The invention belongs to the technical field of synthesis of a
molecular sieve material, and relates to a nanoscale sheet-SAPO-34
molecular sieve and a synthetizing method thereof. The nanoscale sheet-SAPO-34
molecular sieve is mainly prepared from synthetizing an aluminum source, a
phosphorus source, a
silicon source, a formwork agent and water, wherein the aluminum source is pseudo-
boehmite; the formwork agent is a composite formwork agent consisting of a first formwork agent and a second formwork agent; the
molar ratios of the components forming
sol are shown as follows: 1 part of Al2O3 is used as a standard, 0.8-1.2 parts of P2O5, 0.2-1.0 part of SiO2, 2-4 parts of the first formwork agent, 0.1-0.2 part of the second formwork agent, and 20-100 parts of H2O. According to the nanoscale sheet-SAPO-34 molecular
sieve and the synthetizing method thereof, disclosed by the invention, a composite
phosphorus source and a composite formwork agent are adopted, a hydrothermal method is adopted for one-step synthetizing SAPO-34 sheet-nanometer crystals, the process is simple, and cetyl trimethyl
ammonium bromide(CTAB) is a frequently-used surfactant for industrial use, and is low in cost. The thickness of the prepared SAPO-34 molecular
sieve is only scores of nanometers, and the
diffusion path of molecules is obviously shortened.