The invention discloses a preparation method of a through-hole type
lithium battery negative
electrode material, belonging to the technical field of
new energy materials. At first, that
gelatin is dissolve in
glycerol, then
titanate and
silicate are added, aft heating and stirring reaction for 3-5h, the
gelatin is concentrated unde reduced pressure, the residual
glycerol is removed, and the
gelatin is cooled to obtain a refined concentrate; 3 to 5 hour after that refine concentrate and the
sulfuric acid solution are mixed, the
hydrothermal reaction is carried out, the material is discharged, is and dried to obtain a hydrothermal carbonized material. Then the hydrothermal carbonized material is dispersed in water, nanometer
magnesium powder, nanometer
iron powder and
sodium fluoride are added, and after ultrasonic impregnation, the hydrothermal carbonized material is filtered and dried to obtain the impregnated hydrothermal carbonized material. The impregnated hydrothermal carbonized material is transferred into a
vacuum furnace, the temperature is programmed to be 1480-1500 DEG C, the
reaction temperature is preserved and vacuum reacted, then the material is cooled, discharged, washed with dilute
hydrochloric acid, washed with water and dried to obtain a through-hole type
lithium battery negative
electrode material. The through-hole type
lithium battery negative
electrode material obtained by the invention has excellent cycle performance.