The invention discloses a preparation method of
coal based needle
coke, which comprises the following steps of: 1) adding a
raw material and a
diluent into a stirring kettle, stirring and separating out the
solvent insoluble matter; 2) heating the mixed liquid in a 1# tubular
heating furnace, and feeding the mixed liquid into a pressing hot
filtration kettle; 3) filtering, filling an
inert gas, pressing and performing hot
filtration; 4) performing
centrifugal filtration of the filtrate, and feeding the obtained purified
raw material into a purified
raw material tank; 5) heating the purified raw material in the 1# tubular
heating furnace and performing reaction
tower circular condensation
polymerization, fractionating the escape component to obtain gas, light oil and heavy oil, and recycling the light oil; 6) heating the condensation
polymerization concentrate in a 2# tubular
heating furnace, coking by a
coke tower to obtain
coke, and feeding the coke oil gas into a reaction
tower; and 7) feeding the prepared green coke into a calcinator, heating and calcining to obtain the product needle coke. The content of
quinoline insoluble (QI) in the prepared refined purified
asphalt is less than 0.15%, the yield is improved by 10-20%, the coefficient of
thermal expansion of the needle coke is low, the pipeline blockage can be avoided, and the material reaction is uniform.