The invention belongs to the technical field of energy conversion, and discloses an efficient two-dimensional
nitrogen heterocarbon material, a preparation method thereof and an application thereof inthe field of energy conversion, in particular, the application as an electric catalyst in
oxygen reduction reaction and
carbon dioxide electric reduction reaction. A method for prepare a high-efficient two-dimensional
nitrogen heterocarbon material comprises that follow steps of: synthesizing two-dimensional
silicon dioxide by adopting a double template, introducing a
nitrogen-containing precursor into a
silicon dioxide template, performing carbonizing at a high temperature, removing the
silicon dioxide template, and obtaining the high-efficient two-dimensional nitrogen heterocarbon material.The invention also provides an efficient two-dimensional azacarbon material prepared by the method. The efficient two-dimensional nitrogen heterocarbon material has a unique two-dimensional mesoporous structure, which can not only fully
expose the catalytic active sites, but also facilitate the transport of active species, showing excellent electrocatalytic performance, and can be used in
electrochemical energy conversion and storage technology. In particular, the efficient two-dimensional nitrogen heterocarbon material is used as an
electrocatalyst in
oxygen reduction reaction in alkaline condition and
carbon dioxide reduction reaction in alkaline condition.