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35results about How to "Achieve high-value conversion" patented technology

Biodegradable agricultural high-absorbent resin and preparation thereof

The invention discloses a biodegradable agricultural super absorbent resin, which is prepared with the main raw materials by weight ratio as follows: 100 portions of crop biomass, 50-150 portions of acrylic acid, 200-1,000 portions of 1% sulfuric acid aqueous solution, 7-70 portions of sodium hydroxide, 0.25-10.0 portions of N,N`-methylene-bis-acrylamide as cross-linker, as well as at least an initiator selected among 0.5-15.0 portions of persulphate, 0.5-10.0 portions of ferric salt and 0.5-8.0 portions of sodium salt. The resin has good biodegradable performance, moderate water absorption, and greatly reduced costs. The invention also discloses a preparation method of the biodegradable agricultural super absorbent resin.
Owner:SICHUAN NORMAL UNIVERSITY

Method for efficiently extracting mulberry branch bark pectin

The invention discloses a method for efficiently extracting mulberry branch bark pectin. The method comprises the following steps of: (1) treating mulberry branch bark by using a greenhouse ionic liquid to separate pectin in the branch bark from cellulose and the like; (2) after treating with the greenhouse ionic liquid, adding water for dissolving the pectin in the mulberry branch bark pectin into water, and precipitating components such as cellulose, hemicellulose, lignin and the like out; (3) taking an upper layer liquid, adding cellulose for treating, and removing cellulose impurities; and (4) decolorizing a supernatant, adding ethanol for precipitating the pectin out, washing with absolute ethanol, drying, and grinding into powder to obtain mulberry branch bark pectin. In the method, the ionic liquid is taken as a treating agent for extracting mulberry branch bark pectin, so that pectin can be extracted effectively, ionic liquid treatment is only required to be performed for 20-50 minutes, the final yield of pectin can be up to about 11 percent, and the pectin extracting efficiency of the mulberry branch bark is increased.
Owner:JIANGSU UNIV OF SCI & TECH

Method for preparing biodiesel by directly using cellulose through mixed fermentation

The invention discloses a method for preparing biodiesel by directly using cellulose through mixed fermentation. The mixed fermentation is performed by using a plant fiber degrading strain and a grease producing strain, and ethanol is produced by directly using natural plant fiber such as straws. The method comprises the following steps of: designing a culture medium for the mixed fermentation by optimization methods such as a response surface method, and optimizing to obtain the fermentation conditions such as the optimum temperature of mixed fermentation, optimum mixing proportion of strains and optimum mixing time of the strains by utilizing the methods such as orthogonal test and response surface methodology; according to the optimized fermentation conditions, by using the plant fiber as a carbon source, degrading the cellulose into fermentable sugar by using a cellulase producing strain, and adding grease-producing microorganisms into the culture system for the mixed fermentation; and by using the sugar which is produced by the constant enzymolysis of the plant fiber as the carbon source, fermenting to produce grease by using the grease producing strain, and performing methyl esterification reaction of the microbial grease to obtain the biodiesel.
Owner:JIANGSU UNIV OF SCI & TECH

Mulberry twig bark fiber/silk fibroin multilayer composite membrane and preparation method of same

ActiveCN107599544ASolve the problem of purely physical mixingImprove water absorption and moisture retentionLaminationLamination apparatusMultilayer membraneFiber
The invention discloses a preparation method of a mulberry twig bark fiber / silk fibroin multilayer composite membrane. The preparation method includes the steps of: 1) initial separation of mulberry twig bark fibers; 2) identification of content and purity of the mulberry twig bark fibers; 3) modification of the mulberry twig bark fibers; 4) grafting of the mulberry twig bark fibers; 5) productionof single-layer membranes; and 6) production of the multilayer membrane. The multilayer composite membrane not only solves a problem of single physical mixing during preparation of composite membranes in the prior art, has good water absorption and moisture retention effect, has good thermostability, is reduced in crystallization degree, and is improved in mechanical properties.
Owner:JIANGSU UNIV OF SCI & TECH

Method for preparing bioethanol

The invention provides a method for preparing bioethanol. The method comprises the following steps of: performing constant-temperature shaking culture on plant fiber and seed liquid of a cellulase producing strain for 0 to 5 days in a fermentation culture medium, inoculating seed liquid of an ethanol producing strain into the fermentation culture medium, and continuing to perform constant-temperature shaking culture for 3 to 7 days; and filtering fermentation liquor, and distilling a filtrate under reduced pressure to obtain the bioethanol. The method for preparing the bioethanol is high in yield and low in cost, is environment-friendly, and is suitable for industrialized production.
Owner:JIANGSU UNIV OF SCI & TECH

Selenium and nitrogen co-doped biochar catalytic material as well as preparation method and application thereof

The invention discloses a selenium and nitrogen co-doped biochar catalytic material as well as a preparation method and application thereof. High-toxicity selenite is reduced into low-toxicity biological nano-selenium under the biological detoxification action of bacteria (Bacillus megaterium B10 with the preservation number of CGMCC No.15753), then selenium-enriched thalli serve as a carbon source of biochar, a nitrogen source is added, and the novel selenium and nitrogen co-doped biochar catalytic material is prepared with a simple one-step carbonization method. The preparation method of theselenium and nitrogen co-doped biochar provided by the invention is simple, convenient, safe, cheap and easy to control, and can be used for large-scale production. Meanwhile, the reduction effect ofbacteria on high-valence selenium can rapidly achieve detoxification of selenite pollutants, the environment-friendly advantage is achieved, in addition, the biochar can effectively degrade refractory organic matter or pollutants by activating monopersulfate, the removal effect is good, the reaction speed is high, and the application prospect in the field of wastewater remediation is very wide.
Owner:CENT SOUTH UNIV

Method for extraction of mulberry pectin via coupling of N-methyl morpholine oxide and cellulase

The invention discloses a method for extraction of mulberry pectin via coupling of N-methyl morpholine oxide and cellulose, which comprises the following steps of: (1) processing mulberry barks with the N-methyl morpholine oxide: using the mulberry barks as raw materials, processing the mulberry barks with the N-methyl morpholine oxide for equal-component separation of pectin and cellulose in the mulberry barks, adding water after processing, so that the pectin is dissolved in water and the cellulose, hemicellulose, lignin and other components are precipitated; (2) processing the cellulase: taking the supernatant liquid, adding the cellulase for processing, and removing cellulose impurities; and (3) preparing the pectin: bleaching the supernatant liquid, adding ethyl alcohol for precipitation of the pectin, washing with absolute ethyl alcohol, and drying and grounding into powder to obtain the mulberry pectin. The N-methyl morpholine oxide is used as a processing agent to extract the pectin in the mulberry barks, the pectin can be extracted efficiently, only 20-50min is needed for processing with the NMMO (N-methyl morpholine oxide), the final yield of pectin can reach 11 percent, and the efficiency of extraction of the pectin from the mulberry barks can be increased.
Owner:JIANGSU UNIV OF SCI & TECH

Preparation method of mulberry protein active peptide

The invention discloses a preparation method of mulberry protein active peptide. The method comprises the following steps that mulberry leaves and mulberry bark are washed, dried and smashed, a treating agent prepared from magnetic graphene oxide, dilute acid and hydrogen peroxide is added for digestion, the magnetic graphene oxide is recycled through a magnet, the pH value is adjusted to be 4.5-5.5, precipitate is obtained through centrifugation, water is added into the precipitate for dissolving and filtration, filtrate contains mulberry protein solution, heating treatment is carried out, cooling is carried out, the pH value is adjusted to be 7-8.5, protease is added for heat preservation, the product is placed in an ultrasonic field for ultrasonic assisted enzymolysis, high-temperature heating is carried out for inactivating enzyme, centrifugation is carried out, supernate is collected, decoloring, suction filtration, ultrafiltration, dialysis, ion exchange and concentration are carried out, and the mulberry active peptide is obtained. Mulberry leaves and mulberry bark are adopted as raw materials for preparing the active peptide, and the raw materials are agricultural waste, are low in cost and are of great significance in environmental protection and waste resource utilization. The mulberry protein extraction content and mulberry protein active peptide conversion efficiency are higher compared with a conventional method, and physical and chemical property is stable.
Owner:JIANGSU UNIV OF SCI & TECH

Method for efficiently extracting mulberry branch bark pectin

The invention discloses a method for efficiently extracting mulberry branch bark pectin. The method comprises the following steps of: (1) treating mulberry branch bark by using a greenhouse ionic liquid to separate pectin in the branch bark from cellulose and the like; (2) after treating with the greenhouse ionic liquid, adding water for dissolving the pectin in the mulberry branch bark pectin into water, and precipitating components such as cellulose, hemicellulose, lignin and the like out; (3) taking an upper layer liquid, adding cellulose for treating, and removing cellulose impurities; and (4) decolorizing a supernatant, adding ethanol for precipitating the pectin out, washing with absolute ethanol, drying, and grinding into powder to obtain mulberry branch bark pectin. In the method, the ionic liquid is taken as a treating agent for extracting mulberry branch bark pectin, so that pectin can be extracted effectively, ionic liquid treatment is only required to be performed for 20-50 minutes, the final yield of pectin can be up to about 11 percent, and the pectin extracting efficiency of the mulberry branch bark is increased.
Owner:JIANGSU UNIV OF SCI & TECH

Method for extracting DNJ in mulberry leaves through hydrothermal acid control and alcohol extraction

The invention discloses a method for extracting DNJ (1-deoxynojirimycin) in mulberry leaves through hydrothermal acid control alcohol extraction, and belongs to the technical field of extraction of active ingredients in natural products. According to the method, mulberry leaves are used as raw materials, and DNJ is obtained through three steps of raw material pretreatment, synchronous treatment of the mulberry leaves through hydrothermal acid catalysis and preparation of a DNJ (1-deoxynojirimycin) product. And a theoretical basis is provided for mulberry leaf medicinal resource development. The method can be widely applied to extraction of DNJ in mulberry leaves, can also be used for extraction of high-value natural products in biomass, and has important practical significance on improvement of the utilization value of mulberry leaves.
Owner:CHONGQING TECH & BUSINESS UNIV

Preparation method of mulberry fiber composite three-dimensional oil-water separation membrane

ActiveCN112717472ASolve the problem of purely physical mixingIncrease the space contact areaSemi-permeable membranesLiquid separationMultilayer membraneFiber
The invention discloses a preparation method of a mulberry fiber composite three-dimensional oil-water separation membrane, and belongs to the technical field of membranes. The preparation method comprises the following preparation steps: (1) preparing mulberry fibers; (2) treatment and modification of mulberry fibers: using enzyme partial treatment and ionic liquid mixed liquid treatment; (3) preparing a single-layer membrane: adding a cross-linking reagent, a hydrophobic reagent and an initiator, and drying and molding to obtain a molded hydrophobic and oleophylic single-layer membrane; and (4) preparation of the three-dimensional multilayer membrane: preparing the single-layer film into the multi-layer three-dimensional composite membrane by adopting an ionic liquid composite cross-linking agent according to application requirements. The method has the beneficial effect that a new way is provided for resource utilization of biomass wastes. The method has the advantages of high efficiency, environmental friendliness and the like, the spatial dimension and the contact area of the membrane are improved, and the problem of poor mechanical properties of the membrane in the use process is solved.
Owner:JIANGSU UNIV OF SCI & TECH

Component with liver protection effect and application thereof to prevention and control of non-alcoholic fatty liver

The invention relates to lycium ruthenicum extract with a liver protection function and evaluation of an inhibition effect of the lycium ruthenicum extract to non-alcoholic fatty liver and belongs to the field of biomedicines. A main raw material is natural food-borne lycium ruthenicum; a preparation method comprises: weighing the lycium ruthenicum; extracting the lycium ruthenicum with ethanol with the concentration of 50 percent to 70 percent according to the material-liquid ratio ranging from (1 to 1) to (1 to 20), wherein the extracting temperature is 30 DEG C to 100 DEG C and the extracting time is more than 15 minutes; after filtering, taking filtrate and repeating for 1 to 5 times; combining the obtained filtrate and concentrating at low temperature and in vacuum to obtain the extract. Mice which are fed by high fat are fed with the extract by gavage and an inhibition effect on the non-alcoholic fatty liver is evaluated; the extract can obviously inhibit the non-alcoholic fatty liver caused by high fat diet and complicated metabolic diseases is proved; the lycium ruthenicum extract has a remarkable liver function protection effect.

A method for preparing carbon-based transition metal sulfide composite electrode material based on pyrolysis bio-oil

The invention belongs to the technical field of biomass resource utilization and electrode material preparation, and relates to a method for preparing a carbon-based transition metal sulfide composite electrode material based on pyrolysis bio-oil. First, dissolving nickel sulfate or cobalt sulfate into an alcohol / water solution to prepare a bio-oil absorbing solution; then using the absorbing solution to capture the bio-oil produced by biomass pyrolysis, drying the absorbing solution after the pyrolysis reaction, and then passing After being calcined in a reducing atmosphere and cooled to room temperature, the composite electrode material can be prepared. The invention uses bio-oil produced by biomass pyrolysis as raw material, and the prepared composite electrode material has excellent supercapacitor performance: under the current density of 1 A / g, the specific capacitance of the composite electrode material is as high as 1000 F / g above. In addition, the biomass raw material of the invention is cheap, green and sustainable, and the preparation process is simple, which provides a new approach and idea for the high-value conversion of biomass resources and the preparation of carbon-based transition metal sulfide composite electrode materials.
Owner:山东济清科技服务有限公司

Application of lotus leaf alcohol extract in preparation of drug for inhibiting cancer metastasis

The invention discloses an application of a lotus leaf alcohol extract in preparation of a drug for inhibiting cancer metastasis and belongs to the technical field of biomedicine. Mice suffering frommetastatic cancer are used as experimental subjects, compared with a control group fed with normal feed, the mice which suffer from the metastatic cancer and are fed with feed containing the lotus leaf alcohol extract have obviously reduced weight and have the lung metastasis number reduced by about 45% and the total tumor weight at the metastasis part reduced by about 50%. The fact that the lotusleaf alcohol extract can be used for effectively inhibiting cancer metastasis is put forward for the first time, so that a new way is opened up for treatment of metastatic tumor, great significance is made in the development of edible and medicinal dual-purpose resources, high-value conversion of active plant resources is realized, and deep processing and utilization of agricultural products is promoted.
Owner:JIANGNAN UNIV

Production process of 2-amino-3,5-dibromobenzaldehyde

The invention relates to the technical field of pharmaceutical chemicals, in particular to a production process of 2-amino-3,5-dibromobenzaldehyde. The method comprises the following steps: mixing iron powder and hydrochloric acid, adding an extracting agent and 3-nitro-o-dibromomethyl benzene, adjusting the pH value to 7-9 after the reaction is finished, conducting filtering, and separating the liquid to obtain an 3-amino-o-dibromomethyl benzene extraction reaction liquid; adding sulfuric acid into the reaction solution, conducting stirring, and conducting separating to obtain a 3-amino-o-dibromomethyl benzene sulfuric acid reaction solution; adding hydrobromic acid into the sulfuric acid reaction solution, dropwise adding bromogen and / or an oxidizing agent, controlling monobromine to be less than or equal to 0.2%, and adding chloroform to obtain a 2-amino-3,5-dibromodibromomethyl benzene organic solution; adding a dimethylamine aqueous solution and sodium bicarbonate into the organic solution, and separating the solution after the reaction to obtain a 2-amino-3,5-dibromobenzaldehyde chloroform reaction solution; and concentrating, refining and decoloring the chloroform reaction solution to obtain the 2-amino-3,5-dibromobenzaldehyde. The method provided by the invention can be used for industrially synthesizing the 2-amino-3,5-dibromobenzaldehyde, and the nitro waste material generated in the o-nitrobenzaldehyde production process can be utilized.
Owner:JIANGXI RONGXING PHARMA

A kind of preparation method of simulated cellulase

The invention discloses a method for preparing simulated cellulase. The method comprises the following steps: taking a cellulose material, washing, removing the impurities, drying, grinding, and screening, thereby obtaining cellulose powder; uniformly mixing and stirring the obtained cellulose powder with ionic liquid according to a mass ratio of 1-20:100, preserving the temperature, performing assisted microwave treatment so as to expand the fibers, washing to remove the ionic liquid, and drying to remove the moisture, thereby obtaining a primary sample; adding the obtained primary sample into a crucible, putting the crucible into a tube furnace, and performing heating treatment under gas protection; adding a mixed acid, adding water and washing to remove the impurities, and drying to obtain dried powder, thereby obtaining the sample powder; adding the obtained sample powder into an organic base, stirring, heating, reacting, and washing by using a cleaning solvent, thereby obtaining the simulated cellulase. The simulated cellulase prepared by the method is high in binding ability with a substrate (a cellulose material) and good in thermal stability, high-temperature catalysis can be performed, the catalytic effect is good, the cost of the raw materials is low, and the cellulase can be repeatedly utilized.
Owner:JIANGSU UNIV OF SCI & TECH

A method for co-producing bioethanol and pullulan from lignocellulosic substances

The invention discloses a method for combined production of bioethanol and pullulan from lignocellulose substances. The method comprises the following steps: subjecting the lignocellulose substances to alkaline-process pretreatment and xylanase enzymatic hydrolysis and then carrying out solid-liquid separation so as to respectively obtain a hemicellulose hydrolysate (xylose liquid) and a solid-phase residue; subjecting the solid-phase residue to lignin extraction so as to obtain a cellulose residue; directly applying the xylose liquid to fermentation production of pullulan (wherein yield is no less than 0.29 g of pullulan per g of xylose) and subjecting the cellulose residue to synchronous saccharification and fermentation to produce ethanol; subjecting fermentation broth containing pullulan to fermentation and distillation with fiber residue, carrying out alcohol precipitation on obtained ethanol, carrying out extraction and refining so as to obtain a pullulan product, combining ethanol-containing waste liquid produced during purifying with cellulose residue ethanol fermentation broth and carrying out distillation so as to realize recovery and reuse of ethanol. The method can realize full utilization and high-value conversion of hemicellulose and cellulose, saves resources and achieves the purposes of environmental protection and economic benefit improvement.
Owner:TIANJIN UNIV OF SCI & TECH

A kind of selenium, nitrogen co-doped biochar catalytic material and its preparation method and application

The invention discloses a selenium and nitrogen co-doped biochar catalytic material as well as a preparation method and application thereof. The present invention utilizes the biological detoxification effect of bacteria (Bacillus megaterium B-10, preservation number CGMCC No.15753) to reduce highly toxic selenite to low-toxic biological nano-selenium, and then uses selenium-enriched bacteria as the carbon of biochar A new type of selenium and nitrogen co-doped biochar catalytic material was prepared by a simple one-step carbonization method by adding a nitrogen source. The preparation method of the selenium and nitrogen co-doped biochar proposed by the invention is simple, convenient, safe, cheap and easy to control, and can be produced on a large scale. At the same time, the reduction of high-valent selenium by bacteria can quickly detoxify selenite pollutants, which has the advantage of being environmentally friendly. In addition, the biochar can effectively degrade refractory organics or pollutants by activating monopersulfate, and the removal effect is good. The reaction speed is fast, and the application prospect in the field of wastewater restoration is very broad.
Owner:CENT SOUTH UNIV

Method for preparing high-purity sulfur from tail gas containing hydrogen sulfide

The invention relates to a method for preparing high-purity sulfur from tail gas containing hydrogen sulfide. The method comprises the following step: carrying out contact reaction on the tail gas containing hydrogen sulfide and sulfuric acid through a contact device to obtain sulfur with the purity of more than or equal to 99.95%. The molar ratio of the sulfuric acid to the hydrogen sulfide is (0.1-1): 1; the concentration of the sulfuric acid is greater than or equal to 75%; and the high-purity superfine sulfur is obtained by controlling gas-liquid two-phase related parameters in the reaction process. The method is high in absorption reaction efficiency, mild in reaction process, free of secondary pollution and high in applicability. The purity of the sulfur product is greater than or equal to 99.5%, the particle size range is 10-30 [mu]m, and the sulfur product can be directly applied to industries such as medicine, agriculture and chemical engineering; and the treated absorption liquid can be directly sold or used as a by-product.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI

A kind of preparation method of antibacterial fiber sponge material

The invention discloses a preparation method of an antibacterial fiber sponge material, which comprises the following steps: (1) washing mulberry branches, drying and crushing to a certain particle size to obtain mulberry branch powder; (2) taking a certain amount of mulberry branch powder and a certain After a certain amount of configured ionic liquid is mixed in a three-necked flask, heat treatment in a heat-collecting constant temperature heating magnetic stirrer; (3) the sample obtained in step (2) is placed in a mold, an appropriate amount of pore-forming agent is added, and stirred evenly, Molding; (4) washing to remove the pore-forming agent and excess solvent, adding the prepared cellulase solution into the mold for reaction; (5) freezing the molded sample and freeze-drying at low temperature to obtain the finished product of the fiber sponge. The invention adopts the renewable mulberry waste as raw material, the regeneration cycle is rapid, the environmental pollution caused by the mulberry burning is avoided, and the high-value conversion of the mulberry waste is realized at the same time; it has the characteristics of ventilation, water retention and moisturizing, and has no allergens , no immune response, natural antibacterial effect and other advantages.
Owner:浙江省仙居县南方海绵有限公司

A kind of preparation method of stable isotope labeled glucose

The invention relates to a method for preparing stable isotope-labeled glucose, which comprises the following steps: pretreatment of raw materials: 13 C-labeled Chlorella pyrenoidosa as isotopic raw material, using organic solvents for 13 C-labeled Chlorella pyrenoidosa is subjected to decolorization treatment, and the decolorization bacterium cell crushing treatment; starch liquefaction and saccharification reaction: after the pretreatment 13 C-labeled Chlorella pyrenoidosa undergoes a liquefaction reaction with a liquefaction enzyme, and then undergoes a saccharification reaction with a glucoamylase, separates the reaction liquid from solid to liquid, and collects the supernatant; 13 Separation of C-labeled glucose: The supernatant is subjected to resin decolorization treatment to obtain an eluate, which is concentrated, activated carbon decolorized and crystallized to obtain the 13 C labeled glucose. Compared with the prior art, the present invention has 13 The C-labeled glucose product has the advantages of high abundance and purity, mild process conditions, little impact on the environment, and high utilization rate of chlorella.
Owner:SHANGHAI RES INST OF CHEM IND

A kind of preparation method of mulberry base solid acid

The invention discloses a preparation method of a mulberry twig-based solid acid. The preparation method comprises the steps: firstly washing cleanly impurities and mud on mulberry twigs, peeling, drying, smashing, and thus obtaining a mulberry twig powder; then mixing the obtained mulberry twig powder with N-methyl morpholine oxide according to a ratio of 1:8-10, stirring at the temperature of 80-100 DEG C with the stirring time of 0.5-3 h, and assisting with ultrasonic treatment to make fibers swelled, then washing to remove N-methyl morpholine oxide, adding an auxiliary agent according to a ratio of the mulberry twig powder to the auxiliary agent of 20:1 to make the mulberry twig powder activated, and drying to remove water; then putting the obtained product into a crucible, placing in a tube furnace, adjusting the furnace temperature to 400-500 DEG C, and carrying out heating treatment with nitrogen protection and the treatment time of 1-5 h; and finally, adding fuming sulfuric acid according to a ratio of the mulberry twig powder to a 20% fuming sulfuric acid of 1:1-5, treating, washing to remove impurities, and drying to obtain the mulberry twig-based solid acid. The solid acid has the advantages of small particles, good adsorption property on reaction substrates, good catalytic effect, high thermal stability, high acid value, and low cost, and the raw materials are waste materials.
Owner:JIANGSU UNIV OF SCI & TECH

A kind of preparation method of mulberry active peptide

The invention discloses a preparation method of mulberry active peptide, which comprises the following steps: after washing, drying and crushing mulberry leaves and mulberry bark, adding a treatment agent composed of magnetic graphene oxide, dilute acid and hydrogen peroxide to extract, and using Magnet recovers magnetic graphene oxide, adjusts the pH value to 4.5-5.5, centrifuges to obtain the precipitate, dissolves the precipitate with water and filters, the filtrate contains mulberry protein solution, heats it, cools and adjusts the pH value to 7-8.5, adds protease to keep warm, and puts Ultrasonic-assisted enzymolysis in an ultrasonic field, high-temperature heating to inactivate the enzyme, centrifugation, collecting the supernatant, decolorization, suction filtration, ultrafiltration, dialysis, ion exchange and concentration to obtain the mulberry active peptide. The present invention adopts mulberry leaf and mulberry bark as raw material to prepare active peptide, and the raw material is agricultural waste with low cost, which is of great significance for environmental protection and resource utilization of waste; the method extracts mulberry protein content and conversion efficiency of mulberry active peptide Both are more than the conventional method, and the physical and chemical properties are stable.
Owner:JIANGSU UNIV OF SCI & TECH

A stretchable organic waste residue-based degradable mulch film and its preparation method

The invention relates to a stretchable organic waste slag-based degradable plastic film and a preparation method thereof. The mulch film is prepared from organic waste residue, acid treatment agent, oxidizing agent and optional binder and / or plasticizer, and is optionally subjected to esterification reaction under the condition of an esterification reaction catalyst. The mulch film preparation method of the present invention is simple to operate and has high reaction efficiency. The prepared mulch film has excellent tensile properties, elongation at break (%E) ≥ 120%-250%, and tensile load ≥ 1.3-2.8N, all of which meet the national standard Requirements for the physical and mechanical properties of the mulch film (GB 13735-92); the degradation cycle of the prepared mulch film is stable, and the degradation rate is ≥50%-80% (quality) in 120 days, and the degradation cycle is 180 days-1 year.
Owner:BEIJING UNIV OF CHEM TECH

Method for preparing carbon-based transition metal sulfide composite electrode material based on pyrolytic bio-oil

The invention belongs to the technical field of biomass resource utilization and electrode material preparation, and relates to a method for preparing a carbon-based transition metal sulfide compositeelectrode material based on pyrolysis bio-oil. The method comprises the following steps: firstly, dissolving nickel sulfate or cobalt sulfate into an alcohol / water solution to prepare a bio-oil absorption solution, capturing bio-oil generated by biomass pyrolysis by using the absorption liquid, drying the absorption liquid after the pyrolysis reaction is finished, calcining the absorption liquidin a reducing atmosphere, and cooling the absorption liquid to room temperature to obtain the composite electrode material. According to the invention, bio-oil generated by biomass pyrolysis is used as a raw material, and the prepared composite electrode material has excellent supercapacitor performance: under the current density of 1 A / g, the specific capacitance of the composite electrode material is as high as 1000 F / g or above. Besides, the biomass raw material is low in price, green and sustainable, the preparation process is simple, and a new way and idea are provided for biomass resource high-value conversion and preparation of the carbon-based transition metal sulfide composite electrode material.
Owner:山东济清科技服务有限公司
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