The invention discloses a continuous rectification separation device and a continuous rectification
separation method for
coal gasification crude
phenol. The device comprises a first-level pretreatment acidifying unit consisting of a film scraping
evaporator, a primary acid regulating tank group and a
buffer tank, a second-level pretreatment oxidizing unit consisting of a
static mixer and a secondary acid regulating tank and a rectifying
tower system consisting of a deslagging
tower, a dehydrating
tower, a
phenol refining tower, an o-
cresol refining tower and a m, p-
cresol refining tower, wherein the first-level pretreatment acidifying unit is connected with the
phenol deslagging tower; and the phenol deslagging tower is connected with the second-level pretreatment oxidizing unit and is connected with each rectifying tower
system respectively. By the device and the method, the
raw material of the
coal gasification crude phenol is subjected to decoloration, deodorization, desulfuration,
impurity removal and the like effectively, so that products of high-purity phenol with the purity of more than 99.5 weight percent, high-purity o-
cresol with the purity of more than 96.0 weight percent, high-purity m, p-cresol with the purity of more than 99.0 weight percent, mixed
xylenol and phenol
residual oil can be obtained. The method has the characteristics of reasonable process, high
automaticity, low process
energy consumption, high quality of products, high stability and the like, and is an efficient and feasible continuous rectification
separation process for the
coal gasification crude phenol.