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71results about How to "Good alcohol solubility" patented technology

Method for producing phloretin by enzymatic hydrolysis method

The invention discloses a method for producing a phloretin by an enzymatic hydrolysis method, which comprises the following steps of: dissolving phlorizin raw materials with the phlorizin quality content of 10 percent to 80 percent in deionized water; adding activated sino-beta hydrolytic enzyme, stirring and carrying out enzymatic reaction for 5-72 hours at 20-90 DEG C, wherein the weight ratio of the phlorizin raw materials to the sino-beta hydrolytic enzyme is 1-50:1; rapidly raising temperature to 60-100 DEG C for inactivating for 15-25 min; solid-liquid separating, drying the solid to obtain the phloretin. The phlorizin in plants is taken as raw material, and the method has the advantages of easy raw materials acquisition, low price, simple production process, and easy control. In the invention, an aglycon configuration obtained by enzymolysis is not damaged and has stronger biological activity; the enzymatic hydrolysis has strong specifity, and the products obtained have little impurities; because the phloretin obtained by the method is white, the application field of the phloretin is broadened.
Owner:天津市尖峰天然产物研究开发有限公司

Alcohol-soluble molybdenum oxide interface layer material synthesis method and application

The invention discloses an alcohol-soluble molybdenum oxide interface layer material synthesis method and application. Metal molybdenum powder serves as the raw material, hydrogen peroxide serves as oxidant, organic acid is adopted as stabilizer and cosolvent, alcohol serves as a proton donor, and synthesized molybdenum oxide powder is of an amorphous structure. The invention further discloses an organic solar cell device with alcohol-soluble molybdenum oxide as an interface layer. Molybdenum oxide synthesized through the method is good in alcohol solubility and film forming performance, can evenly form a film on a transparent electrode and an organic active layer, can achieve low-temperature processing and is compatible with a flexible substrate. A molybdenum oxide modified anode interface layer can effectively achieve cavitation extraction, and greatly improves photoelectric efficiency of devices. Meanwhile, the stable material overcomes instability of electrode interfaces and organic layer interfaces to a certain extent, and accordingly stability of organic solar cells is improved.
Owner:GUILIN UNIV OF ELECTRONIC TECH +1

Heterocyclic azo metal chelate compound, their preparation and use

A heterocyclic sulphonazo metal chelate compound and its preparation method. In a phosphoric acid system, getting a diazonium salt of a nitrogen heterocyclic aromatic amine by a mild diazotization method, the diazonium salt coupling with different components, and getting a series of heterocyclic sulphonazo compounds; the heterocyclic sulphonazo compound chelating with different bivalent metal to get a series of heterocyclic sulphonazo metal chelate compounds. The heterocyclic sulphonazo metal chelate compound could produce an excellent film by spin coating, and be used for the optical storagemedium for DVD-R. The compound has a low thermal decomposition temperature ( no more than 350degree C), which is advantageous for improving sensitivity of DVD-R dyes.
Owner:INST OF CHEM CHINESE ACAD OF SCI

Preparation and application of polyelectrolyte/silver halide nanocomposite antibacterial material

A silver ion bactericide has a broad-spectrum antibacterial effect and avoids drug resistance as well as strain variation of microorganisms. Therefore, silver ions are currently an important research direction of the biomedical technology industry. According to the invention, an in-situ synthesis method is adopted for the first time to prepare a conductive conjugate polyelectrolyte/silver halide nanocomposite; and a long-acting broad-spectrum antibacterial effect is realized by adopting a silver halide nanocomposite taking the conductive conjugate polyelectrolyte as a carrier as a broad-spectrum antibacterial material and controlling the size of the silver halide nanoparticles complexed in the conductive conjugate polyelectrolyte to regulate the release rate of silver ions. In the invention, the application of the conductive conjugate polyelectrolyte in biomedicine and particularly the antibacterial field is exploited, and an antibacterial material which avoids toxic and side effects to a human body and is easy to spray and regulate and convenient to use is provided; and the antibacterial material has a broad application prospect in various conduits (catheters and air ducts), dressings and preparations as well as the long-acting mould and bacteria prevention of precise instruments.
Owner:QINGDAO INST OF BIOENERGY & BIOPROCESS TECH CHINESE ACADEMY OF SCI

Alcohol soluble high-ionic selective negative ion exchange membrane, preparation method thereof and application of exchange membrane

The invention discloses an alcohol soluble high-ionic selective negative ion exchange membrane, a preparation method thereof and an application of the exchange membrane. A material of the ion exchangemembrane is a tadpole type poly phenylene oxide ionizer PPO-DMODA with a long hydrophobic alkyl side chain, ion selective permeability is 91%-97% at the indoor temperature within the range of ion-exchange capacity of 1.38-2.0meq / g, and sheet resistance is 3.5-30.6 omega / cm<2>. According to the preparation method, the long hydrophobic alkyl side chain is introduced on a PPO (poly phenylene oxide)framework, the method solves the problem of low zwitterion selectivity of the PPO-type negative ion exchange membrane under high IEC (ion-exchange column chromatography), a tadpole type poly phenyleneoxide ionizer structure with the long hydrophobic alkyl side chain can effectively restrain water absorbing swelling of the membrane, zwitterion selective permeability of the membrane and ionic conductivity are improved, the membrane has good mechanical property and performance stability, and requirements of electrodialysis and reverse electrodialysis processes for comprehensive performances of the negative ion exchange membrane can be met.
Owner:SOUTH CHINA UNIV OF TECH

Alcohol-soluble beta-glucan extract, preparing method and application thereof and health-care wine

The invention discloses an alcohol-soluble beta-glucan extract, a preparing method and application thereof and health-care wine, and relates to the technical field of extraction of plant components. The preparing method of the alcohol-soluble beta-glucan extract comprises the steps of taking a medicinal material of hordeum vulgar L.var.nudumHook.f, adding an acid solution, and conducting acid extraction; adding alpha-amylase and glucoamylase into an acid extraction solution for enzymolysis, and then conducting enzyme denaturing to obtain an enzymolysis extraction solution; centrifuging and concentrating the enzymolysis extraction solution to obtain a concentrated solution; adding an ethanol solution into the concentrated solution for alcohol precipitation to obtain an alcohol precipitationsolution; filtering and drying the alcohol precipitation solution. The technology is simple, the operation is convenient, the production period is short, the efficiency is high, and the alcohol-soluble beta-glucan extract is suitable for industrial mass production; the alcohol solublility of the prepared alcohol-soluble beta-glucan extract is good, the alcohol-soluble beta-glucan extract can be dissolved into ethanol of different concentrations and is suitable for producing hordeum vulgar L.var.nudumHook.f beta-glucan products; the alcohol-soluble beta-glucan extract is applied to preparing the health-care wine; the health-care wind contains a large amount of hordeum vulgar L.var.nudumHook.f beta-glucan.
Owner:劲牌持正堂药业有限公司

Inverted organic solar cell adopting phthalocyanine derivative film as cathode buffer layer and preparation method thereof

The invention relates to an inverted organic solar cell adopting a phthalocyanine derivative film as a cathode buffer layer and the preparation method thereof. Crystallization order degree of phthalocyanine derivatives used as buffer layer materials is effectively controlled by solvent steam annealing processing or transfer chamber airflow annealing processing, and roughness of a film surface is reduced, and then the synthetic method of the ionic phthalocyanine derivatives ZnPc(OC8H17OPyCH3I) is simple, and ethanol soluble performance is good, and therefore an environmental-friendly non-toxic harmless ideal cathode interface material is provided. The inverted structural device provided by the invention does not contain acidic hole transfer material PEDOT:PSS and a low power function metal electrode, and therefore the efficiency and the stability of the device are improved obviously. Compared with the prior art, the preparation method is novel, preparation technology is simple, and costs are low, and therefore the effective method of improving the performance of the solar cell is provided. The 80% efficiency of the prepared organic solar cell device is maintained after 500hours, and therefore the efficiency is higher than that of conventional devices.
Owner:NANJING UNIV OF POSTS & TELECOMM

Bio-based polyurethane water-based ink and preparation method thereof

The invention provides bio-based polyurethane water-based ink and a preparation method thereof. The preparation method comprises three steps of preparation of a prepolymer, emulsification desolvation and preparation of ink resin. The bio-based polyurethane water-based ink comprises the following components: bio-based isocyanate, bio-based macromolecular polyol, polypropylene carbonate polyol, a carboxylic acid type hydrophilic chain extender, a sulfonic acid type hydrophilic chain extender and a cross-linking agent, wherein the molar ratio of the bio-based isocyanate to the bio-based macromolecular polyol to the polypropylene carbonate polyol is 3:1:0.5-6:1:0.5, the mass of the carboxylic acid type hydrophilic chain extender is 1-2% of the mass of a polyurethane prepolymer, the mass of the sulfonic acid type hydrophilic chain extender is 2-6% of the mass of the polyurethane prepolymer, and the mass of the cross-linking agent is 1.5%-5.5% of the mass of polyurethane emulsion. According to the ink, the defect that inorganic auxiliaries such as matting powder need to be added to matte resin is overcome, the scratch resistance of the resin can be improved through the added cross-linking agent, and the alcohol solubility of the water-based ink resin is also improved through the addition of the polypropylene carbonate polyol.
Owner:HEFEI KETIAN WATERBORNE TECH CO LTD +1

Preparation method of flower wine

InactiveCN113150929AWell mixedOvercome the problem of insufficient preparation technologyMicroorganism based processesWine preparationBiotechnologyAlcohol
The invention specifically discloses a preparation method of flower wine, which is prepared from 1-30kg of flower powder and 1000kg of wine by the following steps: (1) drying flowers at 35-90 DEG C until the water content is less than 3%, and crushing into 350-600-mesh powder to obtain the flower powder; (2) mixing the flower powder, saccharomycetes and water according to the weight ratio of 1: 0.25: 0.5, putting the mixture into a container, and fermenting at the temperature of 36-38 DEG C for 144-168 hours; (3) turning and stirring the fermentation material once every 3 hours in the fermentation process; (4) adding a proper amount of wine into the fermented material, mixing, and fermenting for 360 hours at the temperature of 18-25 DEG C; (5) stirring once every two hours in the fermentation process, wherein the stirring time is 5-8 minutes; (6) after fermentation is finished, carrying out reduced pressure distillation under the conditions that the pressure is-0.07 MPa to-0.1 MPa and the distillation temperature is 35-55 DEG C to obtain 10kg of alcohol liquid with the concentration of 15% V/V or above; and (7) adding 10kg of the alcohol liquid into 1000kg of wine, and uniformly stirring and mixing to obtain the flower wine. The wine is white spirit, yellow wine, grape wine or beer.
Owner:徐州绿之野生物食品有限公司

Star-like amphiphilic conjugated molecule material, and preparation method and application thereof

The invention relates to a star-like amphiphilic conjugated molecule material, and a preparation method and application thereof. The material adopts a fluorene structure as a skeleton, pyrene as a capping group and phosphonate as a polar side group and selects different alkyl chains, and the obtained star-like amphiphilic conjugated molecule compound has a structural general formula as shown in the following formula I: (the formula I is as shown in the specification), wherein R is one of alkyl, alkoxy, alkylphenyl and alkyl phenyl with phosphate; Ar is one of benzene, triphenylamine and tri-indene. The material has the advantages of simple chemical structure, low synthesis cost and the like, has high solution processability, film-forming property and multifunctional optical-electrical characteristic, and can realize high-brightness blue light emitting and efficient cathode interface modification functions simultaneously. An organic light-emitting diode which takes the material as a light-emitting layer and an interface modification layer simultaneously can realize excellent optical-electric characteristic through a simplified device structure and solves the technical problem that high-performance multi-layer devices are processed and manufactured by the solution.
Owner:NANJING UNIV OF POSTS & TELECOMM

Tobacco double-layer solid flavor ball preparation method and application thereof

The invention discloses a tobacco double-layer solid flavor ball preparation method and an application thereof. Colorless and transparent liquid polyethylene glycol with the molecular weight of 200-600 and white waxy solid polyethylene glycol with the molecular weight of 800-2000 are mixed, dissolved and then solidified in cold to form white pasty soft solid. One or a plurality of types of white solid polyethylene glycol with the molecular weight of 4000-10000 are mixed according to an optional proportion, dissolved and then solidified in cold to form white hard solid. The white pasty soft solid and the white hard solid serve as a ball core and a ball shell of a flavor ball respectively, the breakable structural characteristic of the flavor ball can be achieved, slight noise is generated when the flavor ball is broken, and participation and interestingness of a consumer smoking a cigarette are enhanced. The ball shell of the prepared flavor ball is compact in structure, flavors in the ball core can be effectively protected from volatilization, the structure of the ball core is loose when the cigarette is smoked and the flavor ball is broken, and the flavors can be taken out by smoke.
Owner:HUBEI CHINA TOBACCO IND
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