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30results about How to "Simple and repeatable" patented technology

Thin film composite film taking metal organic framework as functional layer, preparation method thereof and preparation method of metal organic framework

The invention provides a preparation method of a thin film composite film taking a metal organic framework as a functional layer, which comprises the following steps: 1) mixing a metal organic framework mixed solution containing a polyamine with an alcohol to obtain a dispersion solution; (2) spraying the dispersion liquid obtained in the step (1) on a base film by utilizing a spraying technology,so that a uniform metal organic framework layer is formed on the surface of the base film; and 3) spraying a polybasic acyl chloride solution on the surface of the metal organic framework layer prepared in the step 2) by using a spraying technology, and generating a polyamide layer by using an interfacial polymerization reaction to fix the metal organic framework, thereby obtaining the thin filmcomposite film. According to the invention, the spraying technology is applied to the construction of the metal organic framework film composite film; the problems that large-scale preparation of themetal organic framework film composite film is difficult and repeatability is poor are solved, the metal organic framework film composite film with a thin functional layer and excellent dye interception performance can be prepared, and the prepared MOF film composite film has a very high industrial application prospect.
Owner:UNIV OF SCI & TECH OF CHINA

LAMP primer composition for detecting hand-foot-and-mouth disease related pathogens and related application thereof

The invention provides a LAMP primer composition for detecting hand-foot-and-mouth disease related pathogens and related application thereof. The LAMP primer composition is high in sensitivity and accuracy. Microfluidic chip technology based on a LAMP method is applied in detection of the hand-foot-and-mouth disease related pathogens, and the advantages of high flux, quickness, sensitivity and high specificity of a microfluidic chip are utilized, so that detection speed, flux and sensitivity of the hand-foot-and-mouth disease related pathogens are increased, cost is lowered greatly, and detection time is shortened.
Owner:SHANGHAI IGENETEC DIAGNOSTICS CO LTD

Method for enriching and purifying biological marker compound in high-postmature soluble organic matter

The invention provides a method for enriching and purifying a biological marker compound in a high-postmature soluble organic matter. According to the method, a methanol saturated solution of urea is utilized for complexing and purifying n-alkane in the high-postmature soluble organic matter and simultaneously enriching the biological marker compound. The method comprises the following steps: (a) preprocessing a high-postmature soluble organic matter sample, so as to obtain a saturated hydrocarbon sample; (b) concentrating the saturated hydrocarbon sample to a half-dry state, and adding the saturated hydrocarbon sample into a mixed solution of normal hexane and acetone, so as to obtain a mixed solution B; (c) adding the methanol saturated solution of urea into the mixed solution B while stirring, so as to obtain a solution C; (d) filtering the mixed solution C, so as to obtain filtrate and urea; (e) blow-drying the filtrate, carrying out drip washing by virtue of normal hexane, concentrating the filtrate into an automatic feeding bottle, and carrying out determination by virtue of GC-MS; and (f) dissolving urea with deionized water, carrying out extracting by virtue of normal hexane, concentrating extracted liquid into the automatic feeding bottle, and carrying out determination by virtue of GC-MS.
Owner:PETROCHINA CO LTD

Magnetic nanoparticle composite film and preparation method thereof

The invention discloses a magnetic nanoparticle composite film and a preparation method thereof, and belongs to the technical field of magnetic material control of film materials. In the magnetic nanoparticle composite film, the composite film is formed by continuously and alternately depositing a magnetic layer and an insulating layer, and the composite film has a thickness of 15-100 nm; and themagnetic layer is a layer film formed by uniformly embedding magnetic particles in an insulating medium, the component of the magnetic particles is Fe or Fe-Ni, the volume fraction of the magnetic particles is 80-95%, and the thickness of the magnetic layer is 1-20 nm; and the insulating layer is composed of an insulating medium and has a thickness of 0.1-10nm. The magnetic nanoparticle compositefilm prepared by the invention can control the merging and grow of the nanoparticles, the particle size and the distribution uniformity and the like, thereby improving the magnetism while realizing grain refinement. The composite film prepared by using the preparation method provided by the invention is particularly suitable for electronic components in the field of digital electronic industry andcommunication technology.
Owner:NORTHEASTERN UNIV +1

Preparation method of tetragonal-phase barium titanate ceramic powder with antibacterial property

The invention discloses a preparation method of tetragonal-phase barium titanate ceramic powder with antibacterial performance, and belongs to the technical field of ferroelectric and piezoelectric ceramic materials. The method comprises the steps: completing atomic-scale mixing of a barium source and a titanium source in a liquid-phase state by means of a liquid-phase chemical process; then, fixing the mixture in the form of a liquid precursor through a rotary evaporation reaction; and finally, carrying out a certain heat treatment process on the washed and dried precursor, thereby controllably synthesizing the tetragonal-phase barium titanate ceramic powder with good antibacterial performance. In the synthesis process, common inorganic salts and simple reagents are mainly used, so that the method is low in cost, simple and easy to implement and good in repeatability. The synthesized tetragonal-phase barium titanate ceramic powder is stable in component, narrow in size and particle size distribution, high in crystal face index, good in antibacterial performance and suitable for large-scale batch production, and a certain theoretical basis is provided for antibacterial research of ferroelectric materials.
Owner:XIAN UNIV OF TECH

Preparation method of ambroxol hydrochloride impurity reference substance

The invention discloses a preparation method of an ambroxol hydrochloride impurity reference substance. The method comprises the following steps: firstly, dissolving ambroxol hydrochloride in an appropriate amount of dichloromethane solution, then adding a quantitative aqueous solution of sodium hydrogencarbonate for uniform stirring to obtain free ambroxol, separating, drying and concentrating the organic phase, dissolving the concentrated solution in the alcohol solution, then refluxing with excess orthoformate to obtain a crude product of (1R, 4R)-4-(6,8-dibromo-3,4-dihydroquinazoline)-cyclohexanol after condensation, and obtaining a pure product after the crude product is purified by silica gel column chromatography. The invention has the creative application of orthoformate as a condensing agent. Compared with other condensing agents reported in the literature, the orthoformate has the advantages such as good stability, high safety, low cost, high product yield and easy purification.
Owner:SHANGLUO UNIV

Method for quickly detecting metrafenone in water by adopting liquid chromatography-mass spectrometry technology

The invention relates to a detecting method for residual amount of bactericide in water and specifically relates to a method for quickly detecting metrafenone in water by adopting a liquid chromatography-mass spectrometry technology. The method mainly comprises the following steps: sample pretreatment, liquid chromatogram separation and mass spectrometric detection. The specific processes of the method are as follows: filtering and purifying a sample; performing HLB column purification; gathering nitrogen; blow-drying and redissolving with acetonitrile water mixed liquor; by adopting SHIM-PACKXRODSII75L*2.0 high performance liquid chromatography as an analytical column, and taking acetonitrile-0.1% formic acid aqueous solution as a flowing phase, performing gradient elution at flow rate of 0.3ml/min; separating and detecting metrafenone in water under the mode of positive ion electrospray ionization and the mode of multi-reaction monitoring; optimizing mass spectrometry conditions andcreating optimal mass spectrometry conditions, thereby achieving the highest sensitivity of metrafenone. The detecting method has the characteristics of simple sample pretreatment steps, high extraction ratio, high accuracy, excellent purifying effect, less detection time consumption and low cost.
Owner:DALIAN VOCATIONAL & TECHN COLLEGE

Method for preparing mesoporous barium zirconate titanate ceramic nanoparticles

The invention discloses a method for preparing mesoporous barium zirconate titanate ceramic nanoparticles, and belongs to the technical field of electronic ceramic materials. According to the method, barium chloride (BaCl2) is adopted as a barium salt, zirconium oxychloride (ZrOCl2) is adopted as a zirconium source, butyl titanate (C16H36O4Ti) is adopted as a titanium source, ethylene glycol (C2H6O2) is adopted as a reaction chelating agent, under the high-concentration alkaline condition, the crystal growth speed is controlled through a rotary evaporation reaction, and the mesoporous barium zirconate titanate nanometer material is successfully prepared. In the synthesis process, common inorganic salts and simple reagents are taken as main components, so that the method is low in cost, simple, feasible, good in repeatability and suitable for large-scale production, and the commercialization process of electronic ceramic materials can be promoted.
Owner:XIAN UNIV OF TECH

Method for preparing hydroxyapatite nano rod by using egg white template

The invention discloses a method for preparing a hydroxyapatite nano rod by using an egg white template, and belongs to the technical field of biological ceramic materials. The method comprises the following steps: taking calcium chloride (CaCl2) as calcium salt, diammonium hydrogen phosphate ((NH4)2HPO4) as phosphate and ethanol amine (C2H7NO) as a reaction chelating agent, carrying out rotary evaporation reaction under a high-concentration alkaline condition to obtain an HA precursor solution, washing with water and alcohol, carrying out vacuum drying to obtain HA precursor powder, uniformly mixing and stirring the HA precursor powder and whipped egg white, placing the mixture into a drying oven, drying, and successfully preparing the hydroxyapatite nano rod through high-temperature calcination. In the synthesis process, common inorganic salts and simple reagents are mainly used, so that the method is low in cost, simple and feasible, good in repeatability, high in synthesis performance, good in stability, suitable for large-scale production and capable of promoting the commercialization process of biological ceramic materials.
Owner:XIAN UNIV OF TECH

Method for preparing LATP solid electrolyte with blocking electrode in one step at low temperature

The invention discloses a low-temperature one-step preparation method of an LATP solid electrolyte with a blocking electrode, which is characterized in that a gold foil and a green body dropwise added with a proper amount of liquid phase are co-sintered at a low temperature to solve the problems of lithium loss, impurity phase generation and the like which are easy to generate when the LATP electrolyte is sintered at a high temperature. The preparation method has the following advantages: (1) the LATP solid electrolyte can be prepared at a low temperature of 140-280 DEG C, and the process steps are simple; and (2) sintering into a sheet and a subsequent step of magnetron sputtering or silver paste coating for testing conductivity are combined into a whole, an electrolyte with a flat surface, continuous blocking electrode conductivity and uniform and controllable thickness can be realized after the sintering of the green body is completed, gold plating can be realized without magnetron sputtering, the production cost is low, a silver paste layer with a relatively large thickness is also avoided, the implementation is easy, and the production efficiency is high. The method is high in repeatability and time-saving, and is mainly used for preparing the LATP solid electrolyte with the blocking electrode on the surface in one step.
Owner:FUZHOU UNIV

A method and device for evaluating hairy dust on the surface of fabrics

The invention discloses an assess method and device for hair dust on the surface of a fabric. The device comprises a fabric fixing tube, gummed paper and a hair dust testing instrument, wherein the hair dust testing instrument comprises a support platform and a bracket which is erected on the hair dust testing instrument; the middle part of the bracket is provided with a circular hoop; the circular hoop is loosened or fastened through a locking screw on the circular hoop; a support rod at the top end of the bracket is provided with a hammer rod installation channel which corresponds to the position of the circular hoop; a hammer rod is arranged in the hammer rod installation channel; the upper end of the hammer rod is connected with a handle; the lower end of the hammer rod is connected with a hammer head; and the position of the hammer head corresponds to the inner circle of the circular hoop. The method and the device can be used for easily, conveniently, directly and accurately judging the degree of residual hair dust on the surface of the fabric, so that the defects of subjectivity and non-repeatability of human sensitive judgment are overcome. The method and the device have the advantages of easiness and convenience for operating, capability of intuitionally displaying the residual hair dust amount, easiness for judging, high objectivity, high repeatability, unified standard, increase in hair dust judging efficiency on the surface of the fabric, saving in manpower and material resource and wide application prospect.
Owner:PACIFIC (PANYU) TEXTILES LTD

Catalyst for hydroxylation reaction of phenol and preparation method thereof

The invention provides a catalyst for hydroxylation reaction of phenol and a preparation method thereof, belonging to the technical field of chemical engineering and relating to phenol hydroxylation co-production catechol and hydroquinone catalyzer as well as a preparation method thereof. The preparation method of the catalyst is characterized by comprising the following steps: adopting a hydrothermal synthesis method, and packaging phthalocyanine containing water-soluble groups in an MCM-41 channel in the form of molecule to prepare an immobilized homogeneous catalyst. The effects and the benefits of the invention are as follows: the preparation process of the catalyst is simple and has good repeatability; the phthalocyanine packaged in the MCM-41 channel exists in the form of molecule; metal ions or ligands without being subject to complexation do not exit in the MCM-41 channel; the phthalocyanine on the outer surface of the MCM-41 channel is easy to be eliminated; and the prepared catalyst has high capacity and good ordered channel. The catalyst has the advantages that the homogeneous catalyst has mild reaction conditions, high reactivity and good selectivity, and heterogeneouscatalyst is easy to be separated from a product and can be used repeatedly.
Owner:DALIAN UNIV OF TECH

Thin film composite film with metal-organic framework as functional layer, preparation method thereof, and preparation method of metal-organic framework

The invention provides a method for preparing a thin film composite membrane with a metal-organic framework as a functional layer, comprising the following steps: 1) mixing a mixed solution of a metal-organic framework containing polyamines with alcohol to obtain a dispersion; 2) mixing step 1) The obtained dispersion is sprayed on the base film by spraying technology, so that the surface of the base film forms a uniform metal-organic framework layer; 3) spraying the polyacyl chloride solution on the surface of the metal-organic framework layer prepared in step 2) by spraying technology, The interfacial polymerization reaction is used to form a polyamide layer to fix the metal-organic framework to obtain a thin film composite membrane. The present invention applies the spraying technology to the construction of metal-organic framework thin film composite membranes, overcomes the problems of difficult scale-up and poor repeatability in the preparation of metal-organic framework thin-film composite membranes, and can prepare thinner functional layers and excellent dye retention performance The metal-organic framework thin film composite membrane prepared by MOF thin film composite membrane has a high industrial application prospect.
Owner:UNIV OF SCI & TECH OF CHINA
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