming a dielectric layer on a substrate, forming a reflection-resistant layer on the dielectric layer, forming an A photoresist layer on the reflection-resistant layer, and exposing and developing the A photoresist layer. Under the effect of thereflection-resistant layer, the arc-shaped part of the dielectric layer at the gate structure does not reflect light, so that the problem that the patterned photoresist layer generates defects and is even stripped off is avoided, then the opening is etched, the reflection-resistant layer is removed, and finally the silicide layer is formed. the processing device is adopted to remove the anti-reflection layer, the processing device comprises a fixing shaft, a clamping mechanism, a loading tray and an adjusting mechanism, the clamping mechanism is used for clamping the loading tray, elements are loaded in the loading tray, and the adjusting mechanism is used for adjusting the clamping mechanism to intermittently and sequentially enter and exit from a dissolving tank, a flushing tank and a drying mechanism. The reflection-resistant layer layer on the element is dissolved, washed and dried, and automatic machining is achieved.