The invention discloses a preparation method for a composite magnetic
chitosan adsorption material. The preparation method comprises the steps that magnetic
chitosan is dispersed in deionized water,
diethylenetriamine is added, uniform shaking is carried out, then activated
nitrilotriacetic acid is added, uniform mixing is carried out, then the mixture is put into a high-temperature condition forreaction, then washing is carried out with deionized water, and
drying is carried out so as to obtain the composite magnetic
chitosan adsorption material, wherein the
mass volume ratio of the magneticchitosan to a
diethylenetriamine solution is 1 g:10-120 mL, and the
mass ratio of the magnetic chitosan to
nitrilotriacetic acid is 1:0.1-5. The adsorption material prepared through the method has the advantages of being excellent in adsorption capacity, high in stability and easy to separate and recycle; and in addition, the method has the advantages of being simple and easy to operate, low in instrument and
equipment requirement and short in preparation period. The invention also provides application of the composite magnetic chitosan adsorption material in removal of
tetracycline antibiotics in water. According to the application of the composite magnetic chitosan adsorption material, the
tetracycline antibiotics include but are not limited to
tetracycline,
chlortetracycline,
oxytetracycline and
doxycycline.