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654 results about "Bisulfate salt" patented technology

Sodium bisulfate, also known as sodium hydrogen sulfate, is the sodium salt of the bisulfate anion, with the molecular formula NaHSO4. Sodium bisulfate is an acid salt formed by partial neutralization of sulfuric acid by an equivalent of sodium base, typically either in the form of sodium hydroxide or sodium chloride.

Massive bodies containing free halogen source for producing highly converted solutions of chlorine dioxide

A massive body, e.g., a tablet, for producing a solution of chlorine dioxide when the massive body is added to liquid water. The massive body comprises a metal chlorite such as sodium chlorite, an acid source such as sodium bisulfate and a source of free halogen such as the sodium salt of dichloroisocyanuric acid or a hydrate thereof. The concentration of free halogen in the solution will be:(a) less than the concentration of chlorine dioxide in said solution on a weight basis and the ratio of the concentration of chlorine dioxide to the sum of the concentrations of chlorine dioxide and chlorite anion in said solution is at least 0.25:1 by weight; or(b) equal to or greater than the concentration of chlorine dioxide in said solution on a weight basis and the ratio of the concentration of chlorine dioxide to the sum of the concentrations of chlorine dioxide and chlorite anion in said solution is at least 0.50:1 by weight.
Owner:ENGELHARD CORP

Process for preparing atazanavir bisulfate and novel forms

A process is provided for preparing the HIV protease inhibitor atazanavir bisulfate wherein a solution of atazanavir free base is reacted with concentrated sulfuric acid in an amount to react with less than about 15% by weight of the free base, seeds of Form A crystals of atazanavir bisulfate are added to the reaction mixture, and as crystals of the bisulfate form, additional concentrated sulfuric acid is added in multiple stages at increasing rates according to a cubic equation, to effect formation of Form A crystals of atazanavir bisulfate. A process is also provided for preparing atazanavir bisulfate as Pattern C material. A novel form of atazanavir bisulfate is also provided which is Form E3 which is a highly crystalline triethanolate solvate of the bisulfate salt from ethanol.
Owner:BRISTOL MYERS SQUIBB CO

Grafted copolymerized cationic polysaccharide bioflocculant and preparation method thereof

The invention relates to a grafted copolymerized cationic polysaccharide bioflocculant and a preparing method thereof. A product with the cationic degree (DC) of 3-63% is finally prepared through an aqueous solution polymerization technology with a present nonionic polysaccharide bioflocculant (Dx) as a raw material, one or more of dimethyl diallyl ammonium chloride (DMDAAC), methacryloxyethyltrimethyl ammonium chloride (DMC), acryloyloxyethyltrimethyl ammonium chloride (DAC), dimethylaminoethyl methacrylate (DMAEMA), dimethylaminoethyl acrylate (DMAEA) as a monomer, and one or two of ammonium persulfate / sodium bisulfate and dibenzoyl peroxide (BPO) (AIBA) as an initiator. The preparation method is simple, and is easy to control, and the product obtained in the invention has good flocculation effect and high treatment efficiency, and can be widely used in the field of treatment various sewages, the sludge dewatering field and the like.
Owner:威海汉邦生物环保科技股份有限公司

Novel process for preparation of clopidogrel bisulfate polymorph - Form I

A process for making Clopidogrel Bisulfate Form I which comprises dissolving Clopidogrel Bisulfate Form II in a solublizing solvent at room temperature to form a solution; adding an anti-solvent to the said solution till turbid; stirring the said turbid solution; collecting the precipitated solid and drying the final solid product, form I.
Owner:SAWANT KAMLESH DIGAMBAR +2

Non-fluorescence collapse-proof fluid loss additive for oil exploration drilling fluid

The present invention discloses petroleum exploration well-drilling liquid used non-blooming anti-collapse and anti-falling filtration agent, which is confected by coal gangue 500Kg, waste orlon thread 270Kg, sodium hudroxide 100Kg, formaldehyde 20Kg, sodium nitrite 30Kg, sodium bisulfate 30Kg, phenol 50Kg, and water 3000Kg. The cost of the processing raw material of the product of the present invention is low, compared with the same kind of the product, the cost of the well-drilling slurry can be lowered by 30 percent, during the well-drilling process, the using volume is less, in the fresh water, 1 percent volume can be added, in the sea water, 3percent volume can be added, the performance is better than the performance of all the lignite resin products, the circumference of the drilling tool can form smooth and hard filtration cake to prevent the well wall from collapsing, to control the mudstone and the clay shale from swelling by absorbing water, to control the water lost volume, so as to improve the well-drilling schedule. The raw material adopted by the present invention is all non-blooming material, which has no interference to geological log, the product petroleum field is large in demand volume, and great in market potential. The present invention also discloses the preparation method for above anti-collapse and anti-falling filtration agent.
Owner:图们市方正化工助剂厂

Method for processing papermaking wastewater by advanced oxidation treatment of activating persulfate or monoperoxy-hydrosulfate with ferrous salt

The invention discloses a method for processing papermaking wastewater by an advanced oxidation treatment of activating persulfate or monoperoxy-hydrosulfate with ferrous salt. The method is divided into two phases, namely an oxidation phase and a precipitation phase; wherein the oxidation phase is carried out in advanced oxidation equipment where wastewater is prone to mix, the hydraulic retention time is more than 0.5 hour, then persulfate or monoperoxy-hydrosulfate is subjected to carry out reactions with ferrous salt to generate sulfate free radicals with a strong oxidizing property, the sulfate free radicals can degrade organisms in the wastewater; the precipitation phase is carried out in precipitation equipment, the hydraulic retention time is more than 1.5 hours, and an alkaline solution or polymerized aluminum chloride is added so as to promote the flocculation and sedimentation of iron mud. The papermaking wastewater processing method is based on sulfate free radical advanced oxidation treatment, and the processed wastewater is clear and has a low COD value and a low Cr content. The method has the advantages of high efficiency, easy operation, and wide applicable pH range, and is especially suitable for processing papermaking wastewater having complicated components and high requirements on advanced treatment.
Owner:SOUTH CHINA UNIV OF TECH

Acrylate copolymer emulsion, and aqueous industrial anticorrosive paint adopting acrylate copolymer emulsion as film forming substance

The invention discloses an acrylate copolymer emulsion, and belongs to the technical field of aqueous coatings. The acrylate copolymer emulsion comprises, by weight, 450-550 parts of deionized water, 1-2 parts of an anionic surfactant, 5-8 parts of a reactive emulsifier, 3-15 parts of hydroxypropyl acrylate, 50-160 parts of methyl methacrylate, 20-75 parts of butyl acrylate, 200-410 parts of styrene, 5-10 parts of methacrylic acid, 3-10 parts of an adhesion function monomer, 2-9 parts of a cross-linking monomer, 3-10 parts of a cross-linking agent, 0.1-3 parts of an antifoaming agent, 0.8-2 parts of an initiator, 3-5 parts of ammonia water, 0.8-2 parts of an antiseptic, 0.1-1 part of tert-butyl hydroperoxide and 0.1-0.8 parts of sodium bisulfate. The invention also discloses an aqueous industrial anticorrosive coating adopting the acrylate copolymer emulsion as a film forming substance. The coating has the advantages of high adhesion to a substrate, high water resistance and high salt spray resistance.
Owner:HENGSHUI XINGUANG CHEM

Temperature-resistance drilling fluid drill-feeding plugging agent and its preparation method

InactiveCN103937471AEffective blockingDoes not affect rheological parametersDrilling compositionSodium bisulfateVegetable fibers
The invention relates to a temperature-resistance drilling fluid drill-feeding plugging agent and its preparation method, the drill-feeding plugging agent comprises the following components by weight: 30-80 parts of vegetable fiber, 10-40 parts of mineral fiber, 10-40 parts of fruit shell, 0-10 parts of powdered steatile, and 3-10 parts of silicon-based gel deformation particles. The silicon-based gel deformation particles enable emulsification and dispersion of 1.4-2.5 parts of vinyltriethoxysilane monomer according to weight to an aqueous solution composed of 18-24 parts of acrylamide, 0.0025-0.005 parts of N,N'-methylene bisacrylamide, 0.7-1.25 parts of OP-10 and 0.1-0.17 parts of sodium dodecyl benzene sulfonate, 0.003 parts of disodium ethylene diamine tetraacetate, 0.009-0.12 parts of ammonium persulfate and 0.009-0.012 parts of sodium bisulfate, a process of micellar copolymerization is carried out, a polymer is dried, granulated and crushed to obtain the silicon-based gel deformation particles with average particle size of 80-200 meshes; easy-leakage highly-permeable stratum and micro crack are effectively plugged, rheological parameter of the drilling fluid is not influenced, frictional resistance coefficient of the drilling fluid is reduced, a storage layer is protected, and the drill-feeding plugging agent is suitable for plugging the easy-leakage stratum and the storage layer.
Owner:中国石油天然气股份有限公司冀东油田分公司钻采工艺研究院

Composition with capability of providing thermal stability for polymer and application of composition

ActiveCN104419015AReduced thermo-oxidative agingLow yellow indexPolyolefinPolymer resin
The invention relates to a composition with the capability of providing the thermal stability for polymer and application of the composition. The composition is prepared from the following raw materials: (1) hindered phenol, (2) phosphate or thioester, (3) an acid-removing agent and (4) sulfite, bisulfate or sulfide, wherein the mass ratio of hindered phenol, phosphate or thioester, the acid-removing agent and sulfite, bisulfate or sulfide is 1:(1-4):(0.5-2):(0.5-3). The invention also provides the application of the composition serving as an antioxidant in polymer resin. The composition is capable of lowering the melt index of polyolefin, eliminating a quinones compound serving as an intermediate and lowering the yellow index of polyolefin.
Owner:INST OF CHEM CHINESE ACAD OF SCI

Disinfection effervescence tablet capable of continuously generating high oxidation-reduction potential

The invention relates to a disinfectant effervescent tablet which can generate continuously high redox potential. The disinfectant effervescent tablet comprises the following components by weight portions: 4-8 portions of inorganic chloride salt, 8-12 portions of organic acid, 3-5 portions of one or more selected from carbonate, sodium bisulfate and hydroxylamine hydrochloride, 1-2 portions of stabilizing agent and 1-2 portions of corrosion inhibitor. The disinfectant effervescent tablet also comprises 1-2 portions of synergistic agent. An effervescent tablet of 1g/tablet is put in water and completely dissolved in 5-10 minutes to obtain 100ml-1,000ml solution; pH value of the dissolved solution is 3-7; redox potential is 800-1,200mv and concentration of available chlorine is 1000-3,000mg/L. The disinfectant of the invention is put in water; the inorganic chloride salt reacts with the organic acid to generate hypochlorous acid, nascent state chlorine, nascent state oxygen and high redox potential which interact with each other so as to greatly improve the bactericidal function; when in use, the consentration of available chlorine falls below 280ppm, which reduces side effects such as residue and irritation. The disinfectant effervescent tablet is a monobasic solid tablet, overcomes the shortcomings existing in liquid disinfectant and binary packing disinfectant, and improves largely convenience of use.
Owner:CHINESE ACAD OF INSPECTION & QUARANTINE

Method for synthesizing acetyl tributyl citrate by using ion type catalyst

The invention relates to a method for synthesizing acetyl tributyl citrate through electrophoretic catalyst. The method comprises the steps: step one: citric acid, butanol and sodium bisulfate monohydrate are added into a reactor, and the catalyst is recycled and filtered after the cooling of the stirring reflux reaction, filtrate is neutralized by adding alkaline solution and rinsed till neutral state, then the butanol is distilled and recycled under normal pressure, and the residual water is steamed under reduced pressure to acquire crude tirbutyl citrate, and the compound decolurant of acticarbon and aluminum oxide is added into the crude tirbutyl citrat for decoloring treatment, thereby, the finished tirbutyl citrat is acquired; step two: the finished tirbutyl citrate, acetic anhydride and the sodium bisulfate monohydrate are added into the reactor, and the catalyst is filtered , cooled and recycled after 1.0-3.0 hours of stirring reaction under the temperature of 50-90 DEG C; filtrate is neutralized by adding alkaline solution and rinsed till neutral state; acetyl tributyl citrate is acquired after water phase is separated and n-butyl acetate is distilled under reduced pressure and recycled. The catalyst of the method of the invention is easily separated and recycled, the esterification process is not easily influenced by by-product, emulsification is not easy during the rinsing process and the product yield is high.
Owner:李祥庆

Copper and sulphur separation method for copper-sulphur ore

The invention provides a copper and sulphur separation method for copper-sulphur ore and relates to a method for separating copper from sulphur in copper-sulphur ore flotation rough concentrate. The copper and sulphur separation method for the copper-sulphur ore is characterized in that the steps of a treating process comprise that (1) ore grinding is conducted on copper-sulphur rough concentrate obtained through flotation; (2) after the ore grinding, a sulfur inhibitor selected from sodium sulfite, sodium metabisulfite, sodium bisulfate and sodium thiosulfate is added to the copper-sulphur rough concentrate, and a sulfur inhibition reaction is conducted; (3) a copper selective collector is added, and flotation is conducted; (4) a humate inhibitor is added to a flotation froth product; after an reaction with mixing is conducted, concentration is conducted; and (5) a humate inhibitor is added to a concentration froth product; after an reaction with mechanical mixing, concentration is conducted again, and copper concentrate separated from the sulphur is obtained. The copper and sulphur separation method for the copper-sulphur ore is simple in technology; lime and other highly alkaline inhibitors are not required to be added; required reagents are extensive in source and easy to prepare and add; the prepared reagents are good in flowability, easy to control, and not liable to block pipelines. The copper and sulphur separation method for the copper-sulphur ore is a novel copper and sulphur separation method.
Owner:BEIJING GENERAL RES INST OF MINING & METALLURGY +1

Amphoteric water-coal-slurry dispersing agent and preparation method thereof

The invention provides an amphoteric water-coal-slurry dispersing agent and a preparation method thereof. The method comprises that: after polyethyleneglycol and polymerization inhibitor hydroquinone are mixed, acrylic acid, catalyst paratoluenesulfonic acid and a water-carrying agent dimethylbenzene are sequentially added to the mixture, are heated to react and are decompressed and distilled to obtain pale brown transparent liquid; the pale brown transparent liquid is adjusted to neutrality by Na2CO3 solution, is washed by saturated NaCl solution, and is extracted by 30ml aether to obtain an intermediate product I; deionized water, sulphonate or sulfoacid, cationic monomer and sodium bisulfate are stirred and dissolved; and the intermediate product I is dripped into persulfate aqueous solution to react to obtain polymer solution of an amphoteric ionic dispersing agent. The amphoteric water-coal-slurry dispersing agent synthesized by the preparation method introduces a long-chain group on the premise that the amphotericity of the dispersing agent is maintained, and can obviously improve the electric charge condition of coal particle surface so as to change the hydrophobic property of coal surface, thereby playing an excellent effect of viscosity reduction.
Owner:SHAANXI YI HAI CHENG CHEM TECH
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